氰化物分析研究进展
|
摘要
介绍氰化物常用的场外分析和现场检测方法,对实验室(场外)常用分析方法如化学滴定法、分光光度法、色谱法、波谱法等以及现场快速检测方法如目视比色法、分光光度计法等进行了综述,并结合实际需求,总结了不同方法的特点,展望了氰化物检测方法的未来发展趋势。
The common methods of off-site analytical and field detection for cyanide were introduced. Laboratory common analytical methods were summarized such as chemical titration, spectrophotometry, chromatography, spectroscopy, etc., and on-site rapid detection methods, such as visual colorimetry, spectrophotometer method,etc. combined with the actual demand and their characteristics were summaried. The development trends of cyanide detection methods were predicted.
The common methods of off-site analytical and field detection for cyanide were introduced. Laboratory common analytical methods were summarized such as chemical titration, spectrophotometry, chromatography, spectroscopy, etc., and on-site rapid detection methods, such as visual colorimetry, spectrophotometer method,etc. combined with the actual demand and their characteristics were summaried. The development trends of cyanide detection methods were predicted.
引文
[1]马晓年.氰化物的危害及检测方法概述[J].健康必读杂质,2012(5):499-500.
[2]胡德荣.认识化学武器[J].首都师范大学学报:自然科学版,2014,35(6):45-50.
[3]梁洁.氰化物泄露事故应急处置对策[J].广东化工,2012,39(8):375-378.
[4]解放日报.“基地”欲向美下“毒”手[N/OL].http://newspaper.jfdaily.com/jfrb/html/2010-12-23/content_480065.htm
[5]董黎红,王惠亭,王云昌.水质中“有毒”与“无毒”氰化物的检测方法探讨[J].河南科学,2009,27(10):1 216-1 218.
[6]黄森乐,刘清华.氰化物的检测方法[J].广东化工,2014,41(17):183-185.
[7]韩康芹,张云肖,冯敏英.土壤中有害氰化物的检测方法[J].安徽农业科学,2014,42(3):729-730.
[8]史永辉.废水中氰化物测定方法探讨[J].新疆环境保护,2009(4):43-45.
[9]祝旭初,程军蕊.异烟酸-巴比妥酸分光光度法测定水中氰化物的改进[J].中国给水排水,2014,30(18):136-139.
[10]李惠兰,李左丹,邵恩裕.紫外分光光度法测定水中氰化物[J]南京师院学报:自然科学版,1980(1):24-29.
[11]刘大银,陈贤猛.钙离子络合-紫外分光光度法测定水中氰化物[J].环境工程,1994,12(1):37-40.
[12]武建军,池新民.荧光分光光度法测定痕量氰化物的研究及其应用[J].中国公共卫生学报,1989,8(3):174-176.
[13]向双全,张志刚.原子吸收石墨炉法测定白酒中的氰化物[J]酿酒科技,2015(3):127-129.
[14]邸玉敏,朱军,常靖,等.氰化物检测方法研究进展[J].理化检验:化学分册,2011,47(12):1 491-1 494.
[15]刘晓铮.油田化工污水中总氰化物的检测[J].油气田环境保护,2013,43(2):58-60.
[16]赵治兵,王瑞,刘晓燕,等.顶空-气相色谱法测定底泥中氰化物含量[J].贵州农业科学,2015,43(4):68-70.
[17]崔战友,钟其顶,李国辉,等.酒醅中氰化物的测定方法研究[J].酿酒科技,2015(5):101-105.
[18]Guojie Liu,Junting Liu,Kenji Hara,et al.Rapid determination of cyanide in human plasma and urine by gas chromatographymass spectrometry with two-step derivatization[J].Journal of Chromatography B,2009(887):3 054-3 058.
[19]Hye-In Kang,Ho-Sang Shin.Ultra-sensitive determination of cyanide in surface water by gas chromatography-tandem mass spectrometry after derivatization with 2-(dimethylamino)ethanethiol[J].Analytica Chimica Acta,2014(852):168-173.
[20]龙素群,钟志京,辉永庆,等.水中氰化物的安培检测-离子色谱测定[J].环境与健康杂志,2009,26(8):719-720.
[21]Wu Wenlin,Xiao Quanwei,Zhang Ping,et al.Rapid measurement of free cyainde in liquor by ion chromatography with pulsed amperometric detection[J].Food Chemistry,2015(172):681-684
[22]孟梁,申贵隽,张强.金属配位剂衍生-高效液相色谱法测定粮食及白酒中的游离氰化物[J].分析科学学报,2009,25(5)587-589.
[23]孟梁.液相微萃取-毛细管电泳联用技术在毒物和毒品分析中的应用研究[D].大连:大连大学,2010.
[24]Zhang Qiyang,Maddukuri Naveen,Gong Maojun.A direct and rapid method to determinecy anideinurine by capillaryelectrophoresis[J].Journal of Chromatography A,2015(1414):158-162.
