石英纤维增强石英陶瓷复合材料制备研究进展
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摘要
石英纤维增强石英(SiO_(2f)/SiO_2)陶瓷复合材料具有优良的力学、介电、烧蚀和热物理等综合性能,是高速导弹天线罩、天线窗的首选材料。本文从石英纤维增强石英陶瓷复合材料的制备方法、石英纤维织物结构及预处理工艺、循环浸渍及后处理工艺、复合材料防潮处理和复合材料的发展等方面简述了国内外的研究进展,并对其未来发展方向进行了展望。
Silica fiber reinforced silica ceramic composites have excellent mechanical, dielectric, ablation and thermophysical properties,and are the preferred materials for high-speed missile radomes and antenna windows. In this paper, the research progress of silica fiber reinforced silica ceramic composites at home and abroad is summarized from the aspects of their preparation methods, the silica fabric structures and the pretreatment technology, the cyclic impregnation and the post-treatment technology, the moisture-proof treatment of composites and the development of composite materials; the directions of their future development are also analyzed.
Silica fiber reinforced silica ceramic composites have excellent mechanical, dielectric, ablation and thermophysical properties,and are the preferred materials for high-speed missile radomes and antenna windows. In this paper, the research progress of silica fiber reinforced silica ceramic composites at home and abroad is summarized from the aspects of their preparation methods, the silica fabric structures and the pretreatment technology, the cyclic impregnation and the post-treatment technology, the moisture-proof treatment of composites and the development of composite materials; the directions of their future development are also analyzed.
引文
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[23]张剑,吕毅,赵英民.2.5D衍生结构SiO2f/SiO2复合材料的经向力学性能[J].宇航材料工艺,2015,(4):87-91.ZHANG J,LV Y,ZHAO Y M.Aerospace Materials&Technology,2015,(4):87-91.
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[25]廉云清,杨杰,周绍建,等.SiO2f/SiO2复合材料中石英纤维的表面处理[J].纤维复合材料,2011,(4):34-37.LIAN Y Q,YANG J,ZHOU S J,et al.Fiber Composites,2011,(4):34-37.
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[27]范锦鹏,张大海,周军,等.一种氧化硅基天线罩复合材料均匀致密化方法[P].中国专利:CN 105272119 A,2016-01-27.
[28]韩爽,蒋凯辉,唐军务,等.2.5D SiO2f/SiO2复合材料制备工艺及性能研究[J].稀有金属材料与工程,2009,(S2):458-461.HAN S,J K H,TANG J W,et al.Rare Metal Materials and Engineering,2009,(S2):458-461.
[29]宋阳曦.二维石英纤维织物增强宽频透波陶瓷基复合材料的制备及性能研究[D].长沙:国防科学技术大学硕士学位论文,2010.
[30]徐道新.3D SiO2f/SiO2复合材料的制备与性能研究[D].哈尔滨:哈尔滨工业大学硕士学位论文,2017.
[31]周绍建,廉云清,杨杰,等.SiO2f/SiO2陶瓷复合材料弯曲性能的研究[J].玻璃钢/复合材料,2014,(8):27-30.ZHOU S J,LIAN Y Q,YANG J,et al.Fiber Reinforced Plastics/Composites,2014,(8):27-30.
[32]张健,黎义,张大海,等.SiO2基复合材料的防潮研究[A].全国复合材料学术会议[C].2000:325-329.
[33]倪必红,肖志红.复合陶瓷天线罩表面防潮性能的研究[J].航天制造技术,2006,2(1):13-16.Ni B H,Xiao Z H.Aerospace Manufacturing Technology,2006,2(1):13-16.
[34]王盼,夏龙,温广武,等.聚硼硅氧烷涂层及其涂覆工艺对SiO2f/SiO2复合材料防潮性能以及力学性能的影响[J].涂料工业,2017,47(10):18-22.WANG P,XIA L,WEN G W,et al.Paint&Coatings Industry,2017,47(10):18-22.
[35]尹正帅,刘义华,王芬,等.烷基化改性对石英复合陶瓷材料性能的影响研究[J].航天制造技术,2015,(5):23-25,29.YIN Z S,LIU Y H,WANG F,et al.Aerospace Manufacturing Technology,2015,(5):23-25,29.
