环境中PCBs和PBBs的测定研究进展
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摘要
介绍了环境样品中PCBs和PBBs测定的前处理技术,综述了目前该两种持久性有机污染物的监测方法和研究现状。对PCBs和PBBs污染物研究领域发展方向进行了展望,认为今后的工作重点是实现新型前处理方法与大型精密仪器联用技术及开展这两种污染物的同时测定。
The pretreatment techniques of polychlorinated biphenyls and polybrominated biphenyls in environmental samples were introduced. The current monitoring methods and research status of the two persistent organic pollutants(POPs) were reviewed. The development direction of polychlorinated biphenyls and polybrominated biphenyls were also discussed. It is believed that the future work will focus on the combination of new pretreatment methods with large-scale precision instruments and the simultaneous determination of these two pollutants.
The pretreatment techniques of polychlorinated biphenyls and polybrominated biphenyls in environmental samples were introduced. The current monitoring methods and research status of the two persistent organic pollutants(POPs) were reviewed. The development direction of polychlorinated biphenyls and polybrominated biphenyls were also discussed. It is believed that the future work will focus on the combination of new pretreatment methods with large-scale precision instruments and the simultaneous determination of these two pollutants.
引文
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[2]Kramer S,Hikel S M,Adams K,et al.Current status of the epidemiologic evidence linking polychlorinated biphenyls and non-hodgkin lymphoma,and the role of immune dysregulation[J].Environmental Health Perspectives,2012,120(8):1067-1075.
[3]Chen H Y,Zhuang H S,Yang G X.Biological monitoring method of PCBs in environment samples[J].Environmental Chemistry,2011,30(5):954-957.
[4]毛琼晶,陆胜勇,卫樱蕾,等.水平球磨机械化学法处置多氯联苯污染土壤的试验[J].环境化学,2016,35(4):607-614.
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[6]Zheng X,Liu X,Jiang G,et al.Distribution of PCBs and PBDEs in soils along the altitudinal gradients of Balang mountain,the east edge of the Tibetan Plateau[J].Environmental Pollution,2012,161:101-106.
[7]Bayer A,Biziuk M.Applications of sample preparation techniques in the analysis of pesticides and PCBs in food[J].Food Chemistry,2008,108(2):669-680.
[8]王静婷,谷成刚,叶茂,等.土壤中多氯联苯的生物有效性及其影响机制研究[J].土壤,2015,47(1):80-86.
[9]董黎静,戴玄吏,滕加泉,等.SBSE-TDU-GC/MS法同步测定饮用水源水中16种多溴联苯化合物[J].环境监测与预警,2015,7(5):37-41.
[10]刘国瑞,李丽,孙素芳,等.多溴联苯的污染来源、分析方法和环境污染特征[J].化学进展,2014,26(8):1434-1444.
[11]马玉,邹西梅,林竹光.厦门近海沉积物中PBDEs与PBBs残留的GC-NCI/MS和GC-ECD分析[J].分析试验室,2009,28(7):103-107.
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[13]李申杰,杨炳建,陈荣枫,等.固相萃取-高分辨气相色谱/质谱联用法同时检测大气中39种持久性有机污染物[J].分析试验室,2016,35(6):717-721.
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[15]徐恒振,王晓芳,周传光,等.微波萃取海洋沉积物中有机氯农药和多氯联苯[J].海洋环境科学,2010,29(3):420-423.
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[21]高丹,刘劲松,朱国华,等.同位素稀释/高分辨气相色谱-质谱联用同时测定空气中二噁英、多氯联苯、多溴联苯醚和溴代二噁英[J].分析化学,2013,41(12):1862-1868.
[22]胡礼渊,邓集煜,廖和菁,等.分散固相萃取-气相色谱法测定水产品中多氯联苯[J].食品科学,2016,37(14):207-212.
[23]涂逢樟,林竹光,姚辉梅,等.气相色谱-负离子化学源-质谱法分析禽蛋食品中10种多溴联苯和多溴联苯醚残留[J].分析试验室,2010,29(8):18-23.
