大块充填树脂吸水性与溶解性的比较研究
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摘要
目的:比较4种大块充填树脂和1种普通复合树脂的溶解性和吸水性。方法:参照ISO 4049标准,实验选取4种大块充填树脂和1种普通复合树脂为研究对象,分别为Tetric N-Ceram Bulk Fill(TEBF),3M ESPE Filtek Bulk Fill(FBF),X-tra fil(XT),Sure Fil1 SDR Flow(SDR)和3M ESPE Filtek Z350(Z350)。制备圆柱型(d=6 mm,h=4mm)试件30个,每种材料制备6个试件。将试件浸入蒸馏水中4周,根据重量变化计算每种树脂的溶解值和吸水值。结果:5种材料的吸水值顺序由大到小为:SDR、FBF、Z350、TEBF、XT。各材料间差异有统计学意义(P<0. 05)。5种材料溶解值顺序由大到小为:SDR、TEBF、Z350、FBF、XT,其中XT溶解值最小,其余4组间差异无统计学意义(P>0. 05)。结论:低黏度大块充填树脂的吸水值大于普通复合树脂和高黏度大块充填树脂,4种大块充填树脂和Z350普通复合树脂在溶解性方面无明显差异。
Objective: To compare the solubility and water absorption of four kinds of bulk-fill resin and one kind of common composite resin,and explore the influence factors and significance. Methods: According to the ISO 4049 standard,four bulk-fill resins and one common composite resin were selected as the research objects,namely Tetric N-Ceram Bulk Fill( TEBF),3 M ESPE Filtek Bulk Fill( FBF),X-tra fil( XT),Sure Fil1 SDR Flow( SDR) and 3 M ESPE Filtek Z350( Z350).Totally 30 Cylindrical( d = 6 mm,h = 4 mm) test pieces were prepared and dixided into 5 groups.The test piece was immersed in distilled water for 4 weeks,and the dissolution value and water absorption value of each resin were calculated according to the change in weight.Results: The order of water absorption of the 5 materials was from large to small that SDR,FBF,Z350,TEBF and XT.The difference between the materials was statistically significant( P<0. 05).The order of dissolution values of the five materials was from large to small that SDR,TEBF,Z350,FBF and XT.XT dissolution value was the smallest,and the difference between the other four groups was not statistically significant( P>0. 05).Conclusion: The water absorption of lowviscosity bulk-fill resin is larger than that of ordinary composite resin and high-viscosity bulk-fill resin.The four bulk-fill resins and Z350 ordinary composite resin have no significantly different on solubility.
Objective: To compare the solubility and water absorption of four kinds of bulk-fill resin and one kind of common composite resin,and explore the influence factors and significance. Methods: According to the ISO 4049 standard,four bulk-fill resins and one common composite resin were selected as the research objects,namely Tetric N-Ceram Bulk Fill( TEBF),3 M ESPE Filtek Bulk Fill( FBF),X-tra fil( XT),Sure Fil1 SDR Flow( SDR) and 3 M ESPE Filtek Z350( Z350).Totally 30 Cylindrical( d = 6 mm,h = 4 mm) test pieces were prepared and dixided into 5 groups.The test piece was immersed in distilled water for 4 weeks,and the dissolution value and water absorption value of each resin were calculated according to the change in weight.Results: The order of water absorption of the 5 materials was from large to small that SDR,FBF,Z350,TEBF and XT.The difference between the materials was statistically significant( P<0. 05).The order of dissolution values of the five materials was from large to small that SDR,TEBF,Z350,FBF and XT.XT dissolution value was the smallest,and the difference between the other four groups was not statistically significant( P>0. 05).Conclusion: The water absorption of lowviscosity bulk-fill resin is larger than that of ordinary composite resin and high-viscosity bulk-fill resin.The four bulk-fill resins and Z350 ordinary composite resin have no significantly different on solubility.
引文
[1]陈丽红.几种大体积充填树脂边缘微渗漏及机械性能研究[D].石家庄:河北医科大学,2016.
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[3]Yousaf A,Aman N,Manzoor MA,et al.Postoperative sensitivity of self etch versus total etch adhesive[J].J Coll Physicians Surg Pak,2014,24(6):383-386.
[4]潘悦萍,夏文薇.声波充填术与分层充填术对树脂微渗漏的影响[J].口腔医学研究,2015,31(12):1203-1205.
