黄芪甲苷含量测定研究进展
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摘要
对黄芪甲苷含量测定中的样品预处理和各种测定方法的研究进展进行了综述,评述了每种方法的特点,为黄芪甲苷含量的测定提供参考。
This study reviewed the research progress of sample pretreatment and various methods of astragaloside Ⅳ determination, and the characteristics of each method were assessed. It provided the reference for the determination of astragaloside Ⅳ.
This study reviewed the research progress of sample pretreatment and various methods of astragaloside Ⅳ determination, and the characteristics of each method were assessed. It provided the reference for the determination of astragaloside Ⅳ.
引文
[1] 国家药典委员会.中华人民共和国药典(一部)[M].北京:化学工业出版社,2015:302.
[2] Chu Chu,Lian-Wen Qi,E-Hu Liu,et al.Radix Astragali(Astragalus):Latest advancements and trends in chemistry,analysis,pharmacology and pharmacokinetics[J].Current Organic Chemistry,2010,14,1792-1807.
[3] Lei Li,Xiaojiao Hou,Rongfang Xu,et al.Research review on the pharmacological effects of Astragaloside IV[J].Fundamental and Clinical Pharmacology,2017,31(1):17-36.
[4] 丁如贤,李霞,李一珺,等.药材、饮片中黄芪甲苷含量测定方法的改进[J].世界中医药,2013,8(6):669-671.
[5] 刘浩文,刘嘉仪,杨妙荣,等.黄芪药材中黄芪甲苷含量测定的两种方法的比较研究[J].中药新药与临床药理,2011,22(6):659-662.
[6] 朱蕾.柱前衍生-高效液相色谱法测定保健食品中黄芪甲苷含量[D].北京:中国疾病预防与控制中心,2006.
[7] 李永吉,管庆霞,关延彬,等.HPLC与比色法测定复方黄芪注射液中总皂苷与黄芪甲苷含量[J].黑龙江医药,2004,17(1):1-3.
[8] 卢伟,孙晓敏,孙佳佳,等.2种黄芪甲苷含量测定方法比较 [J].中医临床研究,2016,8(2):43-45.
[9] 杨连梅,刘养清,赵慧辉,等.黄芪药材中黄芪甲苷含量的荧光分光光度法测定[J].时珍国医国药,2010,21(9):2272-2273.
[10] 刘丰丰,王海宁,李明,等.薄层扫描法测定黄芪颗粒中黄芪甲苷含量 [J].中国药业,2006,15(14):17-18.
[11] 肖辛垣,李文斌,李楚云,等.薄层扫描法测定健儿涂膜剂中黄芪甲苷含量 [J].医药导报,2007,26(8):954-955.
[12] Jing Zhang,Mei Meng,Ying Jiang,et al.A new approach to develop a standardized method for simultaneous analysis of Astragaloside Ⅳ and formononetin in Radix Astragali by High-Performance Thin Layer Chromatography[J].Journal of Planar Chromatography,2015,28(4):268-273.
[13] 姜丽丽,张传领,苏丽娟,等.HPLC-UV法测定黄芪干燥根中黄芪甲苷的含量[J].安徽农业科学,2014,42(22):7381-7383.
[14] Meicun Yao,Ying Qi,Kaishun Bi,et al.A precolumn derivatization High-Performance Liquid Chromatographic method with improved sensitivity and specificity for the determination of Astragaloside Ⅳ in Radix Astragali[J].Journal of Chromatographic Science,2000,38:325-328.
[15] 侯素云,王宗权,贾继明.黄芪甲苷提取物中黄芪甲苷含量测定方法比较研究[J].河北医科大学学报,2012,33(5):544-547.
[16] Wenkui Li,John F Fitzloff.Determination of AstragalosideⅣ in Radix Astragali(Astragalus membranaceus var.monghulicus) using High-Performance Liquid Chromatography with Evaporative Light-Scattering Detection[J].Journal of Chromatographic Science,2001,39:459-462.
[17] 王佳,冯建安,李希,等.HPLC-ELSD法测定归芪升白颗粒中黄芪甲苷含量[J].亚太传统医药,2017,13(5):41-43.