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[25]赖莺,王鸿辉,蔡鹭欣,等.高效液相色谱法测定电子电气产品中多溴联苯和多溴联苯醚[J].理化检验:化学分册,2012,48(12):1446-1449.
[26]邵阳,杨国胜,韩深,等.加速溶剂萃取-硅胶萃取净化-气相色谱/质谱法检测地表水中有机氯农药和多氯联苯[J].分析化学研究报告,2016,44(5):698-706.
[27]王俊平,姜小梅,王硕,等.气相色谱-电子轰击源质谱测定海产品中多溴联苯(醚)[J].食品工业科技,2011(3):390-393.
[28]张潜,余辉菊,高舸,等.饮用水中16种多环芳烃和6种多氯联苯的固相微萃取/气相色谱/三重四极杆质谱同时测定法[J].环境与健康杂志,2014,31(2):173-176.
[29]蔡小虎,蔡述伟,时磊,等.Qu ECh ERS-GC/ECD法分析土壤和沉积物中残留有机氯农药和多氯联苯[J].环境监控与预警,2016,8(3):14-17.
[30]艾连峰,李玮,王敬,等.气相色谱-串联质谱法测定牛奶中多氯联苯及多环芳烃[J].分析测试学报,2015,34(5):570-575.
[31]叶曦雯,牛增元,张清智,等.气相色谱-质谱法测定压敏胶及其制品中的多溴联苯与多溴二苯醚[J].分析测试学报,2013,32(10):1251-1255.
[32]吴益春,祝世军,罗海军,等.酸消化-气相色谱法测定鱼肉中指示性多氯联苯研究[J].食品安全质量检测学报,2015,6(3):923-928.
[33]姚婷,张蓬,赫春香,等.大连湾和杭州湾表层沉积物中多氯联苯和有机氯农药及风险评价[J].海洋科学,2014,38(7):47-56.
[34]莫凌,吴江平,张云,等.电子垃圾拆解地翠鸟对多氯联苯的累积及风险评估[J].生态毒理学报,2016,11(2):155-162.
[35]刘潇,李敬光,黄飞飞,等.气相色谱-质谱法测定人血清中多溴联苯[J].色谱,2012,30(5):468-473.
[36]何雪芬,熊珺,王妙春,等.超声萃取-气相色谱质谱法测定环境和食品中多溴联苯及多溴联苯醚[J].现代测量与实验室管理,2014(2):3-6.
[37]杨佳佳,吴淑琪,佟玲,等.离子阱串联质谱法测定土壤及沉积物中的有机氯农药与多氯联苯[J].分析测试学报,2011,30(4):374-380.
[38]张瑞,张志辉,刘卓钦,等.高效液相色谱法测定皮革中20种溴代阻燃剂[J].分析试验室,2014,33(1):73-77.
[39]曾立平.超高效液相色谱法测定纺织品中多溴联苯(醚)类阻燃剂[J].毛纺科技,2016,44(7):37-42.
[40]韩善龙,王宝盛,阮挺,等.不同水源灌溉的农田表层土壤中多氯联苯和多溴联苯醚的浓度分布特征[J].环境化学,2012,31(7):958-965.
[41]闻胜,龚艳,史廷明,等.二噁英、多溴联苯醚和多氯联苯同时测定方法的研究[J].分析科学学报,2009,25(6):629-633.
[42]王道玮,赵世民,金伟,等.加速溶剂萃取-固相萃取净化-气相色谱/质谱法测定沉积物中多氯联苯和多环芳烃[J].分析化学,2013,41(6):861-868.
[43]赵起越,赵红帅,刘保献,等.大气颗粒物中多环芳烃及多氯联苯的同步检测分析技术[J].分析试验室,2016,35(4):487-491.
[44]董黎静,戴玄吏,滕加泉,等.DPX快速萃取程序升温大体积进样GC/MS法测定水中19种多溴联苯化合物[J].环境监控与预警,2016,8(4):17-19.
[45]余彬彬,方铖,饶钦全,等.气相色谱质谱法分析土壤中多溴联苯和多溴联苯醚类化合物[J].分析化学研究报告,2011,39(6):833-838.
