苯并[a]芘含量测定的前处理方法研究进展
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摘要
回顾了近年来研究人员在苯并[a]芘检测过程中的前处理方法的研究概况,对比了各方法的优缺点。苯并[a]芘检测过程中的前处理方法主要有液液萃取、索氏提取、固相萃取、凝胶渗透色谱净化、超声萃取、微波辅助萃取等,检测涉及的样品主要为水、油、土壤及各种食品等。每种前处理方法都有一定的适用范围,在实际检测过程中可根据样品的性状以及苯并[a]芘在该样品中的存在形态选择合适的检测方法。
The paper reviewed pretreatment methods during benzo( a) pyrene test process,and analyzed advantages and disadvantages of each method.Pretreatments mainly included liquid-liquid extraction,soxhlet extraction,solid-phase extraction,gel permeation chromatography ultrasonic extraction,and microwave-assisted extraction.The main samples were water,oil,soil,and food etc.Each pretreatment had a certain scope of application,which can be selected according to the sample's property and benzo( a)pyrene exist state in the sample.
The paper reviewed pretreatment methods during benzo( a) pyrene test process,and analyzed advantages and disadvantages of each method.Pretreatments mainly included liquid-liquid extraction,soxhlet extraction,solid-phase extraction,gel permeation chromatography ultrasonic extraction,and microwave-assisted extraction.The main samples were water,oil,soil,and food etc.Each pretreatment had a certain scope of application,which can be selected according to the sample's property and benzo( a)pyrene exist state in the sample.
引文
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[24]王春华,洪抒,董丽波,等.高效液相色谱测定沥青烟雾中3,4-苯并芘[J].环境与职业医学,2007,24(4):443-445.
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[26]贾涛.液相色谱法检测饲料用油中苯并芘的方法研究[J].饲料广角,2014(13):37-39.
[27]杨占南,彭全材,罗世琼,等.贵阳市油炸食品中苯并芘的测定及其安全评价[J].食品科学,2008,29(10):449-452.
[28]苏旭,王英杰,张玉贞,等.空气中3,4-苯并芘的微波萃取-高效液相色谱测定法[J].中国工业医学杂志,2009,22(1):64-65.
[29]王浩,杨红梅,郭启雷,等.高效液相色谱-串联质谱法同时测定植物油中苯并芘与黄曲霉毒素B1,B2,G1,G2[J].分析测试学报,2014,33(8):911-916.
[30]何智慧,练文柳,蒋腊梅,等.GPC-气相色谱质谱法测定卷烟主流烟气中的苯并[a]芘[J].湖南文理学院学报(自然科学版),2009,21(1):42-46.
[2]PEKEY B,KARAKAS D,AYBERK S.Atmospheric deposition of polycyclic aromatic hydrocarbons to Izmit Bay,Turkey[J].Chemosphere,2007,67(3):537-547.
[3]GALVEZ-PERAHA M,SHI Z Q,CHEN J,et al.Oral benzo[a]pyrene in Cyp1al bl(-/-)double-knockout mice:Microarray analysis during squamous cell carcinoma formation in prenuptial gland duct[J].International journal of cancer,2013,132(9):2065-2075.
[4]樊大江,彭景.烹调方法与致癌、致突变作用[J].中国烹饪研究,2000,17(2):24-25.
[5]张根生.食品中有害化学物质的危害与检测[M].北京:中国计量出版社,2006:24-25.
[6]刘艳琴,王浩,杨红梅.凝胶渗透色谱-高效液相色谱法测定植物油中苯并芘[J].食品科技,2013,38(1):327-329.
[7]张哲.固相萃取技术在环境监测领域中的应用及研究进展[J].现代科学仪器,2013(3):33-36.
[8]黄鸾玉,黎小正,秦振发.固相萃取/高效液相色谱荧光法测定水产品中苯并芘[J].分析试验室,2009,28(12):63-65.
[9]徐国涛,李淑忠,王悦.气相色谱-质谱法测定高炉炮泥结合剂中的苯并芘含量[J].耐火材料,2010,44(1):71-72.
[10]胡加文,李天宝,王春利,等.固相萃取-液相色谱法测定方便面中苯并芘[J].化学分析计量,2014,23(3):25-27.
[11]刘玉兰,张小涛,赵欢欢.液相色谱-串联质谱法检测食用油脂中苯并芘[J].粮油加工,2012(10):45-47.
[12]赵欢欢,刘玉兰,张小涛.吸附法脱除芝麻油中苯并芘及脱色效果研究[J].粮油食品科技,2013,21(4):29-33.
[13]CEJPEK K,HAJSLOVA J,KOEOUREK V,et al.Changes in PAH levels during production of rapeseed oil[J].Food additives and contaminants,1998,15(5):563-574.
[14]董广彬,李鹏,姜俊.食用植物油中苯并(a)芘检测结果分析[J].粮油加工,2009(7):67-68.
[15]薛鸣,张虹.食品中多环芳烃残留分析前处理方法的研究[J].食品与发酵工业,2008,34(7):141-145.
[16]齐邦峰,张会成,陈立仁,等.萃取-紫外分光光度法测定微晶蜡中3,4-苯并芘含量[J].分析测试技术与仪器,2003,9(3):169-172.
[17]季雨,彭美春,张华,等.柴油机排气微粒中可溶有机成分及苯并(a)芘的实验测定[J].内燃机学报,1990,8(3):203-208.
[18]张朝青,邢雁,余雷.高效液相色谱法测定水源中苯并芘的方法研究[J].广东化工,2014,41(8):151-152,146.
[19]杨洪彪,刘秋欣.稻谷中苯并(a)芘的测定[J].食品科学,2000,21(9):45-47.
[20]段家修,许斯都,宋崇林,等.柴油机微粒和苯并(a)芘排放特性的研究[J].内燃机学报,1997,15(2):192-198.
[21]杨文珍,张新文,贾瑞宝.饮用水中痕量苯并[a]芘的测定方法研究[J].山东化工,1998(5):53.
[22]田树盛.Blue Rayon人造纤维对多环芳烃的富集作用[J].分析化学,2002,30(11):1404.
[23]贾瑞宝,孙韶华.C18键合相吸附剂富集水中痕量苯并[a]芘[J].色谱,1998,16(5):462.
[24]王春华,洪抒,董丽波,等.高效液相色谱测定沥青烟雾中3,4-苯并芘[J].环境与职业医学,2007,24(4):443-445.
[25]武晓剑,李琼,费玠,等.高效液相色谱法测定反应香精中的3,4-苯并芘[J].食品科技,2008(4):192-194.
[26]贾涛.液相色谱法检测饲料用油中苯并芘的方法研究[J].饲料广角,2014(13):37-39.
[27]杨占南,彭全材,罗世琼,等.贵阳市油炸食品中苯并芘的测定及其安全评价[J].食品科学,2008,29(10):449-452.
[28]苏旭,王英杰,张玉贞,等.空气中3,4-苯并芘的微波萃取-高效液相色谱测定法[J].中国工业医学杂志,2009,22(1):64-65.
[29]王浩,杨红梅,郭启雷,等.高效液相色谱-串联质谱法同时测定植物油中苯并芘与黄曲霉毒素B1,B2,G1,G2[J].分析测试学报,2014,33(8):911-916.
[30]何智慧,练文柳,蒋腊梅,等.GPC-气相色谱质谱法测定卷烟主流烟气中的苯并[a]芘[J].湖南文理学院学报(自然科学版),2009,21(1):42-46.