[18] 赵晓丽.高效液相色谱-蒸发光散射检测器法测定芪芳气血颗粒中黄芪甲苷含量分析[J].实用中医药杂志,2017,33(7):858-860.
[19] 王红,杨慈海,宋军,等.高效液相色谱-蒸发光散射检测法测定抗栓通络丸中黄芪甲苷含量[J].中国药业,2016,25(4):75-77.
[20] 翟晓茹,李永东,张红兵,等.蚁参护肝口服液中黄芪甲苷含量测定的方法研究[J].北方药学,2017,14(7):1-2.
[21] 林帅军,崔燕兵,邢志霞,等.HPLC-ELSD法测定乙肝益气解郁颗粒中黄芪甲苷含量[J].中医药导报,2017,23(5):47-49.
[22] 彭玲娜,李劲平,蒋秋桃,等.HPLC-ELSD测定柏子养心片中黄芪甲苷含量 [J].海峡药学,2017,29(7):63-66.
[23] 卢伟,孙晓敏,孙佳佳,等.2种黄芪甲苷含量测定方法的比较[J].中医临床研究,2016,8(2):43-45.
[24] 张火旺,蔡勇科,吴志国,等.高效液相色谱-蒸发光散射检测法测定养阴生津片中黄芪甲苷含量[J].中国药业,2016,25(20):53-55.
[25] 段春改,陈钟,李菲,等.HPLC-ELSD法测定芪黄通秘软胶囊中黄芪甲苷含量[J].亚太传统医药,2015,11(1):23-25.
[26] 万萌萌,康新莉,谭睿,等.高效液相色谱法测定脑脉康颗粒中黄芪甲苷含量[J].中国药业,2015,24(20):75-76.
[27] 葛德洲,邓祖磊.高效液相色谱-蒸发光散射法测定甜梦胶囊中黄芪甲苷含量[J].中国药业,2015,24(5):31-32.
[28] 王海燕,柳庆坤,刘广文.芪参安胃口服液中黄芪甲苷含量测定的研究[J].中国医院用药评价与分析,2015,15(3):292-295.
[29] 李光河.液相色谱-质谱法测定丹溪玉屏风颗粒中黄芪甲苷含量[J].中国药业,2017,26(7):21-23.
[30] 刘兴国,李丽红,李仁勇,等.新型电喷雾式检测器CAD与蒸发光散射检测器ELSD用于分析黄芪甲苷的对比研究[C]//第11届全国青年药学工作者最新科研成果交流会论文集.杭州:中国药学会,2012:495-501.
[31] 李效宽,张艳海,冯天辉,等.在线固相萃取法结合电雾式检测器测定黄芪及其复方中黄芪甲苷含量[J].分析化学,2014,42(12):1791-1796.
[32] 梁慧敏,欧妮.高效液相色谱-电喷雾检测器法测定贞芪扶正颗粒中黄芪甲苷含量[J].中国药业,2016,25(5):55-57.
[33] 于泓,牟世芬.离子色谱中的安培检测方法及其应用[J].化学通报,2007,7:483-488.
[34] Ha-Jeong Kwon,Yong-Duk Park.Determination of astragalin and astragaloside content in Radix Astragali using high-performance liquid chromatography coupled with pulsed amperometric detection[J].Journal of Chromatography A,2012,1232:212-217.
[35] Li Wang,Zhan Zhang,Xinyu Yu,et al.An efficient,sensitive and accurate method for the detection of astragaloside Ⅳ in Chinese functional spirit by ultra-performance liquid chromatography-quadrupole-orbitrap mass spectrometry[J].Analytical Methods,2015(7):10199-10206.
[36] 华云鹏,雍太萍,宗宁峰,等.UPLC-MS/MS法同时测定安喘舒丸中腺苷和黄芪甲苷含量[J].中国现代中药,2016,18(8):1055-1057.
[37] Li Gu,Ying Liang,Tianshu Zhou,et al.A novel electrochemical sensor based on boronic acid-functionalized multiwalled carbon nanotubes for astragaloside IV determination using ARS as the current indicator[J].Analytical Methods,2012(4):492-495.
