植物提取物微胶囊及其缓释复合织物的制备及胰脂肪酶活性抑制效果
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摘要
本研究旨在制备植物提取物微胶囊并将其与植物复合制备具有一定减肥效果的可用于紧身衣、塑身内衣等的缓释织物。采用界面聚合法以聚乙烯醇为壁材制备了植物提取物(PLE)微胶囊。通过直接涂层的方法将其与涤纶水刺非织造布复合。使用SEM、TG、紫外-可见分光光度计,PhabrOmeter风格仪等测试并评价了微胶囊形貌、耐热性、缓释性能、织物的形貌、服用性能、胰脂肪酶活性抑制率以及微缓释复合织物的最佳制备工艺。结果显示,微胶囊表面光滑圆整,具有较好的热稳定性、缓释性及脂肪酶活性抑制性能;在微胶囊质量分数为4%,热风烘干条件下制备的缓释复合织物具有较好的服用性能以及脂肪酶活性抑制效果,可作为贴衬用于紧身衣,塑身内衣等服装上,起到一定的辅助效果。
This study aimed at preparing a kind of plant extract loaded microcapsules and compositing it with polyester non-woven fabric. The composite fabric could be used as a kind of adjacent fabric in tights and shapewear garments. Plant extracts(PLE) microcapsules were prepared by interfacial polymerization with polyvinyl alcohol as wall material.Through direct coating method, PLE was combined with polyester spunlaced nonwovens. The morphology, thermal stability, slow-release property of the microcapsules, and the morphology, wearability, inhibition rate of pancreatic lipase activity were tested by SEM, TG, UV-Vis spectrophotometer, Phabr Ometer system. The optimum preparation technique was also studied. The results showed that the surface of the microcapsules is smooth, the thermal stability, slow-release property and enzyme inhibition property are relatively good. The composite fabrics which contain 4 w.t % of microcapsules and prepared under hot air drying conditions had relatively good wearability and enzyme inhibition property. It could play a certain auxiliary effect to be used in clothes like tights, shapewear garments, etc.
This study aimed at preparing a kind of plant extract loaded microcapsules and compositing it with polyester non-woven fabric. The composite fabric could be used as a kind of adjacent fabric in tights and shapewear garments. Plant extracts(PLE) microcapsules were prepared by interfacial polymerization with polyvinyl alcohol as wall material.Through direct coating method, PLE was combined with polyester spunlaced nonwovens. The morphology, thermal stability, slow-release property of the microcapsules, and the morphology, wearability, inhibition rate of pancreatic lipase activity were tested by SEM, TG, UV-Vis spectrophotometer, Phabr Ometer system. The optimum preparation technique was also studied. The results showed that the surface of the microcapsules is smooth, the thermal stability, slow-release property and enzyme inhibition property are relatively good. The composite fabrics which contain 4 w.t % of microcapsules and prepared under hot air drying conditions had relatively good wearability and enzyme inhibition property. It could play a certain auxiliary effect to be used in clothes like tights, shapewear garments, etc.
引文
Chakkarapani P.,Subbiah L.,Palanisamy S.,Bibiana A.,Ahrentorp F.,Jonasson C.,and Johansson C.,2015,Encapsulation of methotrexate loaded magnetic microcapsules for magnetic drug targeting and controlled drug release,Journal of Magnetism and Magnetic Materials,380:285-294
Chen M.,Wang Z.W.,Hu C.Y.,and Wang P.L.,2009,Effect of relative humidity on barrier properties of polyvinyl alcohol films,Gaofengzi Cailiao Kexue Yu Gongcheng(Polymer Materials Science and Engineering),(8):61-63(陈默,王志伟,胡长鹰,王平利,2009,湿度对聚乙烯醇膜阻隔性能的影响,高分子材料科学与工程,(8):61-63)
