古代字画加速器质谱~(14)C测年研究
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摘要
古代字画的年代决定了字画的价格,其年代的鉴定是收藏界非常关心的问题和难题。本文采用GXNU-AMS(广西师范大学单极静电~(14)C专用AMS)~(14)C测年法(~(14)C-AMS)测定一幅古画的年代。结果显示,GXNU-AMS系统具备良好的测试条件;此古画纸质材料的~(14)C年龄为(489±20)BP,经年轮校正曲线校正后的结果显示属明代早期(1412-1444AD),与古画内容描述的年代相符。
The age of ancient painting determines it's price,and the identification of its age is a big problem that the collectors concerned about.In this paper,an ancient painting sample is measured with the GXNU-AMS(a single stage dedicated accelerator mass spectrometry at Guangxi Normal University),and the ~(14)C age is determined to be the 489±20 BP.The calendar ages of the samples are determined to be in a period from 1412 to 1444 AD(95% confidence level)calibrated with intcal 13,which show that the ancient painting is a product in the early Ming Dynasty.
The age of ancient painting determines it's price,and the identification of its age is a big problem that the collectors concerned about.In this paper,an ancient painting sample is measured with the GXNU-AMS(a single stage dedicated accelerator mass spectrometry at Guangxi Normal University),and the ~(14)C age is determined to be the 489±20 BP.The calendar ages of the samples are determined to be in a period from 1412 to 1444 AD(95% confidence level)calibrated with intcal 13,which show that the ancient painting is a product in the early Ming Dynasty.
引文
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[2]王亚龙.从纸张特性分析传统书画修复装裱的科学优化[J].文物春秋,2017(2):58-61,79.
[3]余辉.地志学在古画鉴定中的作用[J].美术观察,2004(3):93-96.DOI:10.3969/j.issn.1006-8899.2004.03.044.
[4]徐新云,徐怡涛.试论建筑形制考古类型学研究成果对碳十四测年数据分析的关键性作用:以山西万荣稷王庙大殿为例[J].故宫博物院院刊,2016(3):41-54,160.
[5]徐从先.中国书画鉴定的几种思致[J].河南师范大学学报(哲学社会科学版),2011,38(2):266-268.
[6]彭清涛,胡文祥.现代分析仪器的新应用[J].现代仪器,1999(6):4-9.
[7]鲁力.科技手段与书画鉴定[N].联合日报,2015-07-07(A03).
[8]仇士华,蔡莲珍.14 C测年及科技考古论集[M].北京:文物出版社,2009:1-7.
[9]姜山,董克君,何明.超灵敏加速器质谱技术进展及应用[J].岩矿测试,2012,31(1):7-23.
[10]SHEN Hongtao,JIANG Shan,HE Ming,et al.AMS measurements of fission products at CIAE[J].Nuclear Inst and Methods in Physics Research,B,2013,294:136-142.DOI:10.1016/j.nimb.2012.06.019.
[11]张雪莲.中国碳十四考古年代学的开拓者[J].大众考古,2016(12):43-46.
[12]仇士华、蔡莲珍.夏商周断代工程中的碳十四年代框架[J].考古,2001(2):90-98.
[13]庞义俊,何明,杨旭冉,等.基于小型单极加速器质谱测量14 C的样品制备技术研究[J].原子能科学技术,2017,51(10):1866-1873.
[14]HIROTAKA O,YASUKAZU Y,TOSHIO N,et al.AMS radiocarbon dating of ancient Japanese sutras[J].Nuclear Inst and Methods in Physics Research,B,2000,172(1):736-740.DOI:info:doi/10.18999/sumrua.12.44.
[15]FUSA M.Reconstruction of cosmic-ray intensity in the past from measurements of radiocarbon in tree rings[D].Nagoya,Janpan:Nagoya University,2014.
[16]SZIDAT S,QUINTERO G A,VOGEL E,et al.14 C analysis and sample preparation at the New Bern Laboratory for the analysis of radiocarbon with AMS(LARA)[J].Radiocarbon,2014,56(2):561-566.DOI:10.1017/S0033822200049602.
[17]XU Xiaomei,Trumbore S E,ZHENG Shuhui,et al.Modifying a sealed tube zinc reduction method for preparation of AMS graphite targets:Reducing background and attaining high precision[J].Nuclear Inst and Methods in Physics Research,B,2007,259(1):320-329.DOI:10.1016/j.nimb.2007.01.175.
[18]JIANG S,HE M,DONG K J,et al.Large projects at the accelerator mass spectrometry facility at the China Institute of Atomic Energy during the last 12years[J].Nucl Instrum Methods B,2013,294:39-42.DOI:10.1016/j.nimb.2012.02.011.
[19]SUTER M.Challenging developments in three decades of accelerator mass spectrometry at eth:fromlarge particle accelerators to table size instruments[J].European Journal of Mass Spectrometry,2010,16(3):471-478.DOI:10.1255/ejms.1078.
[20]HE Ming,BAO Yiwen,PANG Yijun,et al.A home-made 14 C AMS system at CIAE[J].Nuclear Inst and Methods in Physics Research,B,2019,438:214-217.DOI:10.1016/j.nimb.2018.03.035.
[21]李坤,郭之虞.加速器质谱14 C断代[J].原子核物理评论,1997,14(1):53-56.
[22]SANTOS G M,MOORE R B,SOUTHON J R,et al.AMS 14 C sample preparation at the KCCAMS/UCI facility:status report and performance of small sample[J].Radiocarbon,2007,49(2):255-270.DOI:10.1017/S0033822200042181.
[23]刘克新,丁杏芳,傅东坡.北京大学AMS 14 C国际比对样品测量[J].第四纪研究,2007,27(3):469-473.DOI:10.3321/j.issn:1001-7410.2007.03.020.
[24]JANOVICS R,KELEMEN D I,KERN Z,et al.Radiocarbon signal of a low and intermediate level radioactive waste disposal facility in nearby trees[J].Journal of Environmental Radioactivity,2016,153:10-14.DOI:10.1016/j.jenvrad.2015.10.008.