应用于高压科学研究的国产铰链式六面顶压机技术发展历程
|
摘要
国产铰链式六面顶压机是我国独立发展起来的大腔体高压装置,经过50多年的不断发展,在工业高压合成和高压科学研究领域取得了丰硕成果,在国际上占据一席之地。本文仅以四川大学高压科学与技术实验室在国产铰链式六面顶压机应用于高压科学研究的技术研发为镜,展示国产铰链式六面顶压机大腔体高压装置在应用于高压科学研究领域的发展历程和技术特点,以利于该装置在今后的研发过程中继续保持和发挥其独特性能,为我国工业高压合成和高压科学研究发挥更大的作用。
The China-made hinge-type large volume cubic press is a high-pressure device independently developed in China.After 50 years of continuous development,it has achieved fruitful results in industrial synthesis and high-pressure scientific research and occupied a special place in the world.In this paper,we take the topic of China-made hinge-type large volume cubic press used in high-pressure scientific research at the High Pressure Science and Technology Laboratory of Sichuan University,and demonstrate its development and technical characteristics.The technical performance of the device will be continuously improved in the development process in the future,so that it will play agreater role in Chinas industrial high-pressure synthesis and high-pressure scientific research.
The China-made hinge-type large volume cubic press is a high-pressure device independently developed in China.After 50 years of continuous development,it has achieved fruitful results in industrial synthesis and high-pressure scientific research and occupied a special place in the world.In this paper,we take the topic of China-made hinge-type large volume cubic press used in high-pressure scientific research at the High Pressure Science and Technology Laboratory of Sichuan University,and demonstrate its development and technical characteristics.The technical performance of the device will be continuously improved in the development process in the future,so that it will play agreater role in Chinas industrial high-pressure synthesis and high-pressure scientific research.
引文
[1]LIEBERMANN R C.Multi-anvil,high pressure apparatus:a half-century of development and progress[J].High Pressure Research,2011,31(4):493-532.
[2]KUNIMOTO T,IRIFUNE T.Pressure generation to 125GPa using a 6-8-2type multianvil apparatus with nanopolycrystalline diamond anvils[C]//Journal of Physics:Conference Series.IOP Publishing,2010,215(1):012190.
[3]KUNIMOTO T,IRIFUNE T,SUMIYA H.Pressure generation in a 6-8-2type multi-anvil system:aperformance test for third-stage anvils with various diamonds[J].High Pressure Research,2008,28(3):237-244.
[4]SUMIYA H,IRIFUNE T.Indentation hardness of nano-polycrystalline diamond prepared from graphite by direct conversion[J].Diamond and Related Materials,2004,13(10):1771-1776.
[5]SUMIYA H,HARANO K,IRIFUNE T.Ultrahard diamond indenter prepared from nanopolycrystalline diamond[J].Review of Scientific Instruments,2008,79(5):056102.
[6]SUMIYA H,IRIFUNE T.Hardness and deformation microstructures of nano-polycrystalline diamonds synthesized from various carbons under high pressure and high temperature[J].Journal of Materials Research,2007,22(8):2345-2351.
[7]LE GUILLOU C,BRUNET F,IRIFUNE T,et al.Nanodiamond nucleation below 2 273Kat 15GPa from carbons with different structural organizations[J].Carbon,2007,45(3):636-648.
[8]IRIFUNE T,KURIO A,SAKAMOTO S,et al.Formation of pure polycrystalline diamond by direct conversion of graphite at high pressure and high temperature[J].Physics of the Earth and Planetary Interiors,2004,143:593-600.
[9]DUBROVINSKY L,DUBROVINSKAIA N,BYKOVA E,et al.The most incompressible metal osmium at static pressures above 750gigapascals[J].Nature,2015,525(7568):226-229.
[10]王福龙,贺端威,房雷鸣,等.基于铰链式六面顶压机的二级6-8型大腔体静高压装置[J].物理学报,2008,57(9):5429-5434.WANG F L,HE D W,FANG L M,et al.Design and assembly of split-sphere high pressure apparatus based on the hinge-type cubic-anvil press[J].Acta Physica Sinica,2008,57(9):5429-5434.
[11]方啸虎.中国超硬材料与制品50周年精选论文集[M].杭州:浙江大学出版社,2014:23-31.
[12]王海阔.基于国产六面顶压机增压装置的压力产生极限扩展与应用[D].成都:四川大学,2013.WANG H K.Devlopment and application of pressure generation techniques based on hinge-type cubic press[D].Chengdu:Sichuan University,2013.
[13]WALKER D,CARPENTER M A,HITCH C M.Some simplifications to multianvil devices for high pressure experiments[J].The American Mineralogist,1990,75(9/10):1020-1028.
[14]OHTANI E,OKADA Y,KAGAWA N,et al.Development of a new guide-block system and high pressure and temperature generation[C]//Abstract of the 28th High Pressure Conference of Japan.Kobe,1987:222-223.