[36]吕小峰.2D-SiO2f/SiO2-BN复合材料的制备与烧蚀性[D].哈尔滨:哈尔滨工业大学硕士学位论文,2013.
[37]李成虎.SiO2f/SiO2-BN复合材料的尿素法制备工艺及性能研究[D].长沙:国防科学技术大学硕士学位论文,2010.
[2]雷景轩.A夹层石英陶瓷的制备[J].硅酸盐通报,2012,31(5):1283-1287.LEI J X.Bulletin of the Chinese Ceramic Society,2012,31(5):1283-1287.
[3]韩桂芳,陈照峰,张立同,等.高温透波材料研究进展[J].航空材料学报,2003,23(1):57-62.HAN G F,CHEN Z F,ZHANG L T,et al.Journal of Aeronautical Materials,2003,23(1):57-62.
[4]陈政伟,那伟,景昭,等.石英陶瓷高温熔融工况动态热响应特性试验及仿真研究[J].人工晶体学报,2018,47(4):873-878.CHEN Z W,NA W,JING Z.Journal of Synthetic Crystals,2018,47(4):873-878.
[5]陈虹,张联盟,李勇,等.三维编织SiO2基复合材料性能的研究[J].硅酸盐学报,2003,31(10):918-922.CHEN H,ZHANG L M,LI Y,et al.Journal of the Chinese Ceramic Society,2003,31(10):918-922.
[6]赵中坚.石英陶瓷天线罩无损检测技术研究[J].陶瓷学报,2014,(4):387-391.ZHAO Z J.Journal of Ceramics,2014,(4):387-391.
[7]刘勇.石英纤维织物结构对二氧化硅基复合材料力学性能影响研究[D].南京:南京航空航天大学博士论文,2013.
[8]马娜,门薇薇,王志强,等.SiBN(C)透波陶瓷纤维研究进展[J].陶瓷学报,2015,36(3):227-232.MA N,MEN W W,WANG Z Q,et al.Journal of Ceramics,2015,36(3):227-232.
[9]李仲平.防热复合材料发展与展望[J].复合材料学报,2011,28(2):1-9.LI Z P.Acta Materiae Compositae Sinica,2011,28(2):1-9.
[10]赖文恩,范锦鹏,张大海,等.针刺石英纤维增强二氧化硅基透波复合材料性能探讨[A].第十八届全国复合材料学术会议论文集(上册)[C].2014:300-304.
[11]雷景轩,邬浩,赵中坚,等.针刺石英纤维预制体增强石英陶瓷复合材料的制备研究[J].玻璃钢,2018,(2):1-5.LEI J X,WU H,ZHAO Z J,et al.Fiber Reinforced Plastics,2018,(2):1-5.
[12]GJB 8358-2015,导弹用石英陶瓷天线罩罩体通用规范[S].
[13]GILREATH M C,CASTELLOW S L.High-temperature dielectric properties of candidate space-shuttle thermalprotection-system and antenna-window materials[R].NASATND-7523,Washington:NASA,1974:1-53.
[14]BRAZEL J,FENTON R.ADL-4D6:A silica/silica composite for hardened antenna windows[C]//Proceedings of the 13th Symposium on Electromagnetic Windows,Atlanta,1976:9-16.
[15]MANOCHA L,PANCHAL C N,MANOCHA S.Silica/silica composites through electrophretic infiltration[C]//26th Annual Conference on Composites,Advanced Ceramics,Materials,and Structures:A.Ceramic Engineering and Science Proceedings,2002,3(3):655-661.
[16]MANOCHA L,PANCHAL C,MANOCHA S.Silica/silica composites through electrophoretic infiltration:Effect of processing conditions on densification of composites[J].Science and Engineering of Composite Materials,2000,9(4):219-230.
[17]张大海,李仲平,范锦鹏,等.热透波材料技术研究进展[J].中国材料进展,2012,31(8):1-6.ZHANG D H,LI Z P,FAN J P,et al.Materials China,2012,31(8):1-6.
[18]韩桂芳,陈照峰,张立同,等.氧化物陶瓷基复合材料研究进展[J].宇航材料工艺,2003,(5):8-11,20.HAN G F,CHEN Z F,ZHANG L T,et al.Aerospace Materials&Technology,2003,(5):8-11,20.
