核磁共振法检测地沟油的研究进展
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摘要
核磁共振法由于测量速度快、准确、重复性高等优点适合用于餐饮业废弃油脂的快速检测。综述核磁共振技术的基本原理、类别、检测地沟油的方法、以及我国利用核磁共振法检测地沟油的研究进展,为食品安全分析检测行业的科技工作者提供新技术和新思路,以期为寻找准确、快速检测地沟油的方法提供参考。
Because of the advantages of quickness,high accuracy,good repeatability nuclear magnetic resonance(NMR) has been applied in hogwash oil detection. The basic principle,classification,detection method and research progress in hogwash oil of NMR technique were introduced. The literature on hogwash oil in domestic and summarized the different analysis methods by NMR in order to give a reference on the further study about hogwash oil detection.
Because of the advantages of quickness,high accuracy,good repeatability nuclear magnetic resonance(NMR) has been applied in hogwash oil detection. The basic principle,classification,detection method and research progress in hogwash oil of NMR technique were introduced. The literature on hogwash oil in domestic and summarized the different analysis methods by NMR in order to give a reference on the further study about hogwash oil detection.
引文
〔1〕何艳妮,唐伟卓,赵余庆.地沟油检测方法的研究进展[J].食品研究与开发,2013,34(13):103–106.
〔2〕李沂光,单杨,李高阳,等.地沟油检测方法研究现状与其应用分析[J].食品与机械,2012,28(3):262–265.
〔3〕陈敏,王世平.食品掺伪检验技术[M].北京:化学工业出版社,2006:10.
〔4〕杨静,朱毅,于新,等.地沟油检测技术及资源化利用研究进展[J].中国食品学报,2013,13(6):185–190.
〔5〕沈雄,郑晓,何东平.餐饮业废弃油脂鉴别检测方法研究进展[J].粮油食品科技,2011,19(4):22–35.
〔6〕崔晓举,蒋世云,张夏辉,等.地沟油检测技术研究进展[J].化学分析计量,2013,22(2):100–104.
〔7〕齐银霞,成坚,王琴.核磁共振技术在食品检测方面的应用[J].食品与机械,2008,24(6):117–120.
〔8〕Nanassy A J.Use of wide line NMR for measurement of moisture content in food[J].Food Sci.,1973,5(3):187–197.
〔9〕Chambers J,Mckevitt N J,Scdamore K A,et al.Nondestructive determination of the moisture content of individual wheat granis by nuclear magnetic resonance[J].J.Sci.Food Agric.,1989,49:2–11.
〔10〕Tollner E W,Hung Y C.Low resolution pulse magnetic resonance for measuring moisture in slected grains and kernels[J].J.Agric.Engineering Res.,1992,53:195–199.
〔11〕Clark C J,Macfall J S,Bieleski R L.Amelioration of water core in Fuji apple viewed by two–and three dimensional nuclear magnetic resonance imaging[R].Taupa:Proc Postharvest'96,1996:76.
〔12〕Clark C J,Hockings P D,Joyce D C,et al.Appliceation of magnetic resonance imaging to pre–and post–harvest studies of fruits and vegetables[J].Postharvest Biology and Technology,1997,11(1):1–21.
〔13〕Barreiro P,Ortiz C,Ruiz–altisent M,et al.Mealiness assessment in apples and peaches using MRI techniques[J].Magnetic Resonance Imaging,2000,18(9):1175–1181.
〔14〕Chaland B,Mariette F,Marchal P,et al.1H nuclear magtnetic resonance relaxometric characterization of fat and water states in soft and hard cheese[J].Journal of Dairy Research,2000,67(4):609–618.
〔15〕Toussaint C,Medale F,Davenel A,et al.Determination of the lipid content in fish muscle by a self–calibrated NMR relaxometry method:comparison with classical chemical extraction methods[J].J.Sci.Food Agric.,2002,82(2):173–178.
〔16〕Pedersen H T,Berg H,Landby F,et al.The multivariate advantage in fat determination in meat by bench–top NMR[J].Innovative Food Science and Energing Technologies,2001,(22):87–94.
〔17〕Marciani L.Fat emulsification measured using NMR transverse relaxation[J].Journal of Magnetic Resonance,2001,153(1):1–6.
〔18〕彭树美,林向阳,阮榕生,等.核磁共振及成像技术在食品工业中的应用[J].食品科学,2008,29(11):712–716.
〔19〕Parker T,Limer E,Watson A D,et al.60 MHz 1H NMR spectroscopy for the analysis of edible oils[J].Trends in Analytical Chemistry,2014(57):147–158.
〔20〕黄慧英,胡友恒,杨朝勇,等.一种地沟油的检测方法:中国102706915 A[P].
