柱前衍生-高效液相色谱法测定水中3种氟乙胺
|
摘要
<正>含氟低级脂肪胺是一种重要的化工原料,具有独特的理化性能和生物活性,广泛应用在医药、农药、染料等领域~([1])。但其毒性大、反应活性高,大量使用与排放会对生态环境造成不可忽视的影响。2-氟乙胺(FEA)是一种高效剧毒的有机氟杀虫农药,具有内吸收作用,有效期长且不易挥发[2];2,2-二氟乙胺(DFEA)常作为活性成分制备中的一种重要的中间体和合成原料,特别是在农药化学活
引文
[1]傅滨,李楠,梁晓梅,等.还原胺化反应的新进展[J].有机化学,2007,27(1):1-7.
[2]赵传奎.氟乙胺中毒的抢救体会[J].现代中西医结合杂志,1999,8(7):1152-1152.
[3]DONETTI A,CEREDA E,EZHAYA A,et al.N-(Fluoroethyl)(imidazolyl-phenyl)formamidines:The issue of the active species of mifentidine[J].Journal of Medicinal Chemistry,1989,32(5):957-961.
[4]DICKEY J B,TOWNE E B,BLOOM M S,et al.Fluorinated aminoanthraquinone dyes[J].Industrial&Engineering Chemistry,1956,48(2):209-213.
[5]徐卫国.三氟乙胺的制备与应用[J].浙江化工,2003,34(9):9-10.
[6]BLACK W C,BAYLY C I,DAVIS D E,et al.Trifluoroethylamines as amide isosteres in inhibitors of cathepsin K[J].Bioorganic&Medicinal Chemistry Letters,2005,15(21):4741-4744.
[7]POLLACK R M,KAYSER R H.Trifluoroethylamine-catalyzed isomerization ofβ,γ-unsaturated ketones.Nucleophitie catalysis via schiff base formation[J].Journal of the American Chemical Society,1976,98(14):4174-4181.
[8]付敏,赵卫红,苗辉,等.高效液相色谱法测定海水中游离态腐胺、精胺和亚精胺[J].分析化学,2010,38(10):1445-1449.
[9]SANTAGATI N A,BOUSQUET E,SPADARO A,et al.Analysis of aliphatic amines in air samples by HPLC with electrochemical detection[J].Journal of Pharmaceutical and Biomedical Analysis,2002,29(6):1105-1111.
[10]KAMAREI F,EBRAHIMZADEH H,YAMINI Y.Optimization of solvent bar microextraction combined with gas chromatography for the analysis of aliphatic amines in water samples[J].Journal of Hazardous Materials,2010,178(1/3):747-752.
[11]赵怀鑫,孙学军,孙志伟,等.EASC荧光标记和LC-APCI-MS检测环境水样中游离脂肪胺[J].高等学校化学学报,2009,30(4):675-681.
[12]李佐卿,谢东华,王宇,等.高效液相色谱荧光检测器快速测定水产品中的组胺[J].光谱实验室,2000,17(5):592-595.
[13]陈丹超,肖玲艳,陈有为,等.柱前衍生-高效液相色谱法测定红酒中小分子脂肪胺[J].理化检验-化学分册,2013,49(8):1008-1010.
[14]赵先恩,石运伟,陈向明,等.脂肪胺荧光衍生物的高效液相色谱分离及质谱鉴定[J].化学研究,2005,16(2):66-69.
[15]卜文,马亚杰,于泓.高效液相色谱/间接紫外检测法分离测定脂肪胺[J].分析测试学报,2014,33(2):203-207.
[16]郭龑茹,彭静.第13届离子色谱学术报告会[C].青岛:中国仪器仪表学会分析仪器分会,2010.
[17]NORIHISA K,KOSUKE K,SHOJI A.Method for preparation of fluoroalkylamines by amination of fluoroalkyl halides:JP2003137844[P].2003-03-14.
[18]HIROKAZU T,KEIICHI O.Process for producing fluorinated alkylamine compound:JP 20030183557[P].2003-03-18.
[2]赵传奎.氟乙胺中毒的抢救体会[J].现代中西医结合杂志,1999,8(7):1152-1152.
[3]DONETTI A,CEREDA E,EZHAYA A,et al.N-(Fluoroethyl)(imidazolyl-phenyl)formamidines:The issue of the active species of mifentidine[J].Journal of Medicinal Chemistry,1989,32(5):957-961.
[4]DICKEY J B,TOWNE E B,BLOOM M S,et al.Fluorinated aminoanthraquinone dyes[J].Industrial&Engineering Chemistry,1956,48(2):209-213.
[5]徐卫国.三氟乙胺的制备与应用[J].浙江化工,2003,34(9):9-10.
[6]BLACK W C,BAYLY C I,DAVIS D E,et al.Trifluoroethylamines as amide isosteres in inhibitors of cathepsin K[J].Bioorganic&Medicinal Chemistry Letters,2005,15(21):4741-4744.
[7]POLLACK R M,KAYSER R H.Trifluoroethylamine-catalyzed isomerization ofβ,γ-unsaturated ketones.Nucleophitie catalysis via schiff base formation[J].Journal of the American Chemical Society,1976,98(14):4174-4181.
[8]付敏,赵卫红,苗辉,等.高效液相色谱法测定海水中游离态腐胺、精胺和亚精胺[J].分析化学,2010,38(10):1445-1449.
[9]SANTAGATI N A,BOUSQUET E,SPADARO A,et al.Analysis of aliphatic amines in air samples by HPLC with electrochemical detection[J].Journal of Pharmaceutical and Biomedical Analysis,2002,29(6):1105-1111.
[10]KAMAREI F,EBRAHIMZADEH H,YAMINI Y.Optimization of solvent bar microextraction combined with gas chromatography for the analysis of aliphatic amines in water samples[J].Journal of Hazardous Materials,2010,178(1/3):747-752.
[11]赵怀鑫,孙学军,孙志伟,等.EASC荧光标记和LC-APCI-MS检测环境水样中游离脂肪胺[J].高等学校化学学报,2009,30(4):675-681.
[12]李佐卿,谢东华,王宇,等.高效液相色谱荧光检测器快速测定水产品中的组胺[J].光谱实验室,2000,17(5):592-595.
[13]陈丹超,肖玲艳,陈有为,等.柱前衍生-高效液相色谱法测定红酒中小分子脂肪胺[J].理化检验-化学分册,2013,49(8):1008-1010.
[14]赵先恩,石运伟,陈向明,等.脂肪胺荧光衍生物的高效液相色谱分离及质谱鉴定[J].化学研究,2005,16(2):66-69.
[15]卜文,马亚杰,于泓.高效液相色谱/间接紫外检测法分离测定脂肪胺[J].分析测试学报,2014,33(2):203-207.
[16]郭龑茹,彭静.第13届离子色谱学术报告会[C].青岛:中国仪器仪表学会分析仪器分会,2010.
[17]NORIHISA K,KOSUKE K,SHOJI A.Method for preparation of fluoroalkylamines by amination of fluoroalkyl halides:JP2003137844[P].2003-03-14.
[18]HIROKAZU T,KEIICHI O.Process for producing fluorinated alkylamine compound:JP 20030183557[P].2003-03-18.