α-AlH_3的制备技术进展
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摘要
AlH3是一种性能优异的功能材料,广泛应用于复合固体推进剂,燃料电池,高分子合成等诸多领域,目前已知的7种晶型中α-AlH3最稳定,介绍了α-AlH3相关理化性质以及表征手段,综述了α-AlH3的制备技术,并简要阐述了各种制备方法的利弊,最后提出Brower法具有规模化生产的潜力,以及目前Brower法所要解决的问题。
AlH3,as an excellent functional material,has been found on a large-scale application in composite of solid propellant,fuel cells,organic and polymer chemistry,andα-AlH3is the most stable in all known 7crystal phases.The physical and chemistry properties ofα-AlH3was introduced.The progress ofα-AlH3in synthesis method and the advantages and disadvantages were introduced.Finally Brower method had the potential in scale production and the problem needed to improve were pointed out.
AlH3,as an excellent functional material,has been found on a large-scale application in composite of solid propellant,fuel cells,organic and polymer chemistry,andα-AlH3is the most stable in all known 7crystal phases.The physical and chemistry properties ofα-AlH3was introduced.The progress ofα-AlH3in synthesis method and the advantages and disadvantages were introduced.Finally Brower method had the potential in scale production and the problem needed to improve were pointed out.
引文
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[27]罗永春,毛松科,阎汝煦.机械球磨固相化学反应制备AlH3及其放氢性能[J].物理化学学报,2009,25(2):237-241.
[28]Sartori S,Istad-Lem A,Brinks H W,et al.[J].Internation Journal of Hydrogen Enegry,2009,34(15):6350-6356.
[29]Sartori S,Opalka S M,et al.[J].Journal of Material Chemistry,2008,18:2361-2370.
[30]Brinks H W,Istad-Lem A,Hauback B C.[J].Journal of Physical Chemistry B,2006,110(51):25833-25837.
[31]Normatov I Sh.[J].Kinetics and catalysis,2004,45(4):558-560.
[2]Finholt A E,Bond Jr A C,Schlesinger H I.[J].Journal of the American Chemical Society,1947,69(5):1199-1203.
[3]Brower FM,Matzek N E,Reigler P F,et al.[J].Journal of the American Chemical Society,1976,98(9):2450-2453.
[4]Graetz J,Reilly J J,Kulleck J G,et al.[J].Journal of Alloys and Compounds,2007,446-447:271-275.
[5]Sandrock G.[J].Journal of Alloys and Compounds,2006,421:185-189.
[6]Cheng Hsiuyi,Hou Duenren.[J].Tetrahedron,2007,63:3000-3005.
[7]Aniko Borbas,Szabo Z B,Szilagyi Lz,et al.[J].Tetrahedron,2002,58:5723-5732.
[8]Bootle-Wibraham A,Steve Head,Longstaff J,et al.[J].Tetrahedron Letters,1999,40(28):5267-5270.
[9]Griffin S,Heath L,Wyatt P.[J].Tetrahedron Letters,1998,39(24):4405-4406.
[10]Dozzi G,et al.Oligomeric iminic derivatives of aluminumhydride and method for their preparation:US 4239692[P],1980-12-16.
[11]Deluca LT,Rossettini L,Kappenstein C,et al.[J].Aerospace Science and Technology,2007,11(2):18-25.
[12]Atwood J L,Bennett FR,Elms F M,et al.[J].Journal of the American Chemical Society,1991,113(21):8183-8185.
[13]Tkacz M,Palasyuk T,Graetz J.[J].Journal of Raman Spectroscy,2008,39(7):922-927.
[14]刘明星,陶永杰,何金选,等.[J].含能材料,2006,14(5):400-403.
[15]Lund G K,Michael W L,Jami I I.37th international annual conference of ICT energetic materials[C].Germany,2006,1-11.
[16]Terada K.Prearation of aluminum hydride:US 3869545[P],1975-5-4.
[17]Reigler P F,Lamoria Lz F.Process for making hexagonal macrocrystal of aluminum hydride:US 3838194[P],1974-9-24.
[18]Knott.Method for the preparation of aluminum hydride by reacting magnesium hydride with aluminum halide:US 5565183[P],1996-10-15.
[19]Klapdor A,Knott W,Windbiel D.Method for synthesizing aluminum hydride:US 5670129[P],1997-09-23.
[20]Bulychev B M,Verbetskii V N,et al.[J].Russian journal of inorganic chemistry,2008,23(7):1000-1005.
[21]Skelcey J S.Preparation of beryllium hydride and aluminum hydride:US 3791846[P],1976-7-27.
[22]Ashby E C,Sanders J R,Claudy P,et al.[J].Inorganic Chemistry,1973,12(12):2860-2868.
[23]Murib J H.Preparation of aluminum hydride:US 3764666[P],1973-10-9.
[24]何丽.三氢化铝的合成[D].北京:北京有色金属研究总院,2011.
[25]Paskevicvius M,Sheppard D A,Buckley C E.[J].Journal of Alloys and Compounds,2009,487(1):370-376.
[26]Konovalov S K,Bulychev BM.[J].Inorganic chemistry,1995,34(1):172-175.
[27]罗永春,毛松科,阎汝煦.机械球磨固相化学反应制备AlH3及其放氢性能[J].物理化学学报,2009,25(2):237-241.
[28]Sartori S,Istad-Lem A,Brinks H W,et al.[J].Internation Journal of Hydrogen Enegry,2009,34(15):6350-6356.
[29]Sartori S,Opalka S M,et al.[J].Journal of Material Chemistry,2008,18:2361-2370.
[30]Brinks H W,Istad-Lem A,Hauback B C.[J].Journal of Physical Chemistry B,2006,110(51):25833-25837.
[31]Normatov I Sh.[J].Kinetics and catalysis,2004,45(4):558-560.