王不留行不同炮制工艺的优选
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摘要
目的:优选出王不留行的最佳炮制工艺。方法:测定王不留行不同炮制品的爆花率,通过高效液相色谱法,以十八烷基硅烷键合硅胶为填充剂,以甲醇为流动相A,0.3%磷酸溶液为流动相B,测定不同炮制品黄酮苷的含量,优选出王不留行最佳炮制工艺。结果:清炒法中火爆花率高,砂炒法中武火爆花率高。对比两组爆花率高的王不留行,清炒法的爆花率高,但是砂炒法完全爆花率高且减少一半炒制时间。两组质量对比中,黄酮苷:砂炒法中武火>清炒法中武火,水分:砂炒法中武火>清炒法中武火,浸出物:砂炒法中武火>清炒法中武火。结论:砂炒法中武火为最佳炮制工艺。
Objective:To optimize the processing technology of Vaccariae.Methods:We measured different popcorn rates of Vaccariae processed products were measured by HPLC,with octadecylsilane bonded silica as a filler and regard methanol as mobile phase A,0.3% phosphoric acid solution as mobile phase B to obtain flavonoid glycoside content determination of different processed products,in the end,the best processing technology of Vaccaria was selected.Results:Fried method popcorn rate and sand fried hot martial popcorn rate was high.Compared to the latter,fried method popcorn rate was high,but sand fried hot martial popcorn rate were high and it can reduce in the half of the frying time.In quality comparison of the two groups,flavonoid glycosides:fried sand Wuhuo Law>fried high heat Law,moisture:fried sand method Wuhuo>fried high heat Law,extract:fried sand Wuhuo Law>fried high heat Law.Conclusion:Fried sand was the best method in high heat processing technology.
Objective:To optimize the processing technology of Vaccariae.Methods:We measured different popcorn rates of Vaccariae processed products were measured by HPLC,with octadecylsilane bonded silica as a filler and regard methanol as mobile phase A,0.3% phosphoric acid solution as mobile phase B to obtain flavonoid glycoside content determination of different processed products,in the end,the best processing technology of Vaccaria was selected.Results:Fried method popcorn rate and sand fried hot martial popcorn rate was high.Compared to the latter,fried method popcorn rate was high,but sand fried hot martial popcorn rate were high and it can reduce in the half of the frying time.In quality comparison of the two groups,flavonoid glycosides:fried sand Wuhuo Law>fried high heat Law,moisture:fried sand method Wuhuo>fried high heat Law,extract:fried sand Wuhuo Law>fried high heat Law.Conclusion:Fried sand was the best method in high heat processing technology.
引文
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[3]崔国静,代珊珊,贺强.王不留行的炮制加工新技术[J].农村新技术,2011,29(12):42.
[4]李帆,梁敬钰.王不留行的研究进展[J].海峡药学,2007,19(3):1-4.
[5]魏薇.中药王不留行的研究进展[J].中国医药指南,2014,12(16):87-88.
[6]郑剑锋,王育红.中药王不留行的研究进展[J].电大理工,2012,34(2):9-10.
[7]牛彩琴,敬华娥,张团笑.王不留行对大鼠子宫平滑肌的影响[J].河南中医,2014,32(2):234-236.
[8]马丽萍,邱丽颖,冯磊,等.王不留行不同提取物抑制人微血管内皮细胞活性的研究[J].中成药,2013,35(11):2315-2319.
[9]贾屹峰,苗培.王不留行的概述与研究[J].畜牧与饲料科学,2012,33(3):32-34.
[10]蔡瑾瑾,陈璐.GC-MS分析王不留行、决明子、酸枣仁炒制前后脂肪油成分的变化[J].中国实验方剂学杂志,2017,23(15):31-34.
[11]郭长强,苏德民,王立春,等.王不留行的炮制技术[J].中药材,2000,23(5):301-303.
[12]李娜,马长华,刘冬,等.炒王不留行的化学成份分析[J].中国实验方剂学杂志,2013,19(10):73-75.
[13]孟贺,陈玉平,秦文杰,等.HPLC测定王不留行中王不留行黄酮苷的含量[J].中国中药杂志,2010,35(16):140.