[25]Avik Mazumder,Ajeet Kumar,Devendra K Dubey.High resolution 19F{1H}nuclear magnetic resonance spectroscopy and liquid chromatography-solid phase extraction-offline 1Hnuclear magnetic resonance spectroscopy for conclusive detection and identification of cyanide in water samples[J].Journal of Chromatography A,2013(1284):88-99.
[26]朱东方,白静,曲春浩,等.水中氰化物应急监测方法研究[J].应用化工,2013,42(10):1 920-1 922.
[27]苏雷.水环境中应急监测研究[J].农业论坛,2015(10):205-206.
[28]杨伟群,管月清.便携式多参数水质检测仪测定水样中的氰化物、氟化物、氨氮和硝酸盐[J].化学试剂,2014,36(5):446-448.
[29]Aguilar M,Farran A.Capillary electrophoretic determination of cyanide leachingsolutions from automobile catalytic converters[J].J Chromatogr A,1997(1-2):397-402.
[30]Ellerbee A K,Phillips S T,Siegel A C,et al.Quantifying colorimetric assays in paper-based microfluidicdevices by measuring the transmission of light through paper[J].Anal.Chem,2009(20):8 447-8 452.
[31]胡明燕,车明秀,刘睿,等.白酒中氰化物含量定性检测方法的研究[J].酿酒科技,2014(10):105-108.
[32]赵露.快速检测水中氰化物-苦味酸试纸法[J].水质分析与检测,2008(5):67-68.
[33]刘奇侠.应用于现场快速检测水中污染物的新材料研究[D].上海:华东理工大学,2012.
[34]陈超,王红勇,高志贤.污染食品中氰化物的快速检测方法[J].中国卫生检验杂质,2010,20(1):34-36.
[35]王静斌,白莉,李树华,等.水中氰化物突发性污染事故应急监测方法研究[J].环境污染治理技术与设备,2003,4(12):79-81.
[36]Lee A Greenawalda,Jay L Snyderb,Nicole L Fryc,et al.Development of a cobinamide-based end-of-service-life indicatorfor detection of hydrogen cyanide gas[J].Sensors and Actuators B:Chemical,2015(221):379-385.
[37]Jalal Isaad,Ahmida El Achari,Fouad Malek.Bio-polymer starch thin film sensors for low concentration detection of cyanide anions in water[J].Dyes and Pigments,2013(97):134-140.
[38]Hongda Li,Bao Li,Longyi Jin,et al.A rapid responsive and highly selective probe for cyanide in the aqueous.Environment[J].Tetrahedron,2011(67):7 348-7 351.
[39]Christine,Mannel-Croise,Felix Zelder.Complex samples cyanide detection with immobilized corrinoids[J].Appl Mater Interfaces,2012(4):725-729.
[40]Archana A Biradar,Ankush V Biradar,Tiffany Sun,et al.Bicinchoninic acid-based colorimetric chemosensor for detection oflow concentrations of cyanide[J].Sensors and Actuators B:Chemical,2016(222):112-119.
[40]高敬.等离激元增强拉曼光谱技术在化学战剂及其相关化合物检测中的应用研究[D].北京:军事医学科学院,2014.
[2]胡德荣.认识化学武器[J].首都师范大学学报:自然科学版,2014,35(6):45-50.
[3]梁洁.氰化物泄露事故应急处置对策[J].广东化工,2012,39(8):375-378.
[4]解放日报.“基地”欲向美下“毒”手[N/OL].http://newspaper.jfdaily.com/jfrb/html/2010-12-23/content_480065.htm
[5]董黎红,王惠亭,王云昌.水质中“有毒”与“无毒”氰化物的检测方法探讨[J].河南科学,2009,27(10):1 216-1 218.
[6]黄森乐,刘清华.氰化物的检测方法[J].广东化工,2014,41(17):183-185.
[7]韩康芹,张云肖,冯敏英.土壤中有害氰化物的检测方法[J].安徽农业科学,2014,42(3):729-730.
[8]史永辉.废水中氰化物测定方法探讨[J].新疆环境保护,2009(4):43-45.
[9]祝旭初,程军蕊.异烟酸-巴比妥酸分光光度法测定水中氰化物的改进[J].中国给水排水,2014,30(18):136-139.
[10]李惠兰,李左丹,邵恩裕.紫外分光光度法测定水中氰化物[J]南京师院学报:自然科学版,1980(1):24-29.
[11]刘大银,陈贤猛.钙离子络合-紫外分光光度法测定水中氰化物[J].环境工程,1994,12(1):37-40.
[12]武建军,池新民.荧光分光光度法测定痕量氰化物的研究及其应用[J].中国公共卫生学报,1989,8(3):174-176.
[13]向双全,张志刚.原子吸收石墨炉法测定白酒中的氰化物[J]酿酒科技,2015(3):127-129.
[14]邸玉敏,朱军,常靖,等.氰化物检测方法研究进展[J].理化检验:化学分册,2011,47(12):1 491-1 494.
