利用XCT技术检测水泥基材料微观结构的研究进展
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摘要
本文归纳了X射线计算机断层扫描技术扫描及重构的工作原理,总结并讨论了该技术在划分材料内部组分、水泥水化过程跟踪、孔结构及细观裂缝判定、外界侵蚀物质迁移造成的微观结构变化和钢筋锈蚀开裂等领域的最新研究进展,介绍了世界上最新XCT仪器研究水泥基材料孔结构实时变化的实例。最后,对今后XCT技术在定量研究水泥基材料微观结构变化的研究方向提出了建议。
In this review,scanning and reconstruction principles of XCT are introduced. The latest progress of XCT application on determination of ce-ment components,tracking of cement hydration process,identification of pore structure and micro-crack,change in microstructure due to ingress of external substances and formation of cracks caused by corrosion of reinforcement are presented. Subsequently,an example of using the most advanced XCT on testing development of pore structure is raised. Finally,existing problems on the application of XCT in testing microstructure development of cementitious materials that need to be solved are recommended.
In this review,scanning and reconstruction principles of XCT are introduced. The latest progress of XCT application on determination of ce-ment components,tracking of cement hydration process,identification of pore structure and micro-crack,change in microstructure due to ingress of external substances and formation of cracks caused by corrosion of reinforcement are presented. Subsequently,an example of using the most advanced XCT on testing development of pore structure is raised. Finally,existing problems on the application of XCT in testing microstructure development of cementitious materials that need to be solved are recommended.
引文
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2 Bertin E P.Principles and practice of X-Ray spectrometric analysis,Plenum,New York,2012.
3 Kalender.Computer tomography,People's Health Publishing House,China,2003(in Chinese).Kalender.计算机体层成像,人民卫生出版社,2003.
4 Wan K,Chen L,Xu Q.Science China Technological Sciences,2015,58(3),485.
5 Herman.Reconstruct image from projection—the theoretical basis of CT,Science Press,China,1985(in Chinese).Herman.由投影重建图像—CT 的理论基础,科学出版社,1985.
6 Wesley D B,Ana D,Hannelore D.Applied Clay Science,2015,118,258.
7 Lechner P,Eckbauer S,Hartmann R,et al.Nuclear Instruments & Methods in Physics Research Section a-Accelerators Spectrometers Detectors and Associated Equipment,1996,377(2-3),346.
8 Boin M,Haibel A.Optics Express,2006,14(25),12071.
9 Moradian M,Hu Q,Aboustait M,et al.Materials & Design,2017,136(Supplement C),137.
10 Kak A C.Principles of computerized tomographic imaging,IEEE Press,New York,1988.
11 Zhang M Z,He Y J,Ye G,et al.Construction and Building Materials,2012,27(1),472.
12 Trtik P,Diaz A,Guizar-Sicairos M,et al.Cement Concrete Composites,2013,36,71.
13 You T,Abu Al-Rub R K,Darabi M K,et al.Construction and Building Materials,2012,28(1),531.
14 Silva D A,Monteiro P J M.Cement and Concrete Research,2006,36(8),1501.
15 Parisatto M,Dalconi M C,Valentini L,et al.Journal of Materials Science,2015,50(4),1805.
16 Cuesta A,De la Torre AG,Santacruz I,et al.Journal of Physical Che-mistry,2017,121(5),3044.
17 Garboczi E J,Bentz D P.Journal of Materials Science,1992,27(8),2083.
18 Bentz D P,Mizell S,Satterfield S,et al.Journal of Research of the National Institute of Standards and Technology,2002,107(2),137.
19 Chotard T J,Boncoeur-Martel M P,Smith A,et al.Cement Concrete Comp,2003,25(1),145.
20 Mehta P K.Concrete:Microstructure,properties and Materials,McGraw-Hill,New York,2006.
21 Jia Y D,Yan P Y.Journal of the Chinese Ceramic Society,2010,38(7),1346(in Chinese).贾耀东,阎培渝.硅酸盐学报,2010,38(7),1346.
22 Bentz D P,Quenard D A,Kunzel H M,et al.Materials and Structures,2000,33,147.
23 Ren W Y,Yang Z J,Huang Y J.Journal of Hydraulic Engineering,2015(4),452(in Chinese).任文渊,杨贞军,黄宇劼.水利学报,2015(4),452.
24 Johns R A,Steude J S,Castanier L M,et al.Journal of Geophysical Research-Solid Earth,1993,98(B2),1889.
25 Yuan Q,Junrui C,Weihua D,et al.Journal of Civil Engineering and Management,2016,22(6),792.
26 Bossa N,Chaurand P,Vicente J,et al.Cement and Concrete Research,2015,67,138.
27 Wang Y S,Dai J G.NDT & E International,2017,86,28.
28 Chung S Y,Abd Elrahman M,Stephan D,et al.Construction and Buil-ding Materials,2016,118,204.
29 Kim K Y,Yun T S,Park K P.Cement and Concrete Research,2013,50,34.
30 Promentilla M A B,Cortez S M,Papel R A D,et al.Materials (Basel),2016,9(5),388.
31 Stovall T,De Larrard F,Buil M.Powder Technology,1986,48(1),1.
32 Sugiyama T,Promentilla M A B,Hitomi T,et al.Cement and Concrete Research,2010,40(8),1265.
33 Darma I S,Sugiyama T,Promentilla M A B.Journal of Advanced Concrete Technology,2013,11(10),266.
34 Bullard J W,Jennings H M,Livingston R A,et al.Cement and Concrete Research,2011,41(12),1208.
35 Prade F,Fischer K,Heinz D,et al.Scientific Reports,2016,6,29108.
36 Prade F,Chabior M,Malm F,et al.Cement and Concrete Research,2015,74,19.
37 Bennett E E,Kopace R,Stein A F,et al.Medical Physics,2010,37(11),6047.
38 Burlion N,Bernard D,Chen D.Cement and Concrete Research,2006,36(2),346.
39 Alonso C,Andrade C,Rodriguez J,et al.Materials and Structures,1998,31(211),435.
40 Dong B,Fang G,Liu Y,et al.Cement and Concrete Research,2017,100,311.
41 Michel A,Pease B J,Geiker M R,et al.Cement and Concrete Research,2011,41(11),1085.
42 Sun H F,Zhao D D,Li G H,et al.Journal of Chinese Electronic Microscopy Society,2015,34(6),514(in Chinese).孙红芳,赵钿钿,李冠桦,等.电子显微学报,2015,34(6),514.