农药产品中多种禁限用农药检测技术研究进展
摘要
本文主要介绍了国内外禁限用农药概况,分析了农药产品中禁限用农药超标的原因,例如违规使用高毒农药、盲目增加用药剂量及用药次数、复混农药成分复杂等,并总结了农药产品中多种禁限用农药检测技术研究进展。
引文
[1]孔志英,吴志凤,董记萍.浅议通过标签内容查找农药隐性成分[J].农药科学与管理,2014,35(11):16-18.
[2]洪华,张晓强,武中平,等.SPE-GC-MS快速定性定量杀虫剂产品中11种违禁添加菊酯类隐性成分[J].农药,2013,52(11):812-814.
[3]乔成奎,黄玉南,罗静,等.HPLC-MS/MS法检测农药产品中30种隐性成分[J].农药,2015,54(05):340-342+345.
[4]毕富春,吴国旭.浅谈农药隐性成分的定性分析[J].生物灾害科学,2015,38(04):354-357.
[5]陈书华,汪浩,张念洁,等.禁限用农药隐性添加的检测与风险分析研究[J].农药科学与管理,2016,37(04):25-30+35.
[6]李海燕,施慧娟,肖峥.农药杀虫剂中11种禁限用农药的同时检测[J].上海计量测试,2015,42(01):21-23.
[7]于峰,国明,贾科玲,等.建立HPLC-DAD-MS/MS指纹图谱快速分析农药隐性成分的方法[J].农药,2018,57(01):39-41+45.
[8]陈樟宝.经贸委农业部封杀高毒剧毒农药[N].21世纪经济报道,2003-03-07.
[9]简秋,朱光艳,郑尊涛.国际禁限用农药残留限量标准制定原则简析[J].农药科学与管理,2014,35(06):20-25.
[10]陈顺序.蔬菜农药残留超标的原因及防治措施[J].甘肃农业,2013,11(365):58-59
[11]Cunniff P official methods of Analysis of AOAC international 16th ed., 1995:Volume 1.
[12]钱立立.农药残留的快速检测和前处理技术的研究[D].合肥:中国科学技术大学,2007.
[13]Schenck F J et al. J. Assoc. Off. Anal.Chem. Int.,1994,74:1036-1040.
[14]仲维科,郝戬,樊耀波,等.食品农药残留分析进展[J].分析化学,2000,28(07):904-910.
[15]Muccio A D, Barbini D A, Generali T, et al. Cleanup of aqueo us acetone veg etable ext racts by solid matrix partition for py rethr oid residue determination by g as chr omato gr aphy——electron-captur e det ection[J]. J Chr omato gr A, 1997,765:39-49.
[16]Fer n-ndez M, Pic Y, MaNes J. Determination o f carbamate residues in fruits and vegetables by matr ix solid-phase dispersion and liquid chromato gr aphymass spectrometry[J].J Chromato g r A,2000, 871:43-56.
[17]郑永权.农药残留研究进展与展望[J].植物保护,2013,39(05):90-98.
[18]Lehotay S J, Eller K I.J. Assoc. Off. Anal.Chem. Int.,1995,78(03):821-833.
[19]Garcia A V, Alba R F, Aguera A. J. Assoc. Off. Anal.Chem. Int., 1995,78(03):867-873.
[20]Howard A L, Braue C, Taylor, J. Chromatogr.Sci.,1993,31(09):323-329.
[21]Nishikawa Y. Anal. Sci., 1991,7(04):567-572.
[22]Tsoutsi C, Konstantinou I, Hela D, et al. Screening method for organophosphorus insecticides and their metabolites in olive oil samples based on headspace solid-phase microextraction coupled with gas chromatography[J].Anal Chim Acta,2006,573/574:216-222.
[23]Cai L S, Gong S L, Chen M, et al. Vinyl crown ether as a novel radical crosslinked sol-gel SPME fiber for determination of organophosphorus pesticides in food samples[J]. Anal Chim Acta,2006, 559:89-96.
[24]Tomkins B A, Barnard A R. Determination of organochlorine pesticides in ground water using solid-phase microextraction follow ed by dual-column gas chromatography with electron-capture detection[J]. J Chromatogr A, 2002, 964:21-33.
[25]López F J, Pitarch E, Egea S, et al. Gas chromatographic determination of organochlorine and organophosphorus pesticides in human fluids using solid phase microextraction[J]. Anal Chim Acta, 2001,433:217-226.