[38] 战皓,吴宏伟,张东,等.近红外光谱法测定不同产地黄芪中毛蕊异黄酮葡糖糖苷和黄芪甲苷含量[J].光谱学与光谱分析,2017,37(5):1391-1396.
[2] Chu Chu,Lian-Wen Qi,E-Hu Liu,et al.Radix Astragali(Astragalus):Latest advancements and trends in chemistry,analysis,pharmacology and pharmacokinetics[J].Current Organic Chemistry,2010,14,1792-1807.
[3] Lei Li,Xiaojiao Hou,Rongfang Xu,et al.Research review on the pharmacological effects of Astragaloside IV[J].Fundamental and Clinical Pharmacology,2017,31(1):17-36.
[4] 丁如贤,李霞,李一珺,等.药材、饮片中黄芪甲苷含量测定方法的改进[J].世界中医药,2013,8(6):669-671.
[5] 刘浩文,刘嘉仪,杨妙荣,等.黄芪药材中黄芪甲苷含量测定的两种方法的比较研究[J].中药新药与临床药理,2011,22(6):659-662.
[6] 朱蕾.柱前衍生-高效液相色谱法测定保健食品中黄芪甲苷含量[D].北京:中国疾病预防与控制中心,2006.
[7] 李永吉,管庆霞,关延彬,等.HPLC与比色法测定复方黄芪注射液中总皂苷与黄芪甲苷含量[J].黑龙江医药,2004,17(1):1-3.
[8] 卢伟,孙晓敏,孙佳佳,等.2种黄芪甲苷含量测定方法比较 [J].中医临床研究,2016,8(2):43-45.
[9] 杨连梅,刘养清,赵慧辉,等.黄芪药材中黄芪甲苷含量的荧光分光光度法测定[J].时珍国医国药,2010,21(9):2272-2273.
[10] 刘丰丰,王海宁,李明,等.薄层扫描法测定黄芪颗粒中黄芪甲苷含量 [J].中国药业,2006,15(14):17-18.
[11] 肖辛垣,李文斌,李楚云,等.薄层扫描法测定健儿涂膜剂中黄芪甲苷含量 [J].医药导报,2007,26(8):954-955.
[12] Jing Zhang,Mei Meng,Ying Jiang,et al.A new approach to develop a standardized method for simultaneous analysis of Astragaloside Ⅳ and formononetin in Radix Astragali by High-Performance Thin Layer Chromatography[J].Journal of Planar Chromatography,2015,28(4):268-273.
[13] 姜丽丽,张传领,苏丽娟,等.HPLC-UV法测定黄芪干燥根中黄芪甲苷的含量[J].安徽农业科学,2014,42(22):7381-7383.
[14] Meicun Yao,Ying Qi,Kaishun Bi,et al.A precolumn derivatization High-Performance Liquid Chromatographic method with improved sensitivity and specificity for the determination of Astragaloside Ⅳ in Radix Astragali[J].Journal of Chromatographic Science,2000,38:325-328.
[15] 侯素云,王宗权,贾继明.黄芪甲苷提取物中黄芪甲苷含量测定方法比较研究[J].河北医科大学学报,2012,33(5):544-547.
[16] Wenkui Li,John F Fitzloff.Determination of AstragalosideⅣ in Radix Astragali(Astragalus membranaceus var.monghulicus) using High-Performance Liquid Chromatography with Evaporative Light-Scattering Detection[J].Journal of Chromatographic Science,2001,39:459-462.
[17] 王佳,冯建安,李希,等.HPLC-ELSD法测定归芪升白颗粒中黄芪甲苷含量[J].亚太传统医药,2017,13(5):41-43.
[18] 赵晓丽.高效液相色谱-蒸发光散射检测器法测定芪芳气血颗粒中黄芪甲苷含量分析[J].实用中医药杂志,2017,33(7):858-860.
