柠檬酸浸取脱除鳙鱼鱼鳞钙的研究
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摘要
以鱼鳞残钙质量分数为试验指标,在磁力搅拌下进行柠檬酸水溶液浸脱鳙鱼鱼鳞钙的研究。考察液固比、反应时间、搅拌速度和柠檬酸浓度对鱼鳞残钙质量分数的影响,确定它们的最适宜值分别为20∶1(V∶m)、60min、900r/min和12.5%,该条件下,鱼鳞中总钙质量分数由10.5%降至0.772%。正交试验结果表明上述4个考察因素对残钙质量分数的影响精度均为不显著,但对残钙质量分数影响程度相对大小的顺序为反应时间、液固比、搅拌速度和柠檬酸浓度。
With residual calcium mass fraction as objective function,the decalcification of bighead fish scales was carried out in citric acid aqueous solution by magnetic stirring.The effects of liquid-solid ratio,reaction time,stirring speed and citric acid concentration on the residual calcium mass fraction of fish scales were investigated and their maximum values were separately to be 20∶1(V∶m),60 min,900r/min and 12.5%,under which the total calcium ion mass fraction of the fish scales were dropped from 10.5%to 0.772%.The variance analysis of orthogonal test indicated that the impact accuracies of the four parameters on the residual calcium mass fraction were not significant,but the order of their relative sizes of the impacts on the residual calcium mass fraction were reaction time,liquid-solid ratio,stirring speed and citric acid concentration.
With residual calcium mass fraction as objective function,the decalcification of bighead fish scales was carried out in citric acid aqueous solution by magnetic stirring.The effects of liquid-solid ratio,reaction time,stirring speed and citric acid concentration on the residual calcium mass fraction of fish scales were investigated and their maximum values were separately to be 20∶1(V∶m),60 min,900r/min and 12.5%,under which the total calcium ion mass fraction of the fish scales were dropped from 10.5%to 0.772%.The variance analysis of orthogonal test indicated that the impact accuracies of the four parameters on the residual calcium mass fraction were not significant,but the order of their relative sizes of the impacts on the residual calcium mass fraction were reaction time,liquid-solid ratio,stirring speed and citric acid concentration.
引文
1 张丰香.酶法制备草鱼鱼鳞明胶及ACE抑制肽的研究[D].无锡:江南大学,2009.
2 吴波,陈运中,律佳雪,等.响应面分析法优化鱼鳞脱钙条件的研究[J].食品科学,2008,29(4):181~184.
3 周光朝,刘良忠,万菡,等.鱼鳞酶解前处理工艺优化研究[J].武汉工业学院学报,2010,29(3):7~10.
4 张俊杰,段蕊,薛婉丽,等.鲤鱼鱼鳞在盐酸脱钙过程中的变化[J].氨基酸和生物资源,2009,31(1):44~47.
5 陈日春.鲢鱼鱼鳞的脱钙工艺[J].农产品加工,2013(2):42~44.
6 涂宗财,沙小梅,王辉,等.鳙鱼鱼鳞酸法脱钙[J].食品与发酵工业,2012,38(2):106~110.
7 段蕊,张俊杰,杜修桥.鱼鳞组成性质及其加工利用的研究进展[J].食品与机械,2006,22(5):128~131.
8 袁燕,李燕萍,曹智启,等.蒜头果中黄酮类化合物的提取及含量测定[J].安徽农业科学,2011,39(21):12 847~12 848.
9 李俶,沈佩仪,吴华星,等.超声波提取菠萝皮渣中多酚类物质的研究[J].食品与机械,2011,27(2):55~58.
10 马秀婷,肖志刚,孙旭,等.超声波辅助提取豆渣蛋白工艺优化[J].食品与机械,2013,29(1):108~112.
11 张丰香,许时婴,王樟.鱼鳞明胶生产的浸酸脱钙工艺研究[J].食品工业科技,2008,29(3):199~204.
12 王迪,罗永康,崔建云.响应面法优化武昌鱼鳞脱钙工艺的研究[J].淡水鱼业,2010,40(3):61~66.
13 蒋柏泉,李春,白立晓,等.石英光纤表面化学镀Ni-P的工艺研究及其表征[J].南昌大学学报(工科版),2008,30(3):205~208.
14 陈建信.工艺与配方的最优化方法[M].杭州:浙江科学技术出版社,1986.
15 曾江南,蒋柏泉,魏林生,等.鳙鱼鱼鳞脱钙的工艺优化[J].南昌大学学报(工科版),2011,33(4):338~342,364.
2 吴波,陈运中,律佳雪,等.响应面分析法优化鱼鳞脱钙条件的研究[J].食品科学,2008,29(4):181~184.
3 周光朝,刘良忠,万菡,等.鱼鳞酶解前处理工艺优化研究[J].武汉工业学院学报,2010,29(3):7~10.
4 张俊杰,段蕊,薛婉丽,等.鲤鱼鱼鳞在盐酸脱钙过程中的变化[J].氨基酸和生物资源,2009,31(1):44~47.
5 陈日春.鲢鱼鱼鳞的脱钙工艺[J].农产品加工,2013(2):42~44.
6 涂宗财,沙小梅,王辉,等.鳙鱼鱼鳞酸法脱钙[J].食品与发酵工业,2012,38(2):106~110.
7 段蕊,张俊杰,杜修桥.鱼鳞组成性质及其加工利用的研究进展[J].食品与机械,2006,22(5):128~131.
8 袁燕,李燕萍,曹智启,等.蒜头果中黄酮类化合物的提取及含量测定[J].安徽农业科学,2011,39(21):12 847~12 848.
9 李俶,沈佩仪,吴华星,等.超声波提取菠萝皮渣中多酚类物质的研究[J].食品与机械,2011,27(2):55~58.
10 马秀婷,肖志刚,孙旭,等.超声波辅助提取豆渣蛋白工艺优化[J].食品与机械,2013,29(1):108~112.
11 张丰香,许时婴,王樟.鱼鳞明胶生产的浸酸脱钙工艺研究[J].食品工业科技,2008,29(3):199~204.
12 王迪,罗永康,崔建云.响应面法优化武昌鱼鳞脱钙工艺的研究[J].淡水鱼业,2010,40(3):61~66.
13 蒋柏泉,李春,白立晓,等.石英光纤表面化学镀Ni-P的工艺研究及其表征[J].南昌大学学报(工科版),2008,30(3):205~208.
14 陈建信.工艺与配方的最优化方法[M].杭州:浙江科学技术出版社,1986.
15 曾江南,蒋柏泉,魏林生,等.鳙鱼鱼鳞脱钙的工艺优化[J].南昌大学学报(工科版),2011,33(4):338~342,364.