溴代反应试剂在化工合成中的应用
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摘要
溴代反应被广泛应用于医药、液晶、OLED等化工合成领域,而溴代试剂是溴代反应的重要组成部分。本文就常用的溴代试剂在化工合成领域的应用做了概述分析,并对其发展前景进行了展望。
The bromine reaction has been widely used in Pharmaceutical, liquid crystal, OLED and other chemical synthesis fields. The bromine agent is an important part of the bromine reaction. In this paper, the commonly used brominated reagents are summarized and analyzed, and their development prospects are prospected.
The bromine reaction has been widely used in Pharmaceutical, liquid crystal, OLED and other chemical synthesis fields. The bromine agent is an important part of the bromine reaction. In this paper, the commonly used brominated reagents are summarized and analyzed, and their development prospects are prospected.
引文
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[2]李文燕,赵冬梅,熊绪琼,等.有机化学,2011,6:784.
[3]Kolvari E,Ghorbani-Choghamarani A,Salehi P,et al.Application of N-halo reagents in organic synthesis[J].JIran Chem Soc,2007,4(2):126-174.
[4]Stuk T L,Assink B K,Bates R C,et al.An efficient and cost-effective synthesis of pagoclone[J].Org Process Res Dev,2003,7(6):851-855.
[5]Ravi S,Mathew K M,Unny V K P,et al.A facile synthesis of racemic carboxyl 14 C-labeled phenylglycine under microwave irradiation[J].J Radioanal Nucl CH,2007,274(1):61-62.
[6]Jiang X F,Shen M H,Tang Y,et al.Chemoselective monobromination of alkanes promoted by unactivated Mn O2[J].Tetrahedron Lett,2005,46(3):487-489.
[7]Amati A,Dosualdo G,Zhao L H,et al.Catalytic processes of oxidation by hydrogen peroxide in the presence of Br2 or HBr Mechanism and synthetic applications[J].Org Process Res Dev,1998,2(4):261-269.
[8]WO2014/202528 A1,2014.
[9]Moretti F,Poisson G,Marsura A.Improved halogenation of methyl aromatics and methyl heteroaromatics:unexpected reactivity of tetrahalogeno-diphenylglycolurils[J].Heteroat Chem,2016,27(3):173-183.
[10]Chiou M S,Li H Y.Adsorption behavior of reactive dye inaqueous solution o n chemical cross-ling ked chitosan beads[J].Chemosphere,2003,50(8):1095-1096.
[11]居洁,李郁锦,高建荣,等.甲苯氧化溴化反应研究[J].浙江工业大学学报,2011,39(4):369-371.
[12]Moretti F,Poisson G,Marsura A.Improved halogenation ofmethyl aromatics and methyl heteroaromatics:unexpected reactivity of tetrahalogeno-diphenylglycolurils[J].Heteroat Chem,2016,27(3):173-183.
[13]Cantillo D,Frutos O D,Rincon J A,et al.Chem Inform Abstract:A scalable procedure for light-induced benzylicbrominations in continuous flow[J].J Org Chem,2015,79(1):223.
[14]Hong T,Qiu Y,Matsumoto M,et al.Nat Commun,2017,8:1359-1361.
[15]Gur D,Pierantoni M,Elool Dov N,et al.Crys Grow Des,2016,16:4975-4980.
[16]Awwadi F F,Hodali H A.J Mol Struct,2018,1154:373-381.
[17]Xu Y,Xie Z,Zhang H,et al.Cryst Eng Comm,2016,18:6824-6829.
[18]Vitorica-Yrezabal I J,Sullivan R A,Purver S L,et al.Cryst Eng Comm,2011,13:3189-3196.
[19]Gur D,Pierantoni M,Elool Dov N,et al.Cryst Grow Des,2016,16:4975-4980.
[20]Cruickshank D L,Hendon C H,Verbeek M J,et al.Cryst Eng Comm,2016,18:3456-3461.
[21]Vitorica-Yrezabal I J,Sullivan R A,Purver S L,et al.Cryst Eng Comm,2011,13:3189-3196.
[22]David A J,Cruz-Cabeza,Bernstein J.Chem Rev,2013,114:2170-2191.
[23]张月,刘亚军.NBS对芳香醚类化合物选择性溴代研究[J].辽宁化工,2012,41(10):1006-1009.
[24]Cantillo D,Frutos O D,Rincon J A,et al.Chem Inform Abstract:A scalable procedure for light-induced benzylicbrominations in continuous flow[J].J.Org.Chem.,2015,79(1):223.
[25]Geboes Y,De Proft F,Herrebout W A.The Journal of Physical Chemistry A,2017.
[26]Awwadi F F,Willett R D,Twamley B,et al.Cryst Growth&Des,2015,15:3746-3754.
[27]Chen Zhanguo,Xia Wei,Liu De'e,et al.Journal of the Chinese Chemical Society,2016,63(2):158-164.