纳米材料理化性能分析方法综述
|
摘要
纳米材料的理化性能包括粒度、形貌、结构、表面界面、成分等,这些理化性能对纳米材料的化学、电学、磁学、机械等性能有重要的影响。准确分析测定这些性能参数对纳米材料的研究有着重大的意义。本文对纳米材料现有的一些理化性能分析方法进行了综述,同时提出了作者的一点意见和建议。
The physicochemical properties of nanomaterials include particle size,morphology,structure,surface and interface,composition and others.They have important influences on chemical properties,electrical properties,magnetic properties and mechanical properties of nanomaterials.Their accurate measurement have important implications for nanomaterial research.This paper reviews the existing physicochemical analysis methods for nanomaterials,and gives some opinions and suggestions.
The physicochemical properties of nanomaterials include particle size,morphology,structure,surface and interface,composition and others.They have important influences on chemical properties,electrical properties,magnetic properties and mechanical properties of nanomaterials.Their accurate measurement have important implications for nanomaterial research.This paper reviews the existing physicochemical analysis methods for nanomaterials,and gives some opinions and suggestions.
引文
[1]中国国家标准化管理委员会.GBT 19619-2004纳米材料术语[S].北京:中国标准出版社,2004:3.
[2]朱世东,周根树,蔡锐,等.纳米材料国内外研究进展Ⅰ—纳米材料的结构、特异效应与性能[J].热处理技术与装备,2010,31(3):1.
[3]钱志勇,耿志挺,崔建国,等.纳米颗粒的粒度对PMMA基复合材料光学性能的影响[J].高分子材料科学与工程,2003,19(2):161.
[4]李成仁.SiC粒度对Al2O3-SiC纳米复合材料结构和机械性能的影响[J].稀有金属材料与工程,2000,1(10):289.
[5]吴建鹏,曹丽云,贺海燕,等.纳米材料的颗粒尺寸分析方法[J].热加工工艺,2007,36(12):72.
[6]Akbari1B,Pirhadi Tavandashti M,Zandrahimi M.Agglomeration assesment of Nano-sized alumina powders[J].Iranian Journal of Materials Science&Engineering,2011,8(2):48.
[7]Varennea F,Bottonc J,Merleta C,et al.Standardization and validation of a protocol of size measurements by dynamic light scattering for monodispersed stable nanomaterial characterization[J].Colloids and Surfaces A:Physicochemical and Engineering Aspects, 2015,486:124.
[8]Mast J,Verleysen E,Temmerman D P.Advanced Transmission Electron Microscopy[M].Switzerland:Springer International Publishing,2015:249.
[9]Chamieh J,Cottet H.Colloid and Interface Science in Pharmaceutical Research and Development[M].The Netherlands:Elsevier B.V,2014:173.
[10]王书运.纳米颗粒的测量与表征[J].山东师范大学学报,2005,20(2):45.
[11]李洪涛,李正民.微纳米粉体粒径大小及分布测定的研究进展[J].化学工程与装备,2008,(11):108.
[12]江发伟,姬景超,程宏飞,等.库尔特Multisizer3粒度分析仪测试条件研究[J].湖南科技大学学报,2015,30(4):103.
[13]熊丽媛.扫描电子显微镜在粒度分析中的应用[J].汽车零部件,2012,7:80.
[14]胡继林,胡传跃,田修营,等.激光粒度仪测定超细碳化硅粉体粒度研究[J].无机盐工业,2016,48(3):66.
[15]刘亚青,刘玉敏,胡永琪.激光粒度仪测定近纳米氢氧化铝粒径的研究[J].现代化工,2015,35(3):175.
[16]陈哲敏,胡朋兵,孟庆强.动态光散射及电子显微镜纳米颗粒测量方法的比较研究[J].光散射学报,2015,27(1):54.
[17]娄本浊.CS-QT-TPP纳米颗粒的动态光散射分析[J].光散射学报,2015,27(3):271.
[18]谢圣中,王柏春,许向阳.纳米氧化铈颗粒的粒度分析研究[J].金属材料与冶金工程,2007,35(6):3.