Hu D.Y.,and Guo J.S.,2005,Application of microcapsule technology to the fabric finishing,Ranzheng Jishu(Textile Dyeing and Finishing Journal),27(12):66-68(胡大艳,郭建生,2005,微胶囊技术在织物整理上的应用,染整技术,27(12):66-68)
Huang L.,Qiu B.Y.,and Liu S.H.,2006,Development of microcapsule antibacterial reagent for fabrics,Sichou(Silk Monthly),3:26-29(黄玲,邱白玉,刘少华,2006,微胶囊织物抗菌剂的研制,丝绸,3:26-29)
Hui P.C.,Wang W.,Kan C.,Ng F.S.,Zhou C.,Wat E.,Zhang V.X.,Chan C.,Lau C.B.,and Leung P.,2013,Preparation and char-acterization of chitosan/sodium alginate(CSA)microcapsule containing Cortex Moutan,Colloids and Surfaces A:Physicochem.Eng.Aspects,434:95-101
Li M.,Wang R.,and Liu X.,2017,Preparation and in vitro release performance of geranium wilfordii maxim filled biodegrad-able microcapsules,Polymer Korea,41(3):404-412
Liao Y.L.,Luo S.L.,Zhang Y.Q.,Zhang Y.L.,Li H.Y.,and Liang X.Y.,2015,Introduction of PhabrOmeter-(R)system and its application,Zhongguo Xianjian(China Fiber Inspection),(13):84-86(廖银琳,罗胜利,张宇群,张玉莲,李红英,梁小焰,2015,PhabrOmeter-(R)织物评价系统简介及其应用探讨,中国纤检,(13):84-86)
Liu X.W.,Wang L.Q.,and Liao Z.S.,2017,Research progress of microencapsulation technology in food packaging,Baozhuang Gongcheng(Packaging Engineering),38(1):149-155(刘晓伟,王利强,廖祝胜,2017,微胶囊技术在食品包装中的研究进展,包装工程,38(1):149-155)
Wang A.Q.,Shen L.P.,and Tang Z.X.,2017,Preparation of lanvender microcapsules and its applications in cotton fabric,Zhenzhi Gongye(Knitting Industry),(2):47-50(王爱琼,沈兰萍,汤铸先,2017,薰衣草微胶囊的制备及在棉针织物上的应用,针织工业,(2):47-50)
Wang Y.J.,Ge F.Y.,Cai Z.S.,Jiang J.Y.,and Chen B.L.,2010,Preparation of the mosquito repellent micro-capsule and its ap-plication in the cotton knitted fabric,Zhenzhi Gongye(Knitting Industries),7:34-37(王玉娟,葛风燕,蔡再生,姜建英,陈炳良,2010,防蚊微胶囊的制备及在棉针织物上的应用,针织工业,7:34-37)
Xing S.,Sharp L.K.,and Touchette D.R.,2016,Weight loss drugs and lifestyle modification:perceptions among a diverse adult sample,Patient Educ.Couns.,100(3):592-597
Yin G.,Zhang N.W.,Zhu B.,Aming B.H.,Yan W.,Lian D.P.,Fan Q.,Liu C.,Du D.X.,Zhang D.D.,Zhang Z.,Zhang Y.K.,and Gong K.,2015,A comparison of roux-en-Y gastric bypass and laparoscopic sleeve gastrectomy for severe obesity,Zhongguo Weichuang Waike Zazhi(Chinese Journal of Minimally Invasive Surgery),15(6):487-491(尹刚,张能维,朱斌,阿民布和,闫巍,廉东坡,樊庆,刘晨,杜德晓,张东东,张振,张雁凯,宫轲,2015,腹腔镜Roux-en-Y胃旁路术与腹腔镜胃袖状切除术治疗肥胖病的对比研究,中国微创外科杂志,15(6):487-491)
Zhang W.,Li Q.J.,and Zhang J.F.,2015,Preparation and controlled release of microcapsules via layer-by-layer assembly,Fangzhi Xuebao(Journal of Textile Research),(3):58-62(张维,李秋瑾,张健飞,2015,层层组装微胶囊的制备及其缓释性能,纺织学报,(3):58-62)
Zhao X.,2015,Preparation of chitosan guanidine hydrochloride and application thereof in antimicrobial finishing of wool fabric,Fangzhi Xuebao(Journal of Textile Rese arch),(4):92-96(赵雪,2015,壳聚糖胍盐酸盐的制备及其在羊毛织物抗菌整理中的应用,纺织学报,(4):92-96)
Zorec B.,Préat V.,Miklavc?ic?D.,and Pav?elj N.,2013,Active enhancement methods for intra-and transdermal drug delivery:a review,Zdravni?ki Vestnik,82(5):339-356
