气相色谱面积归一法测定无水肼的纯度和水含量

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英文篇名：Purity and water content of anhydrous hydrazine determined by gas chromatography area normalization method 作者：赵小红 ; 匙丹丹 ; 何伟国 ; 刘明雪 ; 贾三海 英文作者：Zhao Xiaohong;Shi Dandan;He Weiguo;Liu Mingxue;Jia Sanhai;Liming Chemical Research and Design Institute Co., Ltd.; 关键词：无水肼 ; 气相色谱 ; 面积归一法 ; 纯度 ; 水含量 英文关键词：anhydrous hydrazine;;gas chromatography;;area normalization method;;purity;;water content 中文刊名：HXTJ 英文刊名：Chemical Propellants & Polymeric Materials 机构：黎明化工研究设计院有限责任公司; 出版日期：2015-07-28 出版单位：化学推进剂与高分子材料 年：2015 期：v.13;No.76 语种：中文; 页：HXTJ201504029 页数：3 CN：04 ISSN：41-1354/TQ 分类号：114-116

摘要

使用Tenax单体填充的色谱柱分离无水肼样品,然后利用热导池检测器测定样品的纯度和水含量,并利用面积归一化法进行定量计算。该方法避免了建立工作曲线的繁琐过程,具有测定快速、准确度高、精密度好等优点。
        The anhydrous hydrazine samples were separated by chromatographic column filled with Tenax monomer,and then the purity and water content of the samples were determined by the thermal conductivity cell detector and calculated quantitatively by the area normalization method.This method avoids the cumbersome processes including establishing of working curves and so on.It possesses the advantages of rapid determination,high accuracy and good precision etc.

引文

[1]李亚裕.液体推进剂[M].北京:中国宇航出版社,2011:287.
    [2]GJB 98-1986无水肼[S],1986.
    [3]MIL-PRF-26536F Performance specification propellant hydrozine[S],2011.