[19]吴立新,陈芳玉.现代扫描电镜的发展及其在材料科学中的应用[J].武钢技术,2005,43(6):37.
[20]周莉,吴海艳,臧树良.电子显微技术在纳米材料研究中的应用[J].矿冶,2010,19(1):53.
[21]方克明,邹兴,苏继灵.纳米材料的透射电镜表征[J].现代科学仪器,2003,(2):15.
[22]Egerton R F.Physical Principles of Electron Microscopy[M].Switzerland:Springer International Publishing,2016:55.
[23]万牡华,欧阳健明.STM、AFM、SEM和TEM对溶液中纳米微粒形貌和粒度分布的检测[J].人工晶体学报,2007,36(6):1422.
[24]高金堂,王宏刚,毛绍兰.纳米材料的结构分析[J].分析测试技术与仪器,2000,6(2):70.
[25]Gorelik T.Electron diffraction tomography for structure analysis of nanomaterials[J].Acta Cryst,2014,70:367.
[26]Shi H L,Zhang G L,Zou B,et al.A Method for structure analysis of nanomaterials by electron diffraction:phase identification and unit cell determination[J].Microscopy Research and Technique,2013,76(6):641.
[27]陆金生.X射线衍射技术在纳米材料中的应用[J].现代科学仪器,2003,(2):34.
[28]黄惠忠,刘忠范,杨延莲等.纳米材料分析[M].北京:化学工业出版社,2003:208.
[29]Baer D R.Application of surface analysis methods tonanomaterials:summary of ISO/TC 201technical report:ISO 14187:2011-surfacechemical analysis-characterization of nanomaterials[J].Surface and Interface Analysis,2012,44(9):1305.
[30]Baer D R,Engelhard M H,Johnson G E,et al.Surface characterization of nanomaterials and nanoparticles:Important needs and challenging opportunities[J].Journal of Vacuum Science and Technology,2013,17(3):163.
[31]贾双珠,李长安.X射线光电子能谱在新型催化材料表征中的应用[J].分析试验室,2016,35(7):862
[32]郭沁林.X射线光电子能谱[J].物理,2007,36(5):405.
[33]陈轩,陈玉安,徐幸梓,等.碳氮纳米结构材料的Raman和XPS分析[J].功能材料,2012,(2):137.
[34]吕品,张绍成,唐祯安.对痕量甲醛气体敏感的SnO2-NiO纳米材料的X射线光电子谱研究[J].辽宁大学学报,2016,43(1):32.
[35]张录平,李晖,刘亚平.俄歇电子能谱仪在材料分析中的应用[J].分析仪器,2009,(4):14.
[2]朱世东,周根树,蔡锐,等.纳米材料国内外研究进展Ⅰ—纳米材料的结构、特异效应与性能[J].热处理技术与装备,2010,31(3):1.
[3]钱志勇,耿志挺,崔建国,等.纳米颗粒的粒度对PMMA基复合材料光学性能的影响[J].高分子材料科学与工程,2003,19(2):161.
[4]李成仁.SiC粒度对Al2O3-SiC纳米复合材料结构和机械性能的影响[J].稀有金属材料与工程,2000,1(10):289.
[5]吴建鹏,曹丽云,贺海燕,等.纳米材料的颗粒尺寸分析方法[J].热加工工艺,2007,36(12):72.
[6]Akbari1B,Pirhadi Tavandashti M,Zandrahimi M.Agglomeration assesment of Nano-sized alumina powders[J].Iranian Journal of Materials Science&Engineering,2011,8(2):48.
[7]Varennea F,Bottonc J,Merleta C,et al.Standardization and validation of a protocol of size measurements by dynamic light scattering for monodispersed stable nanomaterial characterization[J].Colloids and Surfaces A:Physicochemical and Engineering Aspects, 2015,486:124.
[8]Mast J,Verleysen E,Temmerman D P.Advanced Transmission Electron Microscopy[M].Switzerland:Springer International Publishing,2015:249.