〔21〕万娟,陈中,杨晓泉.核磁共振技术及其在食品加工中的应用[J].食品与药品,2006,8(11A):17–19.
〔22〕黄东雨,黄雪莲,卢雪华,等.核磁共振技术在食品工业中的应用[J].食品研究与开发,2010,31(11):220–223.
〔23〕周航,李泽荣,李保国.核磁共振技术在食品品质分析中的研究进展[J].农产品加工,2009,166(3):47–49.
〔24〕阮榕生.核磁共振技术在食品和生物体系中的应用[M].北京:中国轻工业出版社,2009.
〔25〕邵小龙,宋伟,李云飞.粮油食品低场核磁共振检测技术研究进展[J].中国粮油学报,2013,28(7):114–118.
〔26〕杜美红,孙永军.低分辨核磁共振技术在食品安全分析检测中的应用[J].食品工业科技,2013:34(21):374–376.
〔27〕夏天兰,刘登勇,徐幸莲,等.低场核磁共振技术在肉与肉制品水分测定及其相关品质特性中的应用[J].食品科学,2011,32(21):253–256.
〔28〕田靖,王玲.核磁共振技术在农业中的应用研究进展[J].江苏农业科学,2015,43(1):12–15.
〔29〕卢海燕,王欣,赵婷婷,等.“地沟油”常见检测方法及低场核磁共振法的研究进展[J].食品安全质量检测学报,2013,4(5):1428–1436.
〔30〕蔡波太,袁龙飞,周影,等.基于1H NMR指纹图谱结合多变量分析的地沟油检测方法[J].中国科学:化学,2013,43(5):558–567.
〔31〕许秀丽,任荷玲,李娜.核磁共振技术在地沟油鉴别中的应用研究[J].检验检疫学刊,2012(4):25–35.
〔32〕黄慧英,胡友恒,杨朝勇,等.一种地沟油的检测方法:中国,102706915 A[P].
〔33〕王士桥,王强.核磁共振结合模式识别方法鉴别食用油品质的方法,中国发明专利,CN 102269720 A[P].
〔34〕王乐,黎勇,胡健华.核磁共振法鉴别食用植物油掺伪餐饮业废油脂[J].中国油脂,2008,33(10):75–77.
〔35〕陈兆圆,李方实.地沟油检测方法的研究进展[J].食品研究与开发,2014,35(8):129–132.
〔36〕周凝,刘宝林,王欣,等.米糠毛油掺伪食用植物油的低场核磁共振检测[J].食品与发酵工业,2011,37(3):177–181.
〔37〕赵婷婷,王欣,卢海燕,等.基于低场核磁共振(LF–NMR)弛豫特性的油脂品质检测研究[J].食品工业科技,2014,35(12):58–65.
〔38〕王永巍,王欣,刘宝林,等.低场核磁共振技术检测煎炸油品质[J].食品科学,2012,33(6):171–175.
〔39〕杨培强,王欣,刘宝林,等.低场核磁共振鉴别食用油品质的方法:中国,101975788 A[P].
〔2〕李沂光,单杨,李高阳,等.地沟油检测方法研究现状与其应用分析[J].食品与机械,2012,28(3):262–265.
〔3〕陈敏,王世平.食品掺伪检验技术[M].北京:化学工业出版社,2006:10.
〔4〕杨静,朱毅,于新,等.地沟油检测技术及资源化利用研究进展[J].中国食品学报,2013,13(6):185–190.
〔5〕沈雄,郑晓,何东平.餐饮业废弃油脂鉴别检测方法研究进展[J].粮油食品科技,2011,19(4):22–35.
〔6〕崔晓举,蒋世云,张夏辉,等.地沟油检测技术研究进展[J].化学分析计量,2013,22(2):100–104.
〔7〕齐银霞,成坚,王琴.核磁共振技术在食品检测方面的应用[J].食品与机械,2008,24(6):117–120.
〔8〕Nanassy A J.Use of wide line NMR for measurement of moisture content in food[J].Food Sci.,1973,5(3):187–197.
〔9〕Chambers J,Mckevitt N J,Scdamore K A,et al.Nondestructive determination of the moisture content of individual wheat granis by nuclear magnetic resonance[J].J.Sci.Food Agric.,1989,49:2–11.
〔10〕Tollner E W,Hung Y C.Low resolution pulse magnetic resonance for measuring moisture in slected grains and kernels[J].J.Agric.Engineering Res.,1992,53:195–199.
〔11〕Clark C J,Macfall J S,Bieleski R L.Amelioration of water core in Fuji apple viewed by two–and three dimensional nuclear magnetic resonance imaging[R].Taupa:Proc Postharvest'96,1996:76.