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[2]Kramer S,Hikel S M,Adams K,et al.Current status of the epidemiologic evidence linking polychlorinated biphenyls and non-hodgkin lymphoma,and the role of immune dysregulation[J].Environmental Health Perspectives,2012,120(8):1067-1075.
[3]Chen H Y,Zhuang H S,Yang G X.Biological monitoring method of PCBs in environment samples[J].Environmental Chemistry,2011,30(5):954-957.
[4]毛琼晶,陆胜勇,卫樱蕾,等.水平球磨机械化学法处置多氯联苯污染土壤的试验[J].环境化学,2016,35(4):607-614.
[5]Liu W,Chen D,Liu X,et al.Transport of semivolatile organic compounds to the tibetan plateau:Spatial and temporal variation in air concentration in mountainous western Sichuan,China[J].Environmental Science&Technology,2010,44(5):1559-1565.
[6]Zheng X,Liu X,Jiang G,et al.Distribution of PCBs and PBDEs in soils along the altitudinal gradients of Balang mountain,the east edge of the Tibetan Plateau[J].Environmental Pollution,2012,161:101-106.
[7]Bayer A,Biziuk M.Applications of sample preparation techniques in the analysis of pesticides and PCBs in food[J].Food Chemistry,2008,108(2):669-680.
[8]王静婷,谷成刚,叶茂,等.土壤中多氯联苯的生物有效性及其影响机制研究[J].土壤,2015,47(1):80-86.
[9]董黎静,戴玄吏,滕加泉,等.SBSE-TDU-GC/MS法同步测定饮用水源水中16种多溴联苯化合物[J].环境监测与预警,2015,7(5):37-41.
[10]刘国瑞,李丽,孙素芳,等.多溴联苯的污染来源、分析方法和环境污染特征[J].化学进展,2014,26(8):1434-1444.
[11]马玉,邹西梅,林竹光.厦门近海沉积物中PBDEs与PBBs残留的GC-NCI/MS和GC-ECD分析[J].分析试验室,2009,28(7):103-107.
[12]Gao F,Luo X J,Yang Z F,et al.Brominated flame retardants,polychlorinated biphenyls,and organochlorine pesticidesin bird eggs from the Yellow River Delta,North China[J].Environmental Science&Technology,2009,43(18):6956-6962.
[13]李申杰,杨炳建,陈荣枫,等.固相萃取-高分辨气相色谱/质谱联用法同时检测大气中39种持久性有机污染物[J].分析试验室,2016,35(6):717-721.
[14]Vetter W,Vonder Recke R,Herzke D,et al.Detailed analysis of polybrominated biphenyl congeners in bird eggs from Norway[J].Environmental Pollution,2008,156(3):1204-1210.
[15]徐恒振,王晓芳,周传光,等.微波萃取海洋沉积物中有机氯农药和多氯联苯[J].海洋环境科学,2010,29(3):420-423.
[16]范成英,谢卢明.微波萃取和气相色谱-质谱测定塑料中的多溴联苯[J].化工生产技术,2008,15(5):46-49.
[17]崔立迁,王欣,催进,等.气相色谱-质谱联用测定艾叶中持久性有机污染物[J].分析科学学报,2016,32(1):111-115.
[18]洪佳.超声波萃取/气相色谱质联用仪分析电动牙刷中的多溴联苯及多溴联苯醚[J].广东化工,2016,43(6):157-158.
[19]董黎静,戴玄吏,滕加泉,等.SBSE-TDU-GC/MS法同步测定饮用水源水中16种多溴联苯化合物[J].环境监控与预警,2015,7(5):37-41.
[20]夏欢,谢美,杨泽玉,等.多溴联苯在聚二甲基硅氧烷与水相间分配系数的固相微萃取技术测定[J].分析测试学报,2008,27(2):148-152.
[21]高丹,刘劲松,朱国华,等.同位素稀释/高分辨气相色谱-质谱联用同时测定空气中二噁英、多氯联苯、多溴联苯醚和溴代二噁英[J].分析化学,2013,41(12):1862-1868.
