显微结构与相图
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摘要
讨论了陶瓷学科相图与显微结构的关系,显微结构分析的可信性,同一系统具有多种不同画法的相图以及应用相图的限制等问题;同时指出,完整、准确的显微结构分析结果是建立相平衡图的关键依据。
The relationship between phase diagram and microstructure,the credibility of microstructure analysis,the problem that the phase diagram of one system has different drawing methods and the limitation of phase diagram application in ceramics were discussed. At the same time,it was pointed out that the complete and accurate results of microstructure analysis were the key to the establishment of a phase equilibrium diagram.
The relationship between phase diagram and microstructure,the credibility of microstructure analysis,the problem that the phase diagram of one system has different drawing methods and the limitation of phase diagram application in ceramics were discussed. At the same time,it was pointed out that the complete and accurate results of microstructure analysis were the key to the establishment of a phase equilibrium diagram.
引文
[1]БЕЛЯНКИНД.С,ЛАБИНВ В,ТОРОПОВН А.Физико-химические системы силикатной технологии[M].МоскваГос:Издат Литерпо Строи Матер,1954.
[2]OSBORN E F.Phase diagrams and refractories[J].Bull Am Ceram Soc,1977,60(7):654-659.
[3]MUAN A,OSBORN E F.Phase equilibria and refractories[J].Bull Am Ceram Soc,1962,45(7):450-455.
[4]FOSTER W R.Contribution to the Interpretation of phase diagram[J].JACS,1951,34(5):151-160.
[5]ANDERSEN O,BOWEN N L.The binary system Mg O-Si O2[J].Am J Sci,1914,37:487-500.
[6]BOWEN N L,GREIG J W.The System Al2O3-SiO2[J].J Am Ceram Soc,1924,7(4):229-254.
[7]BOWEN N L.Petrology and silica technology[J].Bull Am Ceram Soc,1943,26(9):285-301.
[8]HALL F P,INSLEY H.A compilation of phase-rule diagrams of interest to the ceramist and silicate technologist[J].JACS,1933,16(10):463-566.
[9]INSLEY H,VAN FRECHETTE D.Microscopy of ceramics and cements[M].New York:Academic Press Inc,1955.
[10]LEVIN E M,MCMURDIE H F,HALL F P.Phase diagrams for ceramists[M].Columbus:The American Ceramic Society,1956.
[11]高振昕.国外学者关于莫来石问题的研究和争论[J].耐火材料情报,1963(7-8):9-18.
[12]高振昕.Al2O3-SiO2系相平衡的研究和争论[J].硅酸盐学报,1981,9(2):197-217.
[13]БУДНИКОВ П П,ЛИТВАКОВСКИЙ А А.Исследование на Al2O3-SiO2-ZrO2 системе[J].Доклады Академии Науки,СССР,1956,106(2):267-270.
[14]ЛИТВАКОВСКИЙ А А.Стойкость Новых о неупоров[J].Стекло и Керамика,1956(11):11-15.
[15]CEVALES G.Neue untersuchungen in system Al2O3-ZrO2-SiO2[J].Ber Deut Keram Gesel,1975(10):319-321.
[16]高振昕.ZrO2-Al2O3-SiO2系的转熔反应[J].硅酸盐学报,1983,11(3):380-383+391-392.
[17]高振昕,黄振武,梁兰芳.Al2O3-ZrO2系共晶组成研究[J].硅酸盐学报,2000,28(3):291-293.
[18]高振昕,卫晓辉,黄振武,等.ZrO2-莫来石共晶组成研究[J].硅酸盐学报,2000,28(3):288-290.
[19]高振昕.ZrO2-3Al2O3·2SiO2-Al2O3系相关系和相变[J].硅酸盐学报,1988,16(3):280-288.
[20]АДЫЛОВ Г Т,МАНСУРОВА Э П,СИГАЛОВ Л М.Фазовые соотношения и миклоструктура плавленных образцов в системе Al2O3-ZrO2-муллит[J].Огнеупоры,1994(6):19-22.
[21]ORDAN’YAN S S,GUDOVSKIKH P S,POZHIDAEVA O V.Refining the phase diagram of the system 3Al2O3·2SiO2-ZrO2[J].Russ J Appl Chem,2001,74(8):1390-1391.
[22]高振昕.MgO-Al2O3-ZrO2系相关系辩析[J].耐火材料,2017,51(1):68-72.
[23]郁国城.碱性耐火材料理论基础[M].上海:上海科技出版社,1982.
[24]沈继耀,袁启明.相图及其应用实例(Ⅰ)概论[J].硅酸盐通报,1987(5):63-69.
