耐晒黄G的合成与结构表征
摘要
本文通过重氮化反应和偶合反应合成了耐晒黄G,C_(17)H_(16)N_4O_4(Mr=340.34),利用单晶衍射和红外光谱对其进行了结构表征,并对其单晶和红外光谱进行了分析。
引文
[1]穆振义.高档有机颜料专用中间体的合成及其应用[J].上海染料,2001,29(5):29-39.
[2]Frank J Maile,Gerhard Pfaff,Peter Reynders.Effect pigments past,present and future[J].Progress in Organic Coatings,2005,54(3):150-163.
[3]鹏博.近年有机颜料发展中的特点和问题[J].湘潭化工,1991,20(1):1-9.
[4]周春隆.有机颜料工业技术若干领域的进展[J].染料工业,1999(1):20-31.
[5]赵凤云,尹亚森.合成C.I.颜料黄12的最佳配方及工艺条件[J].抚顺石油学院学报,1998,18(2):4-5.
[6]虞幸芝,范宪,陈矩钧,等.一种用工业原料制取高品味有机颜料的方法:CN,94114049[P].1995-08-16.
[7]Wang Shirong,Zhou Chunlong.The effects of mixed coupling on the properties of C.I.Pigment Yellow 12[J].Dyes and Pigmenis,1998,38(4):185-193.
[8]Mather R R.The degree of crystal aggregation in orgnaie pigments[J].Dyes and Pigments,1999,42(1):103-106.
[9]Sheldrake G M[CP].Acta Crystal ogre Sec t A,1990,46:467.
[10]Sheldrake G M.SHELXS97:Program for the refinement of crystal structures[M].Germany:University of Grttingen,1997:44-45.
[2]Frank J Maile,Gerhard Pfaff,Peter Reynders.Effect pigments past,present and future[J].Progress in Organic Coatings,2005,54(3):150-163.
[3]鹏博.近年有机颜料发展中的特点和问题[J].湘潭化工,1991,20(1):1-9.
[4]周春隆.有机颜料工业技术若干领域的进展[J].染料工业,1999(1):20-31.
[5]赵凤云,尹亚森.合成C.I.颜料黄12的最佳配方及工艺条件[J].抚顺石油学院学报,1998,18(2):4-5.
[6]虞幸芝,范宪,陈矩钧,等.一种用工业原料制取高品味有机颜料的方法:CN,94114049[P].1995-08-16.
[7]Wang Shirong,Zhou Chunlong.The effects of mixed coupling on the properties of C.I.Pigment Yellow 12[J].Dyes and Pigmenis,1998,38(4):185-193.
[8]Mather R R.The degree of crystal aggregation in orgnaie pigments[J].Dyes and Pigments,1999,42(1):103-106.
[9]Sheldrake G M[CP].Acta Crystal ogre Sec t A,1990,46:467.
[10]Sheldrake G M.SHELXS97:Program for the refinement of crystal structures[M].Germany:University of Grttingen,1997:44-45.