[5]Misilli T,G9nülol N.Water sorption and solubility of bulk-fill composites polymerized with a third generation LED LCU[J].Braz Oral Res,2017,31:e80.
[6]De IMP,Neves das LE,De CS,et al.A comparative effect of mouthwashes with different alcohol concentrations on surface hardness,sorption and solubility of composite resins[J].Oral Health Dent Manag,2014,13(2):502-506.
[7]Wei YJ,Silikas N,Zhang ZT,et al.Diffusion and concurrent solubility of self-adhering and new resin-matrix composites during water sorption/desorption cycles[J].Dent Mater,2011,27(2):197-205.
[8]Ozer S,Tunc ES,Tuloglu N,et al.Solubility of two resin composites in different mouthrinses[J].Biomed Res Int,2016,2014(2):580675.
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[10]Bociong K,Szczesio A,Sokolowski K,et al.The influence of water sorption of dental light-cured composites on shrinkage stress[J].Materials,2017,10(10):1142.
[11]于健.水浸泡老化对低收缩光固化复合树脂表面硬度的影响[D].长春:吉林大学,2016.
[12]De AMD,Ce DSB,Ambrosano GM,et al.Effect of curing light distance and different mouthwashes on the sorption and solubility of a nanofilled composite[J].Eur J Esthet Dent,2013,8(1):88-102.
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[14]Lopes LG,Jardim ADV,Souza JBD,et al.Influence of pulse-delay curing on sorption and solubility of a composite resin[J].J of Appl Oral Sci,2009,17(1):27-31.
[15]Leal JP,Da SJ,Rfm L,et al.Effect of Mouthwashes on Solubility and Sorption of Restorative Composites[J].Int J Dent,2017,2017:1-5.
[16]严敏,冯丹,高平,等.6种光固化复合树脂吸水性、溶解性和单体释放量的比较[J].吉林大学学报(医学版),2018,44(1):45-51.
[17]Alrahlah A,Silikas N,Watts DC.Hygroscopic expansion kinetics of dental resin-composites[J].Dent Mater,2014,30(2):143-148.
[18]Khokhar ZA,Razzoog ME,Yaman P.Color stability of restorative resins[J].Quintessence Int,1991,22(9):733.
[19]Sideridou ID,Karabela MM,Ech V.Dynamic thermomechanical properties and sorption characteristics of two commercial light cured dental resin composites[J].Dent Mater,2008,24(6):737-743.
[20]Sideridou I,Tserki V,Papanastasiou G.Study of water sorption,solubility and modulus of elasticity of light-cured dimethacrylate-based dental resins[J].Biomaterials,2003,24(4):655-665.
[21]Ortengren U,Wellendorf H,Karlsson S,et al.Water sorption and solubility of dental composites and identification of monomers released in an aqueous environment[J].J Oral Rehabil,2001,28(12):1106-1115.
[22]Ortengren U,Andersson F,Elgh U,et al.Influence of pH and storage time on water sorption and solubility of composite materials[J].J Dent,2001,29(1):35-41.
[23]Chaves LP,Júnior O B,Manso A P,et al.Water interaction with dental luting cements by means of sorption and solubility[J].Braz Dent Sci,2013,15(4):29-35.
[24]Mortier E,Gerdolle DA,Jacquot B,et al.Importance of water sorption and solubility studies for couple bonding agent--resin-based filling material[J].Oper Dent,2004,29(6):669.
[25]Ferracane JL.Elution of leachable components from composites[J].J O-ral Rehabil,1994,6(4):282-287.
[26]Tanaka K,Taira M,Shintani H,et al.Residual monomers(TEGDMAand Bis-GMA)of a set visible-light-cured dental composite resin when immersed in water[J].J Oral Rehabil,1991,18(4):353-362.
[2]Khan TN,Ali Abidi SY,Nawaz Khan KB,et al.Micromechanical intervention in sandwich restoration[J].J Coll Physicians Surg Pak,2015,25(11):781-784.
[3]Yousaf A,Aman N,Manzoor MA,et al.Postoperative sensitivity of self etch versus total etch adhesive[J].J Coll Physicians Surg Pak,2014,24(6):383-386.
