艾叶与艾炭显微特征对比研究
|
摘要
目的为完善艾炭质量控制标准提供实验依据。方法首次采用显微鉴别方法对不同来源和批次(自制)艾炭进行炒炭前后的对比研究。结果艾叶炒炭前后显微特征有变化,其中T形毛和单列性非腺毛无显著差别,而炒炭后草酸钙簇晶少见,鞋底形腺毛未见。结论本项研究不仅首次为艾炭质量控制标准提供了显微鉴别依据,而且为炭化与灰化的本质区别以及中药炮制中的炒炭存性理论提供了实验依据。
Objective To provide experimental evidence for improving the quality control standard of Artemisiae argyi Folium. Methods For the first time, microscopic identification method was used to compare the characteristics between Artemisia argyi Folium and its charred product from different sources and batches of homemade before and after charcoal frying. Results The microscopic characteristics of Artemisia argyi Folium were changed before and after charcoal frying, no significant difference were found between T trichomes and single row non glandular, but the clusters of calcium oxalate crystals were rare after charcoal frying, No glandular hairs on sole. Conclusion This study not only provides the microscopic identification basis for the quality control standard of Charred Artemisiae argyi Folium for the first time, It also provides the experimental basis for the essential difference between carbonization and ashing, together with the theory of maintaining medicinal properties after carbonisatus in Chinese medicine processing.
Objective To provide experimental evidence for improving the quality control standard of Artemisiae argyi Folium. Methods For the first time, microscopic identification method was used to compare the characteristics between Artemisia argyi Folium and its charred product from different sources and batches of homemade before and after charcoal frying. Results The microscopic characteristics of Artemisia argyi Folium were changed before and after charcoal frying, no significant difference were found between T trichomes and single row non glandular, but the clusters of calcium oxalate crystals were rare after charcoal frying, No glandular hairs on sole. Conclusion This study not only provides the microscopic identification basis for the quality control standard of Charred Artemisiae argyi Folium for the first time, It also provides the experimental basis for the essential difference between carbonization and ashing, together with the theory of maintaining medicinal properties after carbonisatus in Chinese medicine processing.
引文
[1]国家药典委员会.中华人民共和国药典[M].北京:中国医药出版社,2015.
[2]张元,康利平,郭兰萍,等.艾叶的本草考证和应用研究进展[J].上海针灸杂志,2017,36(3):245-255.
[3]赵志鸿,侯迎迎,郑立运,等.艾叶乙酸乙酯提取物对HBV的抑制作用[J].郑州大学学报(医学版),2013,48(6):783-785.
[4]努尔比耶·奥布力喀斯木,热娜·卡斯木,杨璐,等.艾叶挥发油化学成分分析和抗真菌活性的研究[J].新疆医科大学学报,2017,40(9):1195-1202.
[5]周英栋,费新应.艾叶的药理作用研究[J].湖北中医杂志,2010,32(11):75-76.
[6]朱超超.艾叶的临床应用[J].中国中医药现代远程教育,2013,11(6):94-97.
[7]Zhang WJ,You CX,Yang K,et al.Bioactivity of essential oilof Artemisia argyi Levl.et Vant.and its main compounds against Lasioderma serricorne[J].Oleo Sci,2014,63(8):829-837.
[8]董爱君,刘华臣,吴昭.艾叶挥发油及其热裂解物成分分析[J].香料香精化妆品,2017,45(3):5-12.
[9]王显著,段石顽.艾叶及其炮制品挥发油的研究[J].陕西中医,2008,29(8):1069-1070.
[10]何正有,张艳红,魏冬,等.三种不同提取方法制备的艾叶挥发油化学成分分析[J].中国医药生物技术,2008,3(4):284-288.
[11]徐新建,宋海,韩玉琦,等.艾叶挥发油化学成分的气相色谱-质谱联用分析[J].时珍国医国药,2007,28(11):2657-2658.
[12]王远敏,吴红梅,杨烨,等.艾叶UPLC指纹图谱[J].中国实验方剂学杂志,2015,21(13):50-52.
[13]周倩,孙立立,江波,等.RP-HPLC法同时测定艾叶及其炮制品中棕矢车菊素和异泽兰黄素的含量[J].中国药房,2013,24(47):4464-4466.
[14]Lv JL,Duan JA,Shen B,et al.Caffeic acid esters from Artemisia argyi and their antioxidant activities[J].Chem Nat Compd,2013,49(1):8-11.
[15]李真真,吕洁丽,张来宾,等.艾叶的化学成分及药理作用研究进展[J].国际药学研究杂志,2016,43(6):1059-1066.
[2]张元,康利平,郭兰萍,等.艾叶的本草考证和应用研究进展[J].上海针灸杂志,2017,36(3):245-255.
[3]赵志鸿,侯迎迎,郑立运,等.艾叶乙酸乙酯提取物对HBV的抑制作用[J].郑州大学学报(医学版),2013,48(6):783-785.
[4]努尔比耶·奥布力喀斯木,热娜·卡斯木,杨璐,等.艾叶挥发油化学成分分析和抗真菌活性的研究[J].新疆医科大学学报,2017,40(9):1195-1202.
[5]周英栋,费新应.艾叶的药理作用研究[J].湖北中医杂志,2010,32(11):75-76.
[6]朱超超.艾叶的临床应用[J].中国中医药现代远程教育,2013,11(6):94-97.
[7]Zhang WJ,You CX,Yang K,et al.Bioactivity of essential oilof Artemisia argyi Levl.et Vant.and its main compounds against Lasioderma serricorne[J].Oleo Sci,2014,63(8):829-837.
[8]董爱君,刘华臣,吴昭.艾叶挥发油及其热裂解物成分分析[J].香料香精化妆品,2017,45(3):5-12.
[9]王显著,段石顽.艾叶及其炮制品挥发油的研究[J].陕西中医,2008,29(8):1069-1070.
[10]何正有,张艳红,魏冬,等.三种不同提取方法制备的艾叶挥发油化学成分分析[J].中国医药生物技术,2008,3(4):284-288.
[11]徐新建,宋海,韩玉琦,等.艾叶挥发油化学成分的气相色谱-质谱联用分析[J].时珍国医国药,2007,28(11):2657-2658.
[12]王远敏,吴红梅,杨烨,等.艾叶UPLC指纹图谱[J].中国实验方剂学杂志,2015,21(13):50-52.
[13]周倩,孙立立,江波,等.RP-HPLC法同时测定艾叶及其炮制品中棕矢车菊素和异泽兰黄素的含量[J].中国药房,2013,24(47):4464-4466.
[14]Lv JL,Duan JA,Shen B,et al.Caffeic acid esters from Artemisia argyi and their antioxidant activities[J].Chem Nat Compd,2013,49(1):8-11.
[15]李真真,吕洁丽,张来宾,等.艾叶的化学成分及药理作用研究进展[J].国际药学研究杂志,2016,43(6):1059-1066.