氮化硼陶瓷纤维的制备与应用
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摘要
氮化硼陶瓷纤维是一种正在发展的新型高性能材料,然而传统的高温法很难制备高质量的氮化硼陶瓷纤维材料,只能通过前驱体转化法实现。概述了氮化硼陶瓷纤维的合成路线以及各种前驱体制备氮化硼陶瓷纤维的优缺点,并对前驱体法制备氮化硼陶瓷纤维的发展趋势做了展望。
Boron nitride ceramic fiber is a new developing high-performance material. But the traditional method of high-temperature synthesis is hard to prepare high-quality boron nitride ceramic fiber which can only be prepared by the method of polymer derived ceramics(PDCs). In the article, synthesis methods of boron nitride ceramic fiber were introduced as well as the advantages and disadvantages of boron nitride ceramic fibers prepared with various precursors. At last, the prospect and trend of research of polymer derived boron nitride ceramic fiber were viewed.
Boron nitride ceramic fiber is a new developing high-performance material. But the traditional method of high-temperature synthesis is hard to prepare high-quality boron nitride ceramic fiber which can only be prepared by the method of polymer derived ceramics(PDCs). In the article, synthesis methods of boron nitride ceramic fiber were introduced as well as the advantages and disadvantages of boron nitride ceramic fibers prepared with various precursors. At last, the prospect and trend of research of polymer derived boron nitride ceramic fiber were viewed.
引文
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[5]丁杨,曹峰,陈莉.先驱体法制备氮化硼陶瓷材料的研究进展[J].材料导报,2013,27(9):142-145.
[6]王开宇,陈斐,李传山,等.无机前驱体法制备连续氮化硼纤维及其结构表征[J].现代技术陶瓷,2013,34(6):3-6.
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[9]雷永鹏.先驱体转化法制备氮化硼纤维研究[D].长沙:国防科学技术大学,2011.
[10]薛金根,王应德,李效东,等.分子设计在聚硅烷合成中的应用[J].有机硅材料,2005,19(3):13-16.
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[13]Dong S,Zhao T,Xu C.Synthesis and ceramic conversion of a new oligomeric precursor to boron nitride[J].Polymers for Advanced Technologies,2011,22(12):2474–2479.
[14]Wideman T,Sneddon L G.Dipentylamine-Modified Polyborazylene:?A New,Melt-Spinnable Polymeric Precursor to Boron Nitride Ceramic Fibers[J].Chemistry of Materials,1996,8(8).
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[20]王钰.六方氮化硼(h-BN)前驱体的合成研究[D].北京:北京化工大学,2007.
[21]Narula C K,Schaeffer R,Paine R T,et al.Synthesis of boron nitride ceramics from poly(borazinylamine)precursors[J].Journal of the American Chemical Society,1987,109(18):5556-5557.
[22]Narula C K,Schaeffer R,Datye A K,et al.Synthesis of boron nitride ceramics from oligomeric precursors derived from2-(dimethylamino)-4,6-dichloroborazine[J].Chemistry of Materials,1990,2(4):384-389.
[23]Kimura Y,Kubo Y,Hayashi N.Boron nitride preceramics based on B,B,B-triaminoborazine[J].Journal of Inorganic&Organometallic Polymers,1992,2(2):231-242.
[24]Duperrier S,Gervais C,Bernard S,et al.Controlling the chemistry,morphology and structure of boron nitride-based ceramic fibers through a comprehensive mechanistic study of the reactivity of spinnable polymers with ammonia[J].Journal of Materials Chemistry,2006,16(30):3126-3138.
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[26]Duperrier S,Chiriac R,Bernard S,et al.Design of a Series of Preceramic B-Tri(methylamino)borazine-Based Polymers as Fiber Precursors:?Architecture,Thermal Behavior,and Melt-Spinnability[J].Macromolecules,2007,40(4):1018-1027.
[27]Duperrier S,Chiriac R,Sigala C,et al.Thermal behaviour of a series of poly[B-(methylamino)borazine]for the preparation of boron nitride fibers[J].Journal of the European Ceramic Society,2009,29(5):851-855.
[28]Toury B,Bernard S,Cornu D,et al.High-Performance Boron Nitride Fibers Obtained from Asymmetric Alkylaminoborazine[J].Journal of Materials Chemistry,2003,13(2):274-279.
[29]邓橙,宋永才,王应德,等.氮化硼纤维先驱体的制备与表征[J].高等学校化学学报,2010,31(3):623-628.
[30]邓橙,宋永才,王应德,等.甲胺/二甲胺共取代合成氮化硼先驱体聚硼氮烷[J].化学学报,2010,68(12):1217-1222.
[31]邓橙.氮化硼纤维先驱体—聚硼氮烷的合成及热解特性研究[D].长沙:国防科学技术大学,2009.
