介孔二氧化硅材料合成与表征的综合性化学实验设计
|
摘要
设计了一个综合性化学实验——MCM-41型介孔二氧化硅材料的合成与表征。实验内容包括MCM-41型介孔二氧化硅材料的制备,以及采用扫描电子显微镜、X射线衍射、傅立叶红外光谱、比表面积与孔隙度分析等多种分析方法对其结构和形貌进行表征。本实验不仅可以锻炼学生的基本实验操作技能,还能使学生加深对相关课程理论内容的理解,并进一步激发学生探索化学前沿知识的兴趣。
A comprehensive chemical experiment named synthesis and characterization of MCM-41 mesoporous silica material was designed.Experimental contents contain the preparation of MCM-41 mesoporous silica material,and its full characterization in structure and morphology including scanning electron microscopy,infrared spectroscopy,low angle X-ray diffraction and nitrogen adsorption-desorption measurement.This experiment can not only improve undergraduates' basic experimental skills,but also make them to comprehend the fundamentals of related chemical courses.Furthermore,the experiment may also arouse undergraduates' interests to explore the advances in chemistry.
A comprehensive chemical experiment named synthesis and characterization of MCM-41 mesoporous silica material was designed.Experimental contents contain the preparation of MCM-41 mesoporous silica material,and its full characterization in structure and morphology including scanning electron microscopy,infrared spectroscopy,low angle X-ray diffraction and nitrogen adsorption-desorption measurement.This experiment can not only improve undergraduates' basic experimental skills,but also make them to comprehend the fundamentals of related chemical courses.Furthermore,the experiment may also arouse undergraduates' interests to explore the advances in chemistry.
引文
[1] Kresge C T,Leonowicz M E,Roth W J,et al.Nature,1992,359:710-712
[2] Wu S-H,Mou C-Y,Lin H-P.Chemical Society Reviews,2013,42:3862-3875
[3]王科志,申秀民,刘正平,等.化学教育,2010,31(3):92-93,104
[4]曹小华,谢宝华,叶姗,等.化学教育,2011,32(5):60-63
[5]曹小华,喻国贞,雷艳红,等.化学教育,2009,30(11):15-16,76
[6]余凡,李艾华,张玉敏,等.大学化学,2016,31(12):64-68
[7]王向东,阴倩倩,向靖宇,等.大学化学,2016,31(8):66-70
[8]邵谦,王小杰,王凌云,等.高校实验室工作研究,2012(4):41-43,67
[9]边绍伟,赵亚萍,咸春颖,等.大学化学,2015,30(3):47-50
[10]李泽胜,李泊林,刘志森,等.广东化工,2016,43(13):27-28
[11]曹丽琴.广东化工,2012,39(5):264-265
[12] Thommes M,Kaneko K,Neimark A V,et al.Pure and Applied Chemistry,2015,87(9/10):1051-1069
[13] Beck J S,Vartuli J C,Roth W J,et al.Journal of the American Chemical Society,1992,114(27):10834-10843
[14] Cai Q,Cui F Z,Chen X H,et al.Chemistry Letters,2000,29(9):1044-1045
[15]赵东元,万颖,周午纵.有序介孔分子筛材料.北京:高等教育出版社,2013:133-134
[2] Wu S-H,Mou C-Y,Lin H-P.Chemical Society Reviews,2013,42:3862-3875
[3]王科志,申秀民,刘正平,等.化学教育,2010,31(3):92-93,104
[4]曹小华,谢宝华,叶姗,等.化学教育,2011,32(5):60-63
[5]曹小华,喻国贞,雷艳红,等.化学教育,2009,30(11):15-16,76
[6]余凡,李艾华,张玉敏,等.大学化学,2016,31(12):64-68
[7]王向东,阴倩倩,向靖宇,等.大学化学,2016,31(8):66-70
[8]邵谦,王小杰,王凌云,等.高校实验室工作研究,2012(4):41-43,67
[9]边绍伟,赵亚萍,咸春颖,等.大学化学,2015,30(3):47-50
[10]李泽胜,李泊林,刘志森,等.广东化工,2016,43(13):27-28
[11]曹丽琴.广东化工,2012,39(5):264-265
[12] Thommes M,Kaneko K,Neimark A V,et al.Pure and Applied Chemistry,2015,87(9/10):1051-1069
[13] Beck J S,Vartuli J C,Roth W J,et al.Journal of the American Chemical Society,1992,114(27):10834-10843
[14] Cai Q,Cui F Z,Chen X H,et al.Chemistry Letters,2000,29(9):1044-1045
[15]赵东元,万颖,周午纵.有序介孔分子筛材料.北京:高等教育出版社,2013:133-134