液相微萃取技术的发展与应用
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摘要
液相微萃取集萃取、分离、净化、富集为一体,操作简单、绿色环保、萃取效率高,成功改善了传统样品前处理方法的不足。随着该技术的不断发展,根据不同的样品和分析物逐步衍生出了种类不同、操作各异的微萃取模式,现已广泛应用在环境分析、药物分析、食品分析、临床医学等领域,具有极大的发展潜力。
Liquid-phase microextraction integrates extraction, separation, purification and concentration. It improves the deficiency of traditional sample preparation methods successfully with its traits, such as easy operation, green protection and high extraction efficiency. With the continuous development of technology, LPME is derived different types and operating mode of microextraction gradually according to different samples and analyses. It has a great development potential and is widely used in environmental, drugs analysis, food analysis, clinical medicine and other fields now.
Liquid-phase microextraction integrates extraction, separation, purification and concentration. It improves the deficiency of traditional sample preparation methods successfully with its traits, such as easy operation, green protection and high extraction efficiency. With the continuous development of technology, LPME is derived different types and operating mode of microextraction gradually according to different samples and analyses. It has a great development potential and is widely used in environmental, drugs analysis, food analysis, clinical medicine and other fields now.
引文
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[3]苗佩佩,丁健桦,张席席,等.中空纤维顶空液相微萃取-气相色谱法测定胶黏剂中正己烷[J].分析试验室,2014,33(11):1296-1300.
[4]向虹霖,何海霞,苗佩佩,等.中空纤维液相微萃取-液相色谱法测定淀粉样品中丁烯二酸异构体[J].食品科技,2016(9):283-288.
[5]Hu S,Song Y H,Bai X H,et al.Derivatization and solidification of floating dispersive liquid-phase microextraction for the analysis of kanamycin in wastewater and soil by HPLC with fluorescence detection[J].CLEAN-Soil,Air,Water,2014,42(3):364-370.
[6]Pedersen-Bjergaard S,Rasmussen K E.Liquid-liquid-liquid microextraction for sample preparation of biological fluids prior to capillary electrophoresis[J].Analytical chemistry,1999,71(14):2650-2656.
[7]刁春鹏,时军波,苑金鹏,等.中空纤维液相微萃取技术及其应用进展[J].光谱实验室,2008,25(2):158-163.
[8]谭小旺,魏瑞萍,宋燕西,等.三相中空纤维膜液相微萃取-高效液相色谱法测定水中痕量双酚A[J].分析化学,2012,40(9):1409-1414.
[9]Rezaee M,Assadi Y,Hosseini M R M,et al.Determination of organic compounds in water using dispersive liquid-liquid microextraction[J].Journal of Chromatography A,2006,1116(1):1-9.
[10]Prosen H.Applications of Liquid-Phase Microextraction in the Sample Preparation of Environmental Solid Samples[J].Molecules,2014,19(5):6776-6808.
[11]Hadi H,Makahleh A,Saad B.Hollow fiber liquid-phase microextraction combined with high performance liquid chromatography for the determination of trace mitiglinide in biological fluids[J].Journal of Chromatography B,2012,895-896:131-136.
[2]Jeannot M A,Cantwell F F.Solvent microextraction into a single drop[J].Analytical chemistry,1996,68(13):2236-2240.
[3]苗佩佩,丁健桦,张席席,等.中空纤维顶空液相微萃取-气相色谱法测定胶黏剂中正己烷[J].分析试验室,2014,33(11):1296-1300.
[4]向虹霖,何海霞,苗佩佩,等.中空纤维液相微萃取-液相色谱法测定淀粉样品中丁烯二酸异构体[J].食品科技,2016(9):283-288.
[5]Hu S,Song Y H,Bai X H,et al.Derivatization and solidification of floating dispersive liquid-phase microextraction for the analysis of kanamycin in wastewater and soil by HPLC with fluorescence detection[J].CLEAN-Soil,Air,Water,2014,42(3):364-370.
[6]Pedersen-Bjergaard S,Rasmussen K E.Liquid-liquid-liquid microextraction for sample preparation of biological fluids prior to capillary electrophoresis[J].Analytical chemistry,1999,71(14):2650-2656.
[7]刁春鹏,时军波,苑金鹏,等.中空纤维液相微萃取技术及其应用进展[J].光谱实验室,2008,25(2):158-163.
[8]谭小旺,魏瑞萍,宋燕西,等.三相中空纤维膜液相微萃取-高效液相色谱法测定水中痕量双酚A[J].分析化学,2012,40(9):1409-1414.
[9]Rezaee M,Assadi Y,Hosseini M R M,et al.Determination of organic compounds in water using dispersive liquid-liquid microextraction[J].Journal of Chromatography A,2006,1116(1):1-9.
[10]Prosen H.Applications of Liquid-Phase Microextraction in the Sample Preparation of Environmental Solid Samples[J].Molecules,2014,19(5):6776-6808.
[11]Hadi H,Makahleh A,Saad B.Hollow fiber liquid-phase microextraction combined with high performance liquid chromatography for the determination of trace mitiglinide in biological fluids[J].Journal of Chromatography B,2012,895-896:131-136.