[32]雷永鹏,王应德.聚正丙胺/甲胺基环硼氮烷的裂解[J].硅酸盐学报,2012,40(8):1179-1183.
[33]Zhong B,Chai Z,Xia L,et al.A Novel Polymeric Precursor for Boron Nitride Ceramics:Synthesis,Characterization,and Ceramic Conversion[J].International Journal of Applied Ceramic Technology,2016,13(5):929-936.
[34]Cornu D,Bernard S,Duperrier S,et al.Alkylaminoborazine-based precursors for the preparation of boron nitride fibers by the polymer-derived ceramics(PDCs)route[J].Journal of the European Ceramic Society,2005,25(2–3):111-121.
[35]曹义苗,李书同,韩克清,等.氮化硼纤维先驱体聚合物的合成及其表征[J].合成纤维,2009,38(1):32-35.
[36]Chen M W,Ge M,Zhang W G.Preparation and properties of hollow BN fibers derived from polymeric precursors[J].Journal of the European Ceramic Society,2012,32(32):1216-1222.
[37]陈明伟,戈敏,张伟刚.有机前驱体法BN纤维的制备和表征[J].无机材料学报,2012,27(11):1216-1222.
[38]叶丽,孙妮娟,韩伟健,等.氮化硼陶瓷前驱体的制备及表征[J].宇航材料工艺,2013,43(4):39-44.
[39]李文华,王军,谢征芳,等.新型氮化硼陶瓷纤维先驱体——含硅聚硼氮烷的合成与表征[J].化学学报,2011,69(16):1936-1940.
[40]李文华,王军,谢征芳,等.含硅聚硼氮烷裂解转化制备氮化硼陶瓷纤维[J].化学学报,2012,70(1):99-102.
[41]李文华.先驱体转化法制备连续Si BN陶瓷纤维基础研究[D].长沙:国防科学技术大学,2012.
[2]顾学民,龚毅生,等.无机化学丛书.第2卷,铍、碱土金属、硼、铝、镓分族[M].北京:科学出版社,2011.
[3]李俊生,张长瑞,李斌.氮化硼陶瓷先驱体研究进展[J].硅酸盐通报,2011,30(3):567-571.
[4]李端,张长瑞,李斌,等.氮化硼透波材料的研究进展与展望[J].硅酸盐通报,2010,29(5):1072-1078.
[5]丁杨,曹峰,陈莉.先驱体法制备氮化硼陶瓷材料的研究进展[J].材料导报,2013,27(9):142-145.
[6]王开宇,陈斐,李传山,等.无机前驱体法制备连续氮化硼纤维及其结构表征[J].现代技术陶瓷,2013,34(6):3-6.
[7]Bernard S,Salameh C,Moussa G,et al.BN Nanoceramics[J].Encyclopedia of Polymeric Nanomaterials,2015:1-12.
[8]李俊生.硼吖嗪的合成及其转化制备氮化硼研究[D].长沙:国防科学技术大学,2011.
[9]雷永鹏.先驱体转化法制备氮化硼纤维研究[D].长沙:国防科学技术大学,2011.
[10]薛金根,王应德,李效东,等.分子设计在聚硅烷合成中的应用[J].有机硅材料,2005,19(3):13-16.
[11]Kimura Y,Taniguchi I,Yamamoto K.Process of preparing organoboron nitride polymer:US,US 4731437 A[P].1988.
[12]Fazen P J,Beck J S,Lynch A T,et al.Thermally induced borazine dehydropolymerization reactions.Synthesis and ceramic conversion reactions of a new high-yield polymeric precursor to boron nitride[J].Chemistry of Materials,1990,2(2):96-97.
[13]Dong S,Zhao T,Xu C.Synthesis and ceramic conversion of a new oligomeric precursor to boron nitride[J].Polymers for Advanced Technologies,2011,22(12):2474–2479.
[14]Wideman T,Sneddon L G.Dipentylamine-Modified Polyborazylene:?A New,Melt-Spinnable Polymeric Precursor to Boron Nitride Ceramic Fibers[J].Chemistry of Materials,1996,8(8).
[15]Wideman T,Edward E.Remsen,Enriqueta Cortez,et al.Amine-Modified Polyborazylenes:?Second-Generation Precursors to Boron Nitride[J].Chemistry of Materials,1998,10(1):412-421.
[16]Lynch A T,Sneddon L G.Transition-metal-promoted reactions of boron hydrides.10.Rhodium-catalyzed syntheses of B-alkenylborazines[J].Journal of the American Chemical Society,2002,109(19):5867-5868.
[17]Lynch A T,Sneddon L G.Transition-metal-promoted reactions of boron hydrides.12.Syntheses,polymerizations,and ceramic conversion reactions of B-alkenylborazines[J].Journal of the American Chemical Society,2002,111(16):6201-6209.
