都匀楼梯草正丁醇和石油醚部位化学成分的研究
|
摘要
采用柱色谱分离技术,在都匀楼梯草(Elatostema duyunens)正丁醇和石油醚部位中分离得到18个化合物,通过MS和NMR数据分析,鉴定出10个化合物,分别为:槲皮素(1)、槲皮素-3-O-β-D-半乳糖苷(2)、槲皮素-3-O-β-D-葡萄糖苷(3)、山奈酚(4)、山奈酚-3-O-β-D-葡萄糖苷(5)、齐墩果酸(6)、β-谷甾醇(7)、熊果酸(8)、豆甾醇(9)和正二十五烷(10)。
Column chromatographic technique was used for the isolation and purification of the chemical constituents of n-butanol and petroleum ether parts from Elatostema duyunens.18 compounds were separated,and 10 compounds were identified by MS and NMR data analysis.They are quereetin(1),quercetin-3-O-β-D-galactoside(2),quercetin-3-O-β-D-glucoside(3),kaempferol(4),kaempferol 3-Oβ-D-glucoside(5),oleanic acid(6),β-sitosterol(7),ursolic acid(8),stigmasterol(9),and npentacosane(10),respectively.
Column chromatographic technique was used for the isolation and purification of the chemical constituents of n-butanol and petroleum ether parts from Elatostema duyunens.18 compounds were separated,and 10 compounds were identified by MS and NMR data analysis.They are quereetin(1),quercetin-3-O-β-D-galactoside(2),quercetin-3-O-β-D-glucoside(3),kaempferol(4),kaempferol 3-Oβ-D-glucoside(5),oleanic acid(6),β-sitosterol(7),ursolic acid(8),stigmasterol(9),and npentacosane(10),respectively.
引文
[1]王文采,韦毅刚.都匀楼梯草—贵州荨麻科一新种[J].广西植物,2008,28(1):1-3.
[2]徐宗海,吴洪新,魏孝义,等.达乌里胡枝子中黄酮类化学成分的研究[J].西北植物学报,2010,30(7):1485-1489.
[3]陈龙,杜力军,丁怡,等.罗布麻花化学成分研究[J].中国中药杂志,2005,30(17):1340-1342.
[4]张晓,彭树林,王明奎,等.聚花过路黄化学成分的研究[J].药学学报,1999,34(11):835.
[5]江纪武,肖庆祥.植物药有效成分手册[M].北京:人民卫生出版社,1986:877.
[6]高丽梅,吴立军,黄健,等.板栗花的化学成分[J].沈阳药科大学学报,2010,27(7):544-562
[7]刘有强,孔令义.Studies on flavonoids of Rhododend ronmolle[J].中草药,2009,40(2):199-201.
[8]周丽光,冯雪松,黄开毅,等.关东丁香化学成分研究[J].中药材,2008,31(5):679.
[9]张援虎,何丽,关焕玉,等.追风伞中黄酮类成分的研究[J].中国中药杂志,2010,35(14):1824-1826.
[10]袁经权,杨俊山,缪剑华.Studies on flavonoids of Eupatorium odoratum L.[J].中药材,2007,30(6):657-660.
[11]Luo X D,Wu S H,Ma B Y,et al.The chemical constituents of Amoora yuuanensis[J].Acta Botanica Sinica,2001,43(4):426-430.
[12]梁光义,武孔云,徐任生,等.尖叶清风藤化学成分的研究[J].药学学报,1995,30(5):367-371.
[13]康文艺,张百让,许启泰,等.帽蕊木化学成分研究[J].中药材,2006,29(6):557-560.
[14]王奇志,梁敬钰.吴茱萸化学成分研究[J].药学学报,2004,39(8):605-608.
[15]冯长根,李琼.香青兰化学成分研究[J].中成药,2006,28(1):94-98.
[16]封士兰,何兰,王敏.百合花化学成分研究[J].中国中药杂志,1994,19:611-612.
[17]刘东,鞠建华,杨俊山.狭叶崖爬藤化学成分的研究[J].中草药,2003,34(1):4-6.
[2]徐宗海,吴洪新,魏孝义,等.达乌里胡枝子中黄酮类化学成分的研究[J].西北植物学报,2010,30(7):1485-1489.
[3]陈龙,杜力军,丁怡,等.罗布麻花化学成分研究[J].中国中药杂志,2005,30(17):1340-1342.
[4]张晓,彭树林,王明奎,等.聚花过路黄化学成分的研究[J].药学学报,1999,34(11):835.
[5]江纪武,肖庆祥.植物药有效成分手册[M].北京:人民卫生出版社,1986:877.
[6]高丽梅,吴立军,黄健,等.板栗花的化学成分[J].沈阳药科大学学报,2010,27(7):544-562
[7]刘有强,孔令义.Studies on flavonoids of Rhododend ronmolle[J].中草药,2009,40(2):199-201.
[8]周丽光,冯雪松,黄开毅,等.关东丁香化学成分研究[J].中药材,2008,31(5):679.
[9]张援虎,何丽,关焕玉,等.追风伞中黄酮类成分的研究[J].中国中药杂志,2010,35(14):1824-1826.
[10]袁经权,杨俊山,缪剑华.Studies on flavonoids of Eupatorium odoratum L.[J].中药材,2007,30(6):657-660.
[11]Luo X D,Wu S H,Ma B Y,et al.The chemical constituents of Amoora yuuanensis[J].Acta Botanica Sinica,2001,43(4):426-430.
[12]梁光义,武孔云,徐任生,等.尖叶清风藤化学成分的研究[J].药学学报,1995,30(5):367-371.
[13]康文艺,张百让,许启泰,等.帽蕊木化学成分研究[J].中药材,2006,29(6):557-560.
[14]王奇志,梁敬钰.吴茱萸化学成分研究[J].药学学报,2004,39(8):605-608.
[15]冯长根,李琼.香青兰化学成分研究[J].中成药,2006,28(1):94-98.
[16]封士兰,何兰,王敏.百合花化学成分研究[J].中国中药杂志,1994,19:611-612.
[17]刘东,鞠建华,杨俊山.狭叶崖爬藤化学成分的研究[J].中草药,2003,34(1):4-6.