[26]Hernández F, Pitarch E, Beltran J, et al. Headspace solid-phase microextraction in combination with gas chromatography and tandem mass spectrometry for the determination of organochlorine and organophosphorus pesticides in whole human blood[J]. J Chromatogr B, 2002,769:65-77.
[2]洪华,张晓强,武中平,等.SPE-GC-MS快速定性定量杀虫剂产品中11种违禁添加菊酯类隐性成分[J].农药,2013,52(11):812-814.
[3]乔成奎,黄玉南,罗静,等.HPLC-MS/MS法检测农药产品中30种隐性成分[J].农药,2015,54(05):340-342+345.
[4]毕富春,吴国旭.浅谈农药隐性成分的定性分析[J].生物灾害科学,2015,38(04):354-357.
[5]陈书华,汪浩,张念洁,等.禁限用农药隐性添加的检测与风险分析研究[J].农药科学与管理,2016,37(04):25-30+35.
[6]李海燕,施慧娟,肖峥.农药杀虫剂中11种禁限用农药的同时检测[J].上海计量测试,2015,42(01):21-23.
[7]于峰,国明,贾科玲,等.建立HPLC-DAD-MS/MS指纹图谱快速分析农药隐性成分的方法[J].农药,2018,57(01):39-41+45.
[8]陈樟宝.经贸委农业部封杀高毒剧毒农药[N].21世纪经济报道,2003-03-07.
[9]简秋,朱光艳,郑尊涛.国际禁限用农药残留限量标准制定原则简析[J].农药科学与管理,2014,35(06):20-25.
[10]陈顺序.蔬菜农药残留超标的原因及防治措施[J].甘肃农业,2013,11(365):58-59
[11]Cunniff P official methods of Analysis of AOAC international 16th ed., 1995:Volume 1.
[12]钱立立.农药残留的快速检测和前处理技术的研究[D].合肥:中国科学技术大学,2007.
[13]Schenck F J et al. J. Assoc. Off. Anal.Chem. Int.,1994,74:1036-1040.
[14]仲维科,郝戬,樊耀波,等.食品农药残留分析进展[J].分析化学,2000,28(07):904-910.
[15]Muccio A D, Barbini D A, Generali T, et al. Cleanup of aqueo us acetone veg etable ext racts by solid matrix partition for py rethr oid residue determination by g as chr omato gr aphy——electron-captur e det ection[J]. J Chr omato gr A, 1997,765:39-49.
[16]Fer n-ndez M, Pic Y, MaNes J. Determination o f carbamate residues in fruits and vegetables by matr ix solid-phase dispersion and liquid chromato gr aphymass spectrometry[J].J Chromato g r A,2000, 871:43-56.
[17]郑永权.农药残留研究进展与展望[J].植物保护,2013,39(05):90-98.
[18]Lehotay S J, Eller K I.J. Assoc. Off. Anal.Chem. Int.,1995,78(03):821-833.
[19]Garcia A V, Alba R F, Aguera A. J. Assoc. Off. Anal.Chem. Int., 1995,78(03):867-873.
[20]Howard A L, Braue C, Taylor, J. Chromatogr.Sci.,1993,31(09):323-329.
[21]Nishikawa Y. Anal. Sci., 1991,7(04):567-572.
[22]Tsoutsi C, Konstantinou I, Hela D, et al. Screening method for organophosphorus insecticides and their metabolites in olive oil samples based on headspace solid-phase microextraction coupled with gas chromatography[J].Anal Chim Acta,2006,573/574:216-222.
[23]Cai L S, Gong S L, Chen M, et al. Vinyl crown ether as a novel radical crosslinked sol-gel SPME fiber for determination of organophosphorus pesticides in food samples[J]. Anal Chim Acta,2006, 559:89-96.
[24]Tomkins B A, Barnard A R. Determination of organochlorine pesticides in ground water using solid-phase microextraction follow ed by dual-column gas chromatography with electron-capture detection[J]. J Chromatogr A, 2002, 964:21-33.
[25]López F J, Pitarch E, Egea S, et al. Gas chromatographic determination of organochlorine and organophosphorus pesticides in human fluids using solid phase microextraction[J]. Anal Chim Acta, 2001,433:217-226.
[26]Hernández F, Pitarch E, Beltran J, et al. Headspace solid-phase microextraction in combination with gas chromatography and tandem mass spectrometry for the determination of organochlorine and organophosphorus pesticides in whole human blood[J]. J Chromatogr B, 2002,769:65-77.