摘要
介绍了一种直接从原材料合成二苯甲酰甲烷钙配合物[Ca(DBM)_2]的方法 ,并对产品进行X射线衍射(XRD)、红外光谱FTIR、热重分析方法表征。
This paper introduces a direct synthesis method of calcium dibenzoylmethane complexes from the?raw materials and the structures of the product are characterized by the XRD, FTIR and thermogravimetric analysis methods.
引文
[1]Naida El Habra,Franco Benetollo,Maurizio Casarin.Synthesis and Characterizati-on of Calciumβ-diketonate complexes.X-Ray Crystal and Molecular Structures of:[{Ca(tmhd)2}2(18-crown-6)],[Ca(dpp)2(thf)2]and[Ca(dpp)2(triglyme)][J].Dalton Trans.,2010,39:8064-8070.
[2]王道永.双β-二酮金属配合物的合成、表征及性质研究[D].西安:西北大学,2005.
[3]殷树梅.二苯甲酰甲烷的合成及应用[J].化学中间体,2009,(8):10-13
[4]时永莉,吴世康.一种新型的紫外光吸收剂[J].高分子学报,1989,(6):924-939.
[5]梅光象,曾锦萍,袁晓玲,等.二苯甲酰甲烷的合成与热稳定性研究[J].宝鸡文理学院学报,2008,28(4):283-286.