Chen M.,Wang Z.W.,Hu C.Y.,and Wang P.L.,2009,Effect of relative humidity on barrier properties of polyvinyl alcohol films,Gaofengzi Cailiao Kexue Yu Gongcheng(Polymer Materials Science and Engineering),(8):61-63(陈默,王志伟,胡长鹰,王平利,2009,湿度对聚乙烯醇膜阻隔性能的影响,高分子材料科学与工程,(8):61-63)
Hu D.Y.,and Guo J.S.,2005,Application of microcapsule technology to the fabric finishing,Ranzheng Jishu(Textile Dyeing and Finishing Journal),27(12):66-68(胡大艳,郭建生,2005,微胶囊技术在织物整理上的应用,染整技术,27(12):66-68)
Huang L.,Qiu B.Y.,and Liu S.H.,2006,Development of microcapsule antibacterial reagent for fabrics,Sichou(Silk Monthly),3:26-29(黄玲,邱白玉,刘少华,2006,微胶囊织物抗菌剂的研制,丝绸,3:26-29)
Hui P.C.,Wang W.,Kan C.,Ng F.S.,Zhou C.,Wat E.,Zhang V.X.,Chan C.,Lau C.B.,and Leung P.,2013,Preparation and char-acterization of chitosan/sodium alginate(CSA)microcapsule containing Cortex Moutan,Colloids and Surfaces A:Physicochem.Eng.Aspects,434:95-101
Li M.,Wang R.,and Liu X.,2017,Preparation and in vitro release performance of geranium wilfordii maxim filled biodegrad-able microcapsules,Polymer Korea,41(3):404-412
Liao Y.L.,Luo S.L.,Zhang Y.Q.,Zhang Y.L.,Li H.Y.,and Liang X.Y.,2015,Introduction of PhabrOmeter-(R)system and its application,Zhongguo Xianjian(China Fiber Inspection),(13):84-86(廖银琳,罗胜利,张宇群,张玉莲,李红英,梁小焰,2015,PhabrOmeter-(R)织物评价系统简介及其应用探讨,中国纤检,(13):84-86)
Liu X.W.,Wang L.Q.,and Liao Z.S.,2017,Research progress of microencapsulation technology in food packaging,Baozhuang Gongcheng(Packaging Engineering),38(1):149-155(刘晓伟,王利强,廖祝胜,2017,微胶囊技术在食品包装中的研究进展,包装工程,38(1):149-155)
Wang A.Q.,Shen L.P.,and Tang Z.X.,2017,Preparation of lanvender microcapsules and its applications in cotton fabric,Zhenzhi Gongye(Knitting Industry),(2):47-50(王爱琼,沈兰萍,汤铸先,2017,薰衣草微胶囊的制备及在棉针织物上的应用,针织工业,(2):47-50)
Wang Y.J.,Ge F.Y.,Cai Z.S.,Jiang J.Y.,and Chen B.L.,2010,Preparation of the mosquito repellent micro-capsule and its ap-plication in the cotton knitted fabric,Zhenzhi Gongye(Knitting Industries),7:34-37(王玉娟,葛风燕,蔡再生,姜建英,陈炳良,2010,防蚊微胶囊的制备及在棉针织物上的应用,针织工业,7:34-37)
Xing S.,Sharp L.K.,and Touchette D.R.,2016,Weight loss drugs and lifestyle modification:perceptions among a diverse adult sample,Patient Educ.Couns.,100(3):592-597
Yin G.,Zhang N.W.,Zhu B.,Aming B.H.,Yan W.,Lian D.P.,Fan Q.,Liu C.,Du D.X.,Zhang D.D.,Zhang Z.,Zhang Y.K.,and Gong K.,2015,A comparison of roux-en-Y gastric bypass and laparoscopic sleeve gastrectomy for severe obesity,Zhongguo Weichuang Waike Zazhi(Chinese Journal of Minimally Invasive Surgery),15(6):487-491(尹刚,张能维,朱斌,阿民布和,闫巍,廉东坡,樊庆,刘晨,杜德晓,张东东,张振,张雁凯,宫轲,2015,腹腔镜Roux-en-Y胃旁路术与腹腔镜胃袖状切除术治疗肥胖病的对比研究,中国微创外科杂志,15(6):487-491)
Zhang W.,Li Q.J.,and Zhang J.F.,2015,Preparation and controlled release of microcapsules via layer-by-layer assembly,Fangzhi Xuebao(Journal of Textile Research),(3):58-62(张维,李秋瑾,张健飞,2015,层层组装微胶囊的制备及其缓释性能,纺织学报,(3):58-62)
Zhao X.,2015,Preparation of chitosan guanidine hydrochloride and application thereof in antimicrobial finishing of wool fabric,Fangzhi Xuebao(Journal of Textile Rese arch),(4):92-96(赵雪,2015,壳聚糖胍盐酸盐的制备及其在羊毛织物抗菌整理中的应用,纺织学报,(4):92-96)
Zorec B.,Préat V.,Miklavc?ic?D.,and Pav?elj N.,2013,Active enhancement methods for intra-and transdermal drug delivery:a review,Zdravni?ki Vestnik,82(5):339-356