拉曼光谱仪反应池的研发
摘要
自主研发的共聚焦拉曼光谱仪反应池,其主要结构有真空腔、石英窗片、加热器、低温盘、冷却水路、液氮管路、电流和热电偶馈通等。共聚焦拉曼光谱仪反应池可以承载固体或液体样品,实现真空或特殊气氛下的原位分析,实现-130℃～500℃温度的精确控温,实现原位施加电压。通过测试铝离子电池在充电过程中阴极石墨的拉曼光谱图,验证了反应池的性能。
引文
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[3]何蔚,孙贤君.拉曼光谱应用技术研究[J].标准科学,2018(3):70-75.
[4]李淑玲.拉曼光谱仪及其应用进展[J].岩矿测试,1998,17(4):312-316.
[5]于永爱,吴维.拉曼光谱技术与便携式拉曼光谱仪[J].技术交流,2009:85-87.
[6]游燕.国产高能量电子枪的研发[D].大连:大连交通大学,2016.
[7]郭方准.实用真空技术[M].大连:大连理工大学出版社,2012.
[8]Meng-Chang Lin,Ming Gong.An ultrafast rechargeable aluminium-ion battery[J].Nature,2015.
[9]Chao Wang,Chuanhai Xiao,Qiang Fu,In-Operando XPS and Raman Studies of graphite electrode in Aluminum Battery[J].Nano And Interface Catalysis Group.
[10]Julio C.Chac’on-Torres.Raman spectroscopy of graphite intercalation compounds:Charge transfer,strain,and electron-phonon coupling in graphene layers[J].Phys.Status Solidi,2014(12):2337-2355.
[11]Anthony S.Childress,PrakashParajuli.ARaman spectroscopic study of graphene cathodes in high-performancealuminum ion batteries[J].Nano Energy,2017(39):69-76.
[12]Julio C,Chaco’n-Torres.Manifestation of Charged and Strained Graphene Layers in the Raman Response of Graphite Intercalation Compounds[J].ACSAuthorChoice,2013,7(10):9249-9259.