〔12〕Clark C J,Hockings P D,Joyce D C,et al.Appliceation of magnetic resonance imaging to pre–and post–harvest studies of fruits and vegetables[J].Postharvest Biology and Technology,1997,11(1):1–21.
〔13〕Barreiro P,Ortiz C,Ruiz–altisent M,et al.Mealiness assessment in apples and peaches using MRI techniques[J].Magnetic Resonance Imaging,2000,18(9):1175–1181.
〔14〕Chaland B,Mariette F,Marchal P,et al.1H nuclear magtnetic resonance relaxometric characterization of fat and water states in soft and hard cheese[J].Journal of Dairy Research,2000,67(4):609–618.
〔15〕Toussaint C,Medale F,Davenel A,et al.Determination of the lipid content in fish muscle by a self–calibrated NMR relaxometry method:comparison with classical chemical extraction methods[J].J.Sci.Food Agric.,2002,82(2):173–178.
〔16〕Pedersen H T,Berg H,Landby F,et al.The multivariate advantage in fat determination in meat by bench–top NMR[J].Innovative Food Science and Energing Technologies,2001,(22):87–94.
〔17〕Marciani L.Fat emulsification measured using NMR transverse relaxation[J].Journal of Magnetic Resonance,2001,153(1):1–6.
〔18〕彭树美,林向阳,阮榕生,等.核磁共振及成像技术在食品工业中的应用[J].食品科学,2008,29(11):712–716.
〔19〕Parker T,Limer E,Watson A D,et al.60 MHz 1H NMR spectroscopy for the analysis of edible oils[J].Trends in Analytical Chemistry,2014(57):147–158.
〔20〕黄慧英,胡友恒,杨朝勇,等.一种地沟油的检测方法:中国102706915 A[P].
〔21〕万娟,陈中,杨晓泉.核磁共振技术及其在食品加工中的应用[J].食品与药品,2006,8(11A):17–19.
〔22〕黄东雨,黄雪莲,卢雪华,等.核磁共振技术在食品工业中的应用[J].食品研究与开发,2010,31(11):220–223.
〔23〕周航,李泽荣,李保国.核磁共振技术在食品品质分析中的研究进展[J].农产品加工,2009,166(3):47–49.
〔24〕阮榕生.核磁共振技术在食品和生物体系中的应用[M].北京:中国轻工业出版社,2009.
〔25〕邵小龙,宋伟,李云飞.粮油食品低场核磁共振检测技术研究进展[J].中国粮油学报,2013,28(7):114–118.
〔26〕杜美红,孙永军.低分辨核磁共振技术在食品安全分析检测中的应用[J].食品工业科技,2013:34(21):374–376.
〔27〕夏天兰,刘登勇,徐幸莲,等.低场核磁共振技术在肉与肉制品水分测定及其相关品质特性中的应用[J].食品科学,2011,32(21):253–256.
〔28〕田靖,王玲.核磁共振技术在农业中的应用研究进展[J].江苏农业科学,2015,43(1):12–15.
〔29〕卢海燕,王欣,赵婷婷,等.“地沟油”常见检测方法及低场核磁共振法的研究进展[J].食品安全质量检测学报,2013,4(5):1428–1436.
〔30〕蔡波太,袁龙飞,周影,等.基于1H NMR指纹图谱结合多变量分析的地沟油检测方法[J].中国科学:化学,2013,43(5):558–567.
〔31〕许秀丽,任荷玲,李娜.核磁共振技术在地沟油鉴别中的应用研究[J].检验检疫学刊,2012(4):25–35.
〔32〕黄慧英,胡友恒,杨朝勇,等.一种地沟油的检测方法:中国,102706915 A[P].
〔33〕王士桥,王强.核磁共振结合模式识别方法鉴别食用油品质的方法,中国发明专利,CN 102269720 A[P].
〔34〕王乐,黎勇,胡健华.核磁共振法鉴别食用植物油掺伪餐饮业废油脂[J].中国油脂,2008,33(10):75–77.
〔35〕陈兆圆,李方实.地沟油检测方法的研究进展[J].食品研究与开发,2014,35(8):129–132.
〔36〕周凝,刘宝林,王欣,等.米糠毛油掺伪食用植物油的低场核磁共振检测[J].食品与发酵工业,2011,37(3):177–181.
〔37〕赵婷婷,王欣,卢海燕,等.基于低场核磁共振(LF–NMR)弛豫特性的油脂品质检测研究[J].食品工业科技,2014,35(12):58–65.
〔38〕王永巍,王欣,刘宝林,等.低场核磁共振技术检测煎炸油品质[J].食品科学,2012,33(6):171–175.
〔39〕杨培强,王欣,刘宝林,等.低场核磁共振鉴别食用油品质的方法:中国,101975788 A[P].