[15]XU C,HE D W,WANG H K,et al.Nano-polycrystalline diamond formation under ultra-high pressure[J].International Journal of Refractory Metals and Hard Materials,2013,36:232-237.
[16]王海阔,贺端威,许超,等.复合型多晶金刚石末级压砧的制备并标定六面顶压机6-8型压腔压力至35GPa[J].物理学报,2013,62(18):180703.WANG H K,HE D W,XU C,et al.Calibration of pressure to 35GPa for the cubic press using the diamond-cemented carbide compound anvil[J].Acta Physica Sinica,2013,62(18):180703.
[17]LIU G D,KOU Z L,YAN X Z,et al.Submicron cubic boron nitride as hard as diamond[J].Applied Physics Letters,2015,106(12):121901.
[18]WANG P,HE D W,WANG L P,et al.Diamond-cBN alloy:a universal cutting material[J].Applied Physics Letters,2015,107(10):101901.
[2]KUNIMOTO T,IRIFUNE T.Pressure generation to 125GPa using a 6-8-2type multianvil apparatus with nanopolycrystalline diamond anvils[C]//Journal of Physics:Conference Series.IOP Publishing,2010,215(1):012190.
[3]KUNIMOTO T,IRIFUNE T,SUMIYA H.Pressure generation in a 6-8-2type multi-anvil system:aperformance test for third-stage anvils with various diamonds[J].High Pressure Research,2008,28(3):237-244.
[4]SUMIYA H,IRIFUNE T.Indentation hardness of nano-polycrystalline diamond prepared from graphite by direct conversion[J].Diamond and Related Materials,2004,13(10):1771-1776.
[5]SUMIYA H,HARANO K,IRIFUNE T.Ultrahard diamond indenter prepared from nanopolycrystalline diamond[J].Review of Scientific Instruments,2008,79(5):056102.
[6]SUMIYA H,IRIFUNE T.Hardness and deformation microstructures of nano-polycrystalline diamonds synthesized from various carbons under high pressure and high temperature[J].Journal of Materials Research,2007,22(8):2345-2351.
[7]LE GUILLOU C,BRUNET F,IRIFUNE T,et al.Nanodiamond nucleation below 2 273Kat 15GPa from carbons with different structural organizations[J].Carbon,2007,45(3):636-648.
[8]IRIFUNE T,KURIO A,SAKAMOTO S,et al.Formation of pure polycrystalline diamond by direct conversion of graphite at high pressure and high temperature[J].Physics of the Earth and Planetary Interiors,2004,143:593-600.
[9]DUBROVINSKY L,DUBROVINSKAIA N,BYKOVA E,et al.The most incompressible metal osmium at static pressures above 750gigapascals[J].Nature,2015,525(7568):226-229.
[10]王福龙,贺端威,房雷鸣,等.基于铰链式六面顶压机的二级6-8型大腔体静高压装置[J].物理学报,2008,57(9):5429-5434.WANG F L,HE D W,FANG L M,et al.Design and assembly of split-sphere high pressure apparatus based on the hinge-type cubic-anvil press[J].Acta Physica Sinica,2008,57(9):5429-5434.
[11]方啸虎.中国超硬材料与制品50周年精选论文集[M].杭州:浙江大学出版社,2014:23-31.
[12]王海阔.基于国产六面顶压机增压装置的压力产生极限扩展与应用[D].成都:四川大学,2013.WANG H K.Devlopment and application of pressure generation techniques based on hinge-type cubic press[D].Chengdu:Sichuan University,2013.
[13]WALKER D,CARPENTER M A,HITCH C M.Some simplifications to multianvil devices for high pressure experiments[J].The American Mineralogist,1990,75(9/10):1020-1028.
[14]OHTANI E,OKADA Y,KAGAWA N,et al.Development of a new guide-block system and high pressure and temperature generation[C]//Abstract of the 28th High Pressure Conference of Japan.Kobe,1987:222-223.
[15]XU C,HE D W,WANG H K,et al.Nano-polycrystalline diamond formation under ultra-high pressure[J].International Journal of Refractory Metals and Hard Materials,2013,36:232-237.
[16]王海阔,贺端威,许超,等.复合型多晶金刚石末级压砧的制备并标定六面顶压机6-8型压腔压力至35GPa[J].物理学报,2013,62(18):180703.WANG H K,HE D W,XU C,et al.Calibration of pressure to 35GPa for the cubic press using the diamond-cemented carbide compound anvil[J].Acta Physica Sinica,2013,62(18):180703.
[17]LIU G D,KOU Z L,YAN X Z,et al.Submicron cubic boron nitride as hard as diamond[J].Applied Physics Letters,2015,106(12):121901.
[18]WANG P,HE D W,WANG L P,et al.Diamond-cBN alloy:a universal cutting material[J].Applied Physics Letters,2015,107(10):101901.