[9]Chamieh J,Cottet H.Colloid and Interface Science in Pharmaceutical Research and Development[M].The Netherlands:Elsevier B.V,2014:173.
[10]王书运.纳米颗粒的测量与表征[J].山东师范大学学报,2005,20(2):45.
[11]李洪涛,李正民.微纳米粉体粒径大小及分布测定的研究进展[J].化学工程与装备,2008,(11):108.
[12]江发伟,姬景超,程宏飞,等.库尔特Multisizer3粒度分析仪测试条件研究[J].湖南科技大学学报,2015,30(4):103.
[13]熊丽媛.扫描电子显微镜在粒度分析中的应用[J].汽车零部件,2012,7:80.
[14]胡继林,胡传跃,田修营,等.激光粒度仪测定超细碳化硅粉体粒度研究[J].无机盐工业,2016,48(3):66.
[15]刘亚青,刘玉敏,胡永琪.激光粒度仪测定近纳米氢氧化铝粒径的研究[J].现代化工,2015,35(3):175.
[16]陈哲敏,胡朋兵,孟庆强.动态光散射及电子显微镜纳米颗粒测量方法的比较研究[J].光散射学报,2015,27(1):54.
[17]娄本浊.CS-QT-TPP纳米颗粒的动态光散射分析[J].光散射学报,2015,27(3):271.
[18]谢圣中,王柏春,许向阳.纳米氧化铈颗粒的粒度分析研究[J].金属材料与冶金工程,2007,35(6):3.
[19]吴立新,陈芳玉.现代扫描电镜的发展及其在材料科学中的应用[J].武钢技术,2005,43(6):37.
[20]周莉,吴海艳,臧树良.电子显微技术在纳米材料研究中的应用[J].矿冶,2010,19(1):53.
[21]方克明,邹兴,苏继灵.纳米材料的透射电镜表征[J].现代科学仪器,2003,(2):15.
[22]Egerton R F.Physical Principles of Electron Microscopy[M].Switzerland:Springer International Publishing,2016:55.
[23]万牡华,欧阳健明.STM、AFM、SEM和TEM对溶液中纳米微粒形貌和粒度分布的检测[J].人工晶体学报,2007,36(6):1422.
[24]高金堂,王宏刚,毛绍兰.纳米材料的结构分析[J].分析测试技术与仪器,2000,6(2):70.
[25]Gorelik T.Electron diffraction tomography for structure analysis of nanomaterials[J].Acta Cryst,2014,70:367.
[26]Shi H L,Zhang G L,Zou B,et al.A Method for structure analysis of nanomaterials by electron diffraction:phase identification and unit cell determination[J].Microscopy Research and Technique,2013,76(6):641.
[27]陆金生.X射线衍射技术在纳米材料中的应用[J].现代科学仪器,2003,(2):34.
[28]黄惠忠,刘忠范,杨延莲等.纳米材料分析[M].北京:化学工业出版社,2003:208.
[29]Baer D R.Application of surface analysis methods tonanomaterials:summary of ISO/TC 201technical report:ISO 14187:2011-surfacechemical analysis-characterization of nanomaterials[J].Surface and Interface Analysis,2012,44(9):1305.
[30]Baer D R,Engelhard M H,Johnson G E,et al.Surface characterization of nanomaterials and nanoparticles:Important needs and challenging opportunities[J].Journal of Vacuum Science and Technology,2013,17(3):163.
[31]贾双珠,李长安.X射线光电子能谱在新型催化材料表征中的应用[J].分析试验室,2016,35(7):862
[32]郭沁林.X射线光电子能谱[J].物理,2007,36(5):405.
[33]陈轩,陈玉安,徐幸梓,等.碳氮纳米结构材料的Raman和XPS分析[J].功能材料,2012,(2):137.
[34]吕品,张绍成,唐祯安.对痕量甲醛气体敏感的SnO2-NiO纳米材料的X射线光电子谱研究[J].辽宁大学学报,2016,43(1):32.
[35]张录平,李晖,刘亚平.俄歇电子能谱仪在材料分析中的应用[J].分析仪器,2009,(4):14.