[4]潘悦萍,夏文薇.声波充填术与分层充填术对树脂微渗漏的影响[J].口腔医学研究,2015,31(12):1203-1205.
[5]Misilli T,G9nülol N.Water sorption and solubility of bulk-fill composites polymerized with a third generation LED LCU[J].Braz Oral Res,2017,31:e80.
[6]De IMP,Neves das LE,De CS,et al.A comparative effect of mouthwashes with different alcohol concentrations on surface hardness,sorption and solubility of composite resins[J].Oral Health Dent Manag,2014,13(2):502-506.
[7]Wei YJ,Silikas N,Zhang ZT,et al.Diffusion and concurrent solubility of self-adhering and new resin-matrix composites during water sorption/desorption cycles[J].Dent Mater,2011,27(2):197-205.
[8]Ozer S,Tunc ES,Tuloglu N,et al.Solubility of two resin composites in different mouthrinses[J].Biomed Res Int,2016,2014(2):580675.
[9]Alshali RZ,Salim NA,Satterthwaite JD,et al.Long-term sorption and solubility of bulk-fill and conventional resin-composites in water and artificial saliva[J].J Dent,2015,43(12):1511-1518.
[10]Bociong K,Szczesio A,Sokolowski K,et al.The influence of water sorption of dental light-cured composites on shrinkage stress[J].Materials,2017,10(10):1142.
[11]于健.水浸泡老化对低收缩光固化复合树脂表面硬度的影响[D].长春:吉林大学,2016.
[12]De AMD,Ce DSB,Ambrosano GM,et al.Effect of curing light distance and different mouthwashes on the sorption and solubility of a nanofilled composite[J].Eur J Esthet Dent,2013,8(1):88-102.
[13]Almeida GS,Poskus LT,Guimar2￡Es JG,et al.The effect of mouthrinses on salivary sorption,solubility and surface degradation of a nanofilled and a hybrid resin composite[J].Oper Dent,2010,35(1):105-111.
[14]Lopes LG,Jardim ADV,Souza JBD,et al.Influence of pulse-delay curing on sorption and solubility of a composite resin[J].J of Appl Oral Sci,2009,17(1):27-31.
[15]Leal JP,Da SJ,Rfm L,et al.Effect of Mouthwashes on Solubility and Sorption of Restorative Composites[J].Int J Dent,2017,2017:1-5.
[16]严敏,冯丹,高平,等.6种光固化复合树脂吸水性、溶解性和单体释放量的比较[J].吉林大学学报(医学版),2018,44(1):45-51.
[17]Alrahlah A,Silikas N,Watts DC.Hygroscopic expansion kinetics of dental resin-composites[J].Dent Mater,2014,30(2):143-148.
[18]Khokhar ZA,Razzoog ME,Yaman P.Color stability of restorative resins[J].Quintessence Int,1991,22(9):733.
[19]Sideridou ID,Karabela MM,Ech V.Dynamic thermomechanical properties and sorption characteristics of two commercial light cured dental resin composites[J].Dent Mater,2008,24(6):737-743.
[20]Sideridou I,Tserki V,Papanastasiou G.Study of water sorption,solubility and modulus of elasticity of light-cured dimethacrylate-based dental resins[J].Biomaterials,2003,24(4):655-665.
[21]Ortengren U,Wellendorf H,Karlsson S,et al.Water sorption and solubility of dental composites and identification of monomers released in an aqueous environment[J].J Oral Rehabil,2001,28(12):1106-1115.
[22]Ortengren U,Andersson F,Elgh U,et al.Influence of pH and storage time on water sorption and solubility of composite materials[J].J Dent,2001,29(1):35-41.
[23]Chaves LP,Júnior O B,Manso A P,et al.Water interaction with dental luting cements by means of sorption and solubility[J].Braz Dent Sci,2013,15(4):29-35.
[24]Mortier E,Gerdolle DA,Jacquot B,et al.Importance of water sorption and solubility studies for couple bonding agent--resin-based filling material[J].Oper Dent,2004,29(6):669.
[25]Ferracane JL.Elution of leachable components from composites[J].J O-ral Rehabil,1994,6(4):282-287.
[26]Tanaka K,Taira M,Shintani H,et al.Residual monomers(TEGDMAand Bis-GMA)of a set visible-light-cured dental composite resin when immersed in water[J].J Oral Rehabil,1991,18(4):353-362.