[25]FLORKE O W.Quartz,cristobalite and tridymite[J].Silikattech,1961(12):304-305.
[26]BECHTA S V,KRUSHINOV E V,ALMJASHEV V I,et al.Phase diagram of the ZrO2-FeO system[J].J Nucl Mater,2006,348(1-2):114-121.
[27]SAENKO I,ILATOVSKAIA M,SAVINYKH G,et al.Experimental investigation of phase relations and thermodynamic properties in the Zr O2-TiO2system[J].J Am Ceram Soc,2018,101(1):386-399.
[2]OSBORN E F.Phase diagrams and refractories[J].Bull Am Ceram Soc,1977,60(7):654-659.
[3]MUAN A,OSBORN E F.Phase equilibria and refractories[J].Bull Am Ceram Soc,1962,45(7):450-455.
[4]FOSTER W R.Contribution to the Interpretation of phase diagram[J].JACS,1951,34(5):151-160.
[5]ANDERSEN O,BOWEN N L.The binary system Mg O-Si O2[J].Am J Sci,1914,37:487-500.
[6]BOWEN N L,GREIG J W.The System Al2O3-SiO2[J].J Am Ceram Soc,1924,7(4):229-254.
[7]BOWEN N L.Petrology and silica technology[J].Bull Am Ceram Soc,1943,26(9):285-301.
[8]HALL F P,INSLEY H.A compilation of phase-rule diagrams of interest to the ceramist and silicate technologist[J].JACS,1933,16(10):463-566.
[9]INSLEY H,VAN FRECHETTE D.Microscopy of ceramics and cements[M].New York:Academic Press Inc,1955.
[10]LEVIN E M,MCMURDIE H F,HALL F P.Phase diagrams for ceramists[M].Columbus:The American Ceramic Society,1956.
[11]高振昕.国外学者关于莫来石问题的研究和争论[J].耐火材料情报,1963(7-8):9-18.
[12]高振昕.Al2O3-SiO2系相平衡的研究和争论[J].硅酸盐学报,1981,9(2):197-217.
[13]БУДНИКОВ П П,ЛИТВАКОВСКИЙ А А.Исследование на Al2O3-SiO2-ZrO2 системе[J].Доклады Академии Науки,СССР,1956,106(2):267-270.
[14]ЛИТВАКОВСКИЙ А А.Стойкость Новых о неупоров[J].Стекло и Керамика,1956(11):11-15.
[15]CEVALES G.Neue untersuchungen in system Al2O3-ZrO2-SiO2[J].Ber Deut Keram Gesel,1975(10):319-321.
[16]高振昕.ZrO2-Al2O3-SiO2系的转熔反应[J].硅酸盐学报,1983,11(3):380-383+391-392.
[17]高振昕,黄振武,梁兰芳.Al2O3-ZrO2系共晶组成研究[J].硅酸盐学报,2000,28(3):291-293.
[18]高振昕,卫晓辉,黄振武,等.ZrO2-莫来石共晶组成研究[J].硅酸盐学报,2000,28(3):288-290.
[19]高振昕.ZrO2-3Al2O3·2SiO2-Al2O3系相关系和相变[J].硅酸盐学报,1988,16(3):280-288.
[20]АДЫЛОВ Г Т,МАНСУРОВА Э П,СИГАЛОВ Л М.Фазовые соотношения и миклоструктура плавленных образцов в системе Al2O3-ZrO2-муллит[J].Огнеупоры,1994(6):19-22.
[21]ORDAN’YAN S S,GUDOVSKIKH P S,POZHIDAEVA O V.Refining the phase diagram of the system 3Al2O3·2SiO2-ZrO2[J].Russ J Appl Chem,2001,74(8):1390-1391.
[22]高振昕.MgO-Al2O3-ZrO2系相关系辩析[J].耐火材料,2017,51(1):68-72.
[23]郁国城.碱性耐火材料理论基础[M].上海:上海科技出版社,1982.
[24]沈继耀,袁启明.相图及其应用实例(Ⅰ)概论[J].硅酸盐通报,1987(5):63-69.
[25]FLORKE O W.Quartz,cristobalite and tridymite[J].Silikattech,1961(12):304-305.
[26]BECHTA S V,KRUSHINOV E V,ALMJASHEV V I,et al.Phase diagram of the ZrO2-FeO system[J].J Nucl Mater,2006,348(1-2):114-121.
[27]SAENKO I,ILATOVSKAIA M,SAVINYKH G,et al.Experimental investigation of phase relations and thermodynamic properties in the Zr O2-TiO2system[J].J Am Ceram Soc,2018,101(1):386-399.