从NIST Ca标准溶液证书的演变规律揭示标准溶液的使用原则
|
摘要
重点揭示了标准溶液的使用原则。通过对比近30年来NIST Ca标准溶液证书的演变,提出了标准溶液应用的注意事项,并对无机单元素标准溶液的标准值、有效期、定值方法、介质、包装材质及应用等6个方面的技术要素进行了系统地研究与分析。该研究提供了详实的技术信息,有助于实验人员正确地识读和学习证书信息,并合理应用无机单元素标准溶液。
The application principle of standard solution was revealed. By comparing the evolution of NIST Ca standard solution certificate in the past 30 years, the matters needing attention in the application of standard solution were put forward. The technical elements of standard value, validity period, method of setting value, medium, packaging material and application of the inorganic single element standard solution were systematically studied and analyzed. This study provides detailed technical information, it is helpful for the experimenters to correctly read and learn the certi?cate information, and to rationally apply the inorganic single element standard solution.
The application principle of standard solution was revealed. By comparing the evolution of NIST Ca standard solution certificate in the past 30 years, the matters needing attention in the application of standard solution were put forward. The technical elements of standard value, validity period, method of setting value, medium, packaging material and application of the inorganic single element standard solution were systematically studied and analyzed. This study provides detailed technical information, it is helpful for the experimenters to correctly read and learn the certi?cate information, and to rationally apply the inorganic single element standard solution.
引文
[1]张秀艳,常诚,赵静.电感耦合等离子体原子发射光谱法测定铈铁合金中铝硅镍[J].冶金分析,2018,38(9):69-74.
[2]李秋莹,甘建壮,何姣.多元光谱拟合校正-电感耦合等离子体原子发射光谱法测定铱化合物中19种杂质元素[J].冶金分析,2018,38(9):63-68.
[3]孔会民.电感耦合等离子体原子发射光谱(ICP-AES)法测定铅锌选矿流程原尾矿中铅、锌、铜[J].中国无机分析化学,2018,8(5):41-44.
[4]王志远,李帆,王强.电感耦合等离子体原子发射光谱(ICP-AES)法测定钢中Al元素光谱干扰的研究[J].中国无机分析化学,2018,8(5):53-57.
[5]钟跃汉,王利华,孙友宝.ICP-MS微量进样法直接测定海水中微量元素的含量[J].环境化学,2018,37(10):2 329-2 331.
[6]朱有涛,张遐,邵梅.ICP-MS法同时测定预包装食品中的5种常见元素[J].食品工业,2018,39(8):313-315.
[7]陈少萍.ICP-MS法测定水环境中的20种金属元素的含量[J].能源与环境,2018(2):76-77.
[8]赵小学,懋闫锋.微波消解/ICP-MS法测定粮食中的18种痕量元素[J].环境化学,2018,37(3):609-613.
[9]张昂,王飞,钟亚莉.微量乙醇对59种无机元素ICP-MS行为的影响[J].分析实验室,2018,37(3):275-279.
[10]JJG 196-2006常用玻璃量具[S].
[11]JJG 1036-2008电子天平[S].
[12]李云巧.实验室溶液制备手册[M].北京:化学工业出版社,2006:49-50.
[13](英)K.E.贾维斯等著,尹明,李冰译.电感耦合等离子体质谱手册[M].北京:原子能出版社,1997:120-122.
[14]HJ 700-2014水质65种元素的测定电感耦合等离子体质谱法[S].
[15]辛仁轩.等离子体发射光谱分析[M].北京:化学工业出版社,2011:157-158.
[16]李海平.无机标准溶液的稳定性[J].化学分析计量,2016,6(25):106-108.
[2]李秋莹,甘建壮,何姣.多元光谱拟合校正-电感耦合等离子体原子发射光谱法测定铱化合物中19种杂质元素[J].冶金分析,2018,38(9):63-68.
[3]孔会民.电感耦合等离子体原子发射光谱(ICP-AES)法测定铅锌选矿流程原尾矿中铅、锌、铜[J].中国无机分析化学,2018,8(5):41-44.
[4]王志远,李帆,王强.电感耦合等离子体原子发射光谱(ICP-AES)法测定钢中Al元素光谱干扰的研究[J].中国无机分析化学,2018,8(5):53-57.
[5]钟跃汉,王利华,孙友宝.ICP-MS微量进样法直接测定海水中微量元素的含量[J].环境化学,2018,37(10):2 329-2 331.
[6]朱有涛,张遐,邵梅.ICP-MS法同时测定预包装食品中的5种常见元素[J].食品工业,2018,39(8):313-315.
[7]陈少萍.ICP-MS法测定水环境中的20种金属元素的含量[J].能源与环境,2018(2):76-77.
[8]赵小学,懋闫锋.微波消解/ICP-MS法测定粮食中的18种痕量元素[J].环境化学,2018,37(3):609-613.
[9]张昂,王飞,钟亚莉.微量乙醇对59种无机元素ICP-MS行为的影响[J].分析实验室,2018,37(3):275-279.
[10]JJG 196-2006常用玻璃量具[S].
[11]JJG 1036-2008电子天平[S].
[12]李云巧.实验室溶液制备手册[M].北京:化学工业出版社,2006:49-50.
[13](英)K.E.贾维斯等著,尹明,李冰译.电感耦合等离子体质谱手册[M].北京:原子能出版社,1997:120-122.
[14]HJ 700-2014水质65种元素的测定电感耦合等离子体质谱法[S].
[15]辛仁轩.等离子体发射光谱分析[M].北京:化学工业出版社,2011:157-158.
[16]李海平.无机标准溶液的稳定性[J].化学分析计量,2016,6(25):106-108.