[19] 王红,杨慈海,宋军,等.高效液相色谱-蒸发光散射检测法测定抗栓通络丸中黄芪甲苷含量[J].中国药业,2016,25(4):75-77.
[20] 翟晓茹,李永东,张红兵,等.蚁参护肝口服液中黄芪甲苷含量测定的方法研究[J].北方药学,2017,14(7):1-2.
[21] 林帅军,崔燕兵,邢志霞,等.HPLC-ELSD法测定乙肝益气解郁颗粒中黄芪甲苷含量[J].中医药导报,2017,23(5):47-49.
[22] 彭玲娜,李劲平,蒋秋桃,等.HPLC-ELSD测定柏子养心片中黄芪甲苷含量 [J].海峡药学,2017,29(7):63-66.
[23] 卢伟,孙晓敏,孙佳佳,等.2种黄芪甲苷含量测定方法的比较[J].中医临床研究,2016,8(2):43-45.
[24] 张火旺,蔡勇科,吴志国,等.高效液相色谱-蒸发光散射检测法测定养阴生津片中黄芪甲苷含量[J].中国药业,2016,25(20):53-55.
[25] 段春改,陈钟,李菲,等.HPLC-ELSD法测定芪黄通秘软胶囊中黄芪甲苷含量[J].亚太传统医药,2015,11(1):23-25.
[26] 万萌萌,康新莉,谭睿,等.高效液相色谱法测定脑脉康颗粒中黄芪甲苷含量[J].中国药业,2015,24(20):75-76.
[27] 葛德洲,邓祖磊.高效液相色谱-蒸发光散射法测定甜梦胶囊中黄芪甲苷含量[J].中国药业,2015,24(5):31-32.
[28] 王海燕,柳庆坤,刘广文.芪参安胃口服液中黄芪甲苷含量测定的研究[J].中国医院用药评价与分析,2015,15(3):292-295.
[29] 李光河.液相色谱-质谱法测定丹溪玉屏风颗粒中黄芪甲苷含量[J].中国药业,2017,26(7):21-23.
[30] 刘兴国,李丽红,李仁勇,等.新型电喷雾式检测器CAD与蒸发光散射检测器ELSD用于分析黄芪甲苷的对比研究[C]//第11届全国青年药学工作者最新科研成果交流会论文集.杭州:中国药学会,2012:495-501.
[31] 李效宽,张艳海,冯天辉,等.在线固相萃取法结合电雾式检测器测定黄芪及其复方中黄芪甲苷含量[J].分析化学,2014,42(12):1791-1796.
[32] 梁慧敏,欧妮.高效液相色谱-电喷雾检测器法测定贞芪扶正颗粒中黄芪甲苷含量[J].中国药业,2016,25(5):55-57.
[33] 于泓,牟世芬.离子色谱中的安培检测方法及其应用[J].化学通报,2007,7:483-488.
[34] Ha-Jeong Kwon,Yong-Duk Park.Determination of astragalin and astragaloside content in Radix Astragali using high-performance liquid chromatography coupled with pulsed amperometric detection[J].Journal of Chromatography A,2012,1232:212-217.
[35] Li Wang,Zhan Zhang,Xinyu Yu,et al.An efficient,sensitive and accurate method for the detection of astragaloside Ⅳ in Chinese functional spirit by ultra-performance liquid chromatography-quadrupole-orbitrap mass spectrometry[J].Analytical Methods,2015(7):10199-10206.
[36] 华云鹏,雍太萍,宗宁峰,等.UPLC-MS/MS法同时测定安喘舒丸中腺苷和黄芪甲苷含量[J].中国现代中药,2016,18(8):1055-1057.
[37] Li Gu,Ying Liang,Tianshu Zhou,et al.A novel electrochemical sensor based on boronic acid-functionalized multiwalled carbon nanotubes for astragaloside IV determination using ARS as the current indicator[J].Analytical Methods,2012(4):492-495.
[38] 战皓,吴宏伟,张东,等.近红外光谱法测定不同产地黄芪中毛蕊异黄酮葡糖糖苷和黄芪甲苷含量[J].光谱学与光谱分析,2017,37(5):1391-1396.