消化止泻口服液中主要成分的薄层鉴别研究
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摘要
目的建立消化止泻口服液中主要成分的质量标准。方法采用薄层色谱法对处方中炒陈皮、炒苍术、广木香、薏苡仁、焦山楂进行定性鉴别。结果所采用的薄层鉴别方法斑点清晰,分离效果好,专属性强。结论该方法简便、重现性好、结果可靠,可用于消化止泻口服液的定性质量控制。
Objective To establish the quality control standard of main components in Xiaohuazhixie oral liquid. Methods TLC was used to qualitatively identify the fried pericarpium citri reticulatae,fried rhizoma atractylodis,radix aucklandiae,semen coicis and coke hawthorn in prescription. Results TLC spots were clear and well-separated. The method has strong specificity and without interference.Conclusions The method is simple,reproducible and reliable and can be used for the qualitative quality control of Xiaohuazhixie oral liquid.
Objective To establish the quality control standard of main components in Xiaohuazhixie oral liquid. Methods TLC was used to qualitatively identify the fried pericarpium citri reticulatae,fried rhizoma atractylodis,radix aucklandiae,semen coicis and coke hawthorn in prescription. Results TLC spots were clear and well-separated. The method has strong specificity and without interference.Conclusions The method is simple,reproducible and reliable and can be used for the qualitative quality control of Xiaohuazhixie oral liquid.
引文
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[2]陆文峰.小儿腹泻的发病机制与临床治疗措施研究进展[J].中国医药科学,2013,3(18):47-48.
[3]赵洪波.小儿腹泻病临床新观点与研究进展[J].现代中西医结合杂志,2013,22(23):2620-2622.
[4]崔淑杰,朱新颖,王霞.儿泻停颗粒治疗小儿轮状病毒性肠炎52例临床观察[J].安徽医药,2005,9(5):343.
[5]张相武.消化止泻汤治疗顽固性伤寒沙门氏菌肠炎15例[J].陕西中医,1994,15(7):307.
[6]李若蒙,王悦,常冬梅.参苓白术散联合双歧杆菌治疗脾胃虚弱型小儿腹泻临床观察[J].光明中医,2018,33(12):1785-1787.
[7]牛宛柯.中西医结合治疗小儿腹泻临床观察[J].实用中医药杂志,2017,33(9):1045-1046.
[8]冯娇梅.小儿止泻汤内服治疗小儿腹泻的效果研究[J].饮食保健,2018,5(14):93-94.
[9]庆祖乾,叶养玉.消化止泻口服液的研制及应用[J].江苏药学与临床研究,1998,6(3):27-28.
[10]赵向阳.止泻灵颗粒质量标准研究[J].安徽医药,2007,11(7):614-615.
[11]昝丹娅,马洪涛,许世辉,等.女宝胶囊的薄层鉴别研究[J].安徽医药,2008,12(4):322-323.
[12]国家药典委员会.中华人民共和国药典[M].一部.北京:中国医药科技出版社,2010:353-354.
[13]李德华,卢方晋,倪艳.止痢宁片质量控制方法研究[J].中国中医药信息杂志,2008,15(3):47-48.
[14]李亚萍,庄义修,雷晓林.治带胶囊质控方法研究[J].淮海医药,2007,25(4):363-364.
[15]张明艳.香陈颗粒的薄层色谱鉴别[J].时珍国医国药,2006,17(7):1261-1262.
[16]李彩东,张伟,王信.参芪心舒胶囊中6种药物的薄层鉴别[J].中国现代中药,2013,15(10):891-894.
[17]郑颖,蓝闽波,张宁.健胃消食片中山楂及山药的薄层色谱鉴别[J].时珍国医国药,2006,17(8):1512-1513.