[19]陈晨.新型石英纤维的表征及其石英基复合材料的制备与性能[D].长沙:国防科学技术大学硕士学位论文,2014.
[20]董波,陈达谦,王重海,等.液相渗积工艺制备致密化纤维复合材料[J].现代技术陶瓷,2012,(1):8-9.DONG B,CHEN D Q,WANG C H,et al.Advanced Ceramics,2012,(1):8-9.
[21]贾光耀,陈虹,胡利明,等.三向石英复合材料的研制[J].硅酸盐通报,2002,21(1):3-6.JIA G Y,CHEN H,HU L M,et al.Bulletin of the Chinese Ceramic Society,2002,21(1):3-6.
[22]陈照峰,张立同,成来飞,等.一种透波纤维增强二氧化硅基复合材料的制备方法[P].中国专利:ZL 02114501,2003-10-15.
[23]张剑,吕毅,赵英民.2.5D衍生结构SiO2f/SiO2复合材料的经向力学性能[J].宇航材料工艺,2015,(4):87-91.ZHANG J,LV Y,ZHAO Y M.Aerospace Materials&Technology,2015,(4):87-91.
[24]韦其红,王重海,王洪升,等.耐高温超薄天线窗的制备方法[P].中国专利:CN 103601479 B,2016-05-18.
[25]廉云清,杨杰,周绍建,等.SiO2f/SiO2复合材料中石英纤维的表面处理[J].纤维复合材料,2011,(4):34-37.LIAN Y Q,YANG J,ZHOU S J,et al.Fiber Composites,2011,(4):34-37.
[26]贺光军,李鹏举.复合石英陶瓷材料制造工艺研究[J].空间电子技术,2006,(增刊):186-192.HE G J,LI P J.Space Electronic Technology,2006,(S1):186-192.
[27]范锦鹏,张大海,周军,等.一种氧化硅基天线罩复合材料均匀致密化方法[P].中国专利:CN 105272119 A,2016-01-27.
[28]韩爽,蒋凯辉,唐军务,等.2.5D SiO2f/SiO2复合材料制备工艺及性能研究[J].稀有金属材料与工程,2009,(S2):458-461.HAN S,J K H,TANG J W,et al.Rare Metal Materials and Engineering,2009,(S2):458-461.
[29]宋阳曦.二维石英纤维织物增强宽频透波陶瓷基复合材料的制备及性能研究[D].长沙:国防科学技术大学硕士学位论文,2010.
[30]徐道新.3D SiO2f/SiO2复合材料的制备与性能研究[D].哈尔滨:哈尔滨工业大学硕士学位论文,2017.
[31]周绍建,廉云清,杨杰,等.SiO2f/SiO2陶瓷复合材料弯曲性能的研究[J].玻璃钢/复合材料,2014,(8):27-30.ZHOU S J,LIAN Y Q,YANG J,et al.Fiber Reinforced Plastics/Composites,2014,(8):27-30.
[32]张健,黎义,张大海,等.SiO2基复合材料的防潮研究[A].全国复合材料学术会议[C].2000:325-329.
[33]倪必红,肖志红.复合陶瓷天线罩表面防潮性能的研究[J].航天制造技术,2006,2(1):13-16.Ni B H,Xiao Z H.Aerospace Manufacturing Technology,2006,2(1):13-16.
[34]王盼,夏龙,温广武,等.聚硼硅氧烷涂层及其涂覆工艺对SiO2f/SiO2复合材料防潮性能以及力学性能的影响[J].涂料工业,2017,47(10):18-22.WANG P,XIA L,WEN G W,et al.Paint&Coatings Industry,2017,47(10):18-22.
[35]尹正帅,刘义华,王芬,等.烷基化改性对石英复合陶瓷材料性能的影响研究[J].航天制造技术,2015,(5):23-25,29.YIN Z S,LIU Y H,WANG F,et al.Aerospace Manufacturing Technology,2015,(5):23-25,29.
[36]吕小峰.2D-SiO2f/SiO2-BN复合材料的制备与烧蚀性[D].哈尔滨:哈尔滨工业大学硕士学位论文,2013.
[37]李成虎.SiO2f/SiO2-BN复合材料的尿素法制备工艺及性能研究[D].长沙:国防科学技术大学硕士学位论文,2010.