[15]刘晓铮.油田化工污水中总氰化物的检测[J].油气田环境保护,2013,43(2):58-60.
[16]赵治兵,王瑞,刘晓燕,等.顶空-气相色谱法测定底泥中氰化物含量[J].贵州农业科学,2015,43(4):68-70.
[17]崔战友,钟其顶,李国辉,等.酒醅中氰化物的测定方法研究[J].酿酒科技,2015(5):101-105.
[18]Guojie Liu,Junting Liu,Kenji Hara,et al.Rapid determination of cyanide in human plasma and urine by gas chromatographymass spectrometry with two-step derivatization[J].Journal of Chromatography B,2009(887):3 054-3 058.
[19]Hye-In Kang,Ho-Sang Shin.Ultra-sensitive determination of cyanide in surface water by gas chromatography-tandem mass spectrometry after derivatization with 2-(dimethylamino)ethanethiol[J].Analytica Chimica Acta,2014(852):168-173.
[20]龙素群,钟志京,辉永庆,等.水中氰化物的安培检测-离子色谱测定[J].环境与健康杂志,2009,26(8):719-720.
[21]Wu Wenlin,Xiao Quanwei,Zhang Ping,et al.Rapid measurement of free cyainde in liquor by ion chromatography with pulsed amperometric detection[J].Food Chemistry,2015(172):681-684
[22]孟梁,申贵隽,张强.金属配位剂衍生-高效液相色谱法测定粮食及白酒中的游离氰化物[J].分析科学学报,2009,25(5)587-589.
[23]孟梁.液相微萃取-毛细管电泳联用技术在毒物和毒品分析中的应用研究[D].大连:大连大学,2010.
[24]Zhang Qiyang,Maddukuri Naveen,Gong Maojun.A direct and rapid method to determinecy anideinurine by capillaryelectrophoresis[J].Journal of Chromatography A,2015(1414):158-162.
[25]Avik Mazumder,Ajeet Kumar,Devendra K Dubey.High resolution 19F{1H}nuclear magnetic resonance spectroscopy and liquid chromatography-solid phase extraction-offline 1Hnuclear magnetic resonance spectroscopy for conclusive detection and identification of cyanide in water samples[J].Journal of Chromatography A,2013(1284):88-99.
[26]朱东方,白静,曲春浩,等.水中氰化物应急监测方法研究[J].应用化工,2013,42(10):1 920-1 922.
[27]苏雷.水环境中应急监测研究[J].农业论坛,2015(10):205-206.
[28]杨伟群,管月清.便携式多参数水质检测仪测定水样中的氰化物、氟化物、氨氮和硝酸盐[J].化学试剂,2014,36(5):446-448.
[29]Aguilar M,Farran A.Capillary electrophoretic determination of cyanide leachingsolutions from automobile catalytic converters[J].J Chromatogr A,1997(1-2):397-402.
[30]Ellerbee A K,Phillips S T,Siegel A C,et al.Quantifying colorimetric assays in paper-based microfluidicdevices by measuring the transmission of light through paper[J].Anal.Chem,2009(20):8 447-8 452.
[31]胡明燕,车明秀,刘睿,等.白酒中氰化物含量定性检测方法的研究[J].酿酒科技,2014(10):105-108.
[32]赵露.快速检测水中氰化物-苦味酸试纸法[J].水质分析与检测,2008(5):67-68.
[33]刘奇侠.应用于现场快速检测水中污染物的新材料研究[D].上海:华东理工大学,2012.
[34]陈超,王红勇,高志贤.污染食品中氰化物的快速检测方法[J].中国卫生检验杂质,2010,20(1):34-36.
[35]王静斌,白莉,李树华,等.水中氰化物突发性污染事故应急监测方法研究[J].环境污染治理技术与设备,2003,4(12):79-81.
[36]Lee A Greenawalda,Jay L Snyderb,Nicole L Fryc,et al.Development of a cobinamide-based end-of-service-life indicatorfor detection of hydrogen cyanide gas[J].Sensors and Actuators B:Chemical,2015(221):379-385.
[37]Jalal Isaad,Ahmida El Achari,Fouad Malek.Bio-polymer starch thin film sensors for low concentration detection of cyanide anions in water[J].Dyes and Pigments,2013(97):134-140.
[38]Hongda Li,Bao Li,Longyi Jin,et al.A rapid responsive and highly selective probe for cyanide in the aqueous.Environment[J].Tetrahedron,2011(67):7 348-7 351.
[39]Christine,Mannel-Croise,Felix Zelder.Complex samples cyanide detection with immobilized corrinoids[J].Appl Mater Interfaces,2012(4):725-729.
[40]Archana A Biradar,Ankush V Biradar,Tiffany Sun,et al.Bicinchoninic acid-based colorimetric chemosensor for detection oflow concentrations of cyanide[J].Sensors and Actuators B:Chemical,2016(222):112-119.
[40]高敬.等离激元增强拉曼光谱技术在化学战剂及其相关化合物检测中的应用研究[D].北京:军事医学科学院,2014.