[22]胡礼渊,邓集煜,廖和菁,等.分散固相萃取-气相色谱法测定水产品中多氯联苯[J].食品科学,2016,37(14):207-212.
[23]涂逢樟,林竹光,姚辉梅,等.气相色谱-负离子化学源-质谱法分析禽蛋食品中10种多溴联苯和多溴联苯醚残留[J].分析试验室,2010,29(8):18-23.
[24]徐恒振,王晓芳,周传光,等.微波萃取海洋沉积物中有机氯农药和多氯联苯[J].海洋环境科学,2010,29(3):420-423.
[25]赖莺,王鸿辉,蔡鹭欣,等.高效液相色谱法测定电子电气产品中多溴联苯和多溴联苯醚[J].理化检验:化学分册,2012,48(12):1446-1449.
[26]邵阳,杨国胜,韩深,等.加速溶剂萃取-硅胶萃取净化-气相色谱/质谱法检测地表水中有机氯农药和多氯联苯[J].分析化学研究报告,2016,44(5):698-706.
[27]王俊平,姜小梅,王硕,等.气相色谱-电子轰击源质谱测定海产品中多溴联苯(醚)[J].食品工业科技,2011(3):390-393.
[28]张潜,余辉菊,高舸,等.饮用水中16种多环芳烃和6种多氯联苯的固相微萃取/气相色谱/三重四极杆质谱同时测定法[J].环境与健康杂志,2014,31(2):173-176.
[29]蔡小虎,蔡述伟,时磊,等.Qu ECh ERS-GC/ECD法分析土壤和沉积物中残留有机氯农药和多氯联苯[J].环境监控与预警,2016,8(3):14-17.
[30]艾连峰,李玮,王敬,等.气相色谱-串联质谱法测定牛奶中多氯联苯及多环芳烃[J].分析测试学报,2015,34(5):570-575.
[31]叶曦雯,牛增元,张清智,等.气相色谱-质谱法测定压敏胶及其制品中的多溴联苯与多溴二苯醚[J].分析测试学报,2013,32(10):1251-1255.
[32]吴益春,祝世军,罗海军,等.酸消化-气相色谱法测定鱼肉中指示性多氯联苯研究[J].食品安全质量检测学报,2015,6(3):923-928.
[33]姚婷,张蓬,赫春香,等.大连湾和杭州湾表层沉积物中多氯联苯和有机氯农药及风险评价[J].海洋科学,2014,38(7):47-56.
[34]莫凌,吴江平,张云,等.电子垃圾拆解地翠鸟对多氯联苯的累积及风险评估[J].生态毒理学报,2016,11(2):155-162.
[35]刘潇,李敬光,黄飞飞,等.气相色谱-质谱法测定人血清中多溴联苯[J].色谱,2012,30(5):468-473.
[36]何雪芬,熊珺,王妙春,等.超声萃取-气相色谱质谱法测定环境和食品中多溴联苯及多溴联苯醚[J].现代测量与实验室管理,2014(2):3-6.
[37]杨佳佳,吴淑琪,佟玲,等.离子阱串联质谱法测定土壤及沉积物中的有机氯农药与多氯联苯[J].分析测试学报,2011,30(4):374-380.
[38]张瑞,张志辉,刘卓钦,等.高效液相色谱法测定皮革中20种溴代阻燃剂[J].分析试验室,2014,33(1):73-77.
[39]曾立平.超高效液相色谱法测定纺织品中多溴联苯(醚)类阻燃剂[J].毛纺科技,2016,44(7):37-42.
[40]韩善龙,王宝盛,阮挺,等.不同水源灌溉的农田表层土壤中多氯联苯和多溴联苯醚的浓度分布特征[J].环境化学,2012,31(7):958-965.
[41]闻胜,龚艳,史廷明,等.二噁英、多溴联苯醚和多氯联苯同时测定方法的研究[J].分析科学学报,2009,25(6):629-633.
[42]王道玮,赵世民,金伟,等.加速溶剂萃取-固相萃取净化-气相色谱/质谱法测定沉积物中多氯联苯和多环芳烃[J].分析化学,2013,41(6):861-868.
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