[18]Bernard S,Cornu D,Duperrier S,et al.Borazine Based Preceramic Polymers for Advanced BN Materials[C].Inorganic and Organometallic Macromolecules Design and Applications,Springer,2008:351-371.
[19]Brown C A,Laubengayer A W.B-trichloroborazole[J].Journal of the American Chemical Society,1955,77(14):3699-3700.
[20]王钰.六方氮化硼(h-BN)前驱体的合成研究[D].北京:北京化工大学,2007.
[21]Narula C K,Schaeffer R,Paine R T,et al.Synthesis of boron nitride ceramics from poly(borazinylamine)precursors[J].Journal of the American Chemical Society,1987,109(18):5556-5557.
[22]Narula C K,Schaeffer R,Datye A K,et al.Synthesis of boron nitride ceramics from oligomeric precursors derived from2-(dimethylamino)-4,6-dichloroborazine[J].Chemistry of Materials,1990,2(4):384-389.
[23]Kimura Y,Kubo Y,Hayashi N.Boron nitride preceramics based on B,B,B-triaminoborazine[J].Journal of Inorganic&Organometallic Polymers,1992,2(2):231-242.
[24]Duperrier S,Gervais C,Bernard S,et al.Controlling the chemistry,morphology and structure of boron nitride-based ceramic fibers through a comprehensive mechanistic study of the reactivity of spinnable polymers with ammonia[J].Journal of Materials Chemistry,2006,16(30):3126-3138.
[25]Kimura Y,Kubo Y,Hayashi N.High-performance boron-nitride fibers from poly(borazine)preceramics[J].Composites Science&Technology,1994,51(2):173-179.
[26]Duperrier S,Chiriac R,Bernard S,et al.Design of a Series of Preceramic B-Tri(methylamino)borazine-Based Polymers as Fiber Precursors:?Architecture,Thermal Behavior,and Melt-Spinnability[J].Macromolecules,2007,40(4):1018-1027.
[27]Duperrier S,Chiriac R,Sigala C,et al.Thermal behaviour of a series of poly[B-(methylamino)borazine]for the preparation of boron nitride fibers[J].Journal of the European Ceramic Society,2009,29(5):851-855.
[28]Toury B,Bernard S,Cornu D,et al.High-Performance Boron Nitride Fibers Obtained from Asymmetric Alkylaminoborazine[J].Journal of Materials Chemistry,2003,13(2):274-279.
[29]邓橙,宋永才,王应德,等.氮化硼纤维先驱体的制备与表征[J].高等学校化学学报,2010,31(3):623-628.
[30]邓橙,宋永才,王应德,等.甲胺/二甲胺共取代合成氮化硼先驱体聚硼氮烷[J].化学学报,2010,68(12):1217-1222.
[31]邓橙.氮化硼纤维先驱体—聚硼氮烷的合成及热解特性研究[D].长沙:国防科学技术大学,2009.
[32]雷永鹏,王应德.聚正丙胺/甲胺基环硼氮烷的裂解[J].硅酸盐学报,2012,40(8):1179-1183.
[33]Zhong B,Chai Z,Xia L,et al.A Novel Polymeric Precursor for Boron Nitride Ceramics:Synthesis,Characterization,and Ceramic Conversion[J].International Journal of Applied Ceramic Technology,2016,13(5):929-936.
[34]Cornu D,Bernard S,Duperrier S,et al.Alkylaminoborazine-based precursors for the preparation of boron nitride fibers by the polymer-derived ceramics(PDCs)route[J].Journal of the European Ceramic Society,2005,25(2–3):111-121.
[35]曹义苗,李书同,韩克清,等.氮化硼纤维先驱体聚合物的合成及其表征[J].合成纤维,2009,38(1):32-35.
[36]Chen M W,Ge M,Zhang W G.Preparation and properties of hollow BN fibers derived from polymeric precursors[J].Journal of the European Ceramic Society,2012,32(32):1216-1222.
[37]陈明伟,戈敏,张伟刚.有机前驱体法BN纤维的制备和表征[J].无机材料学报,2012,27(11):1216-1222.
[38]叶丽,孙妮娟,韩伟健,等.氮化硼陶瓷前驱体的制备及表征[J].宇航材料工艺,2013,43(4):39-44.
[39]李文华,王军,谢征芳,等.新型氮化硼陶瓷纤维先驱体——含硅聚硼氮烷的合成与表征[J].化学学报,2011,69(16):1936-1940.
[40]李文华,王军,谢征芳,等.含硅聚硼氮烷裂解转化制备氮化硼陶瓷纤维[J].化学学报,2012,70(1):99-102.
[41]李文华.先驱体转化法制备连续Si BN陶瓷纤维基础研究[D].长沙:国防科学技术大学,2012.