页岩气实验测试技术进展
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摘要
页岩气是指赋存于具有生烃能力的泥质页岩及页岩等地层中,以吸附和游离状态存在的非常规天然气;具有自身产生、自身吸附储存成藏、隐蔽聚集等特点~([1])。20世纪70年代末,页岩气在北美地区成功开发,成为油气勘查的一个新的领域。目前对页岩气的储量评估与产气能力评价主要集中在页岩气藏的岩性成分、成因来源、赋存形式、成藏特征、成藏条件、页岩气含量等方面~([2])。而这些研究需要准确测定页岩的岩石学、含气量和有机地球化学等相关参数。通过对页岩的测试分析,得到含气量、渗透率、孔隙度、有机碳含量、岩石干酪根成熟度等数据,这些数据的分析,对于页岩的勘查与开发有着重要的作用。
Shale gas refers to the unconventional natural gas that exists in the shale in the form of adsorption and dissociation. This kind of natural gas that occurs in mud shale and shale with hydrocarbon generation capacity is characterized by self-generation and self-storage, adsorption and accumulation, and hidden accumulation [1].Since the United States began large-scale development in the late 1970 s, it has been successfully developed in North America and become a new field for oil and gas exploration. Currently, evaluation of shale gas reserve and productivity mainly focuses on lithologic composition of the gas reservoir, origin, occurrence form, accumulation characteristic, accumulation condition, shale gas content and so on [2]. And these studies need to accurately determine the lithology, shale gas content, organic geochemistry and correlation parameters. Through analysis of shale, the gas content, permeability, porosity, organic carbon content, kerogen maturity of rocks have been obtained, which play a major role in shale exploration and development.
Shale gas refers to the unconventional natural gas that exists in the shale in the form of adsorption and dissociation. This kind of natural gas that occurs in mud shale and shale with hydrocarbon generation capacity is characterized by self-generation and self-storage, adsorption and accumulation, and hidden accumulation [1].Since the United States began large-scale development in the late 1970 s, it has been successfully developed in North America and become a new field for oil and gas exploration. Currently, evaluation of shale gas reserve and productivity mainly focuses on lithologic composition of the gas reservoir, origin, occurrence form, accumulation characteristic, accumulation condition, shale gas content and so on [2]. And these studies need to accurately determine the lithology, shale gas content, organic geochemistry and correlation parameters. Through analysis of shale, the gas content, permeability, porosity, organic carbon content, kerogen maturity of rocks have been obtained, which play a major role in shale exploration and development.
引文
[1]聂海宽,张金川.页岩气储层类型和特征研究:以四川盆地及周缘下古生界为例[J].石油实验地质,2011,33(3):19~22.
[2]帅琴,黄瑞成,高强,徐生瑞,邱海鸥,汤志勇.页岩气实验测试技术现状与研究进展[J].岩矿测试,2012,30(6):931~938.
[3]腾吉文,刘有山.中国页岩气成藏和潜在产能与环境的污染分析[J].中国地质,2013,13(1):1~11.
[4]RONALD J H,DANIEL M J,JOHN ZIMBERGE,et al Oil and gas geochemistry and petroleum systems of the Fort Worth Basin[J].AAPG Bulletin,2007,91(4):445~473.
[5]张金川,聂海宽,徐波,等.四川盆地页岩气成藏地质条件[J].天然气工业,2008,28(2):151~126.
[6]张金川,金之钧,袁明生.页岩气成藏机理和分布[J].天然气工业,2004,24(7):15~18.
[7]姜呈馥,王香增,张丽霞,万永平,雷裕红,孙建博,郭超.鄂尔多斯盆地东南延长组长7段陆相页岩气地质特征及勘查潜力评价[J].中国地质,2013,40(6):1884~1885.
[8]曾胜强,王剑,付修根,冯兴雷,孙伟.北羌塘盆地长蛇山油页岩剖面烃源岩生烃潜力及沉积环境[J].中国地质,2013,40(6):1864~1865.
[9]成海燕,李安龙,龚建明.陆相烃源岩评价参数浅析[J].海洋地质动态,2008,24(2):6~9.
[10]范昌育,王震亮.页岩气富集与高产的地质因素和过程[J].ADVANCES IN TESTING TEC石油实验地质.2010,32(5):465~469.
[11]董谦,刘小平,李武广,董清源.关于页岩含气量确定方法的探讨[J].天然气与石油.2012,30(5):34~35.
[12]唐颖,张金川,刘珠江,李乐忠.解析法测量页岩含气量及其方法的改进[J].天然气工业.2011,31(10):108~112.
[13]刘弋生,谢军,武浩宁.页岩气储层评价技术的方法--实验分析技术[J].内江科技.2012,31(3):101~102.
[14]国家能源局发布.SY/T 7550-2004《原油中蜡、胶质、沥青质含量测定法》[S].
[15]国家质量监督检验检疫局发布.GB/T 19145-2003《.沉积岩中总有机碳的测定》[S].
[16]国家能源局发布.SY/T 5125-1996《透射光-荧光干酪根显微组分鉴定及类型划分方法》[S].国家质量监督检验检疫局发布.GB/T18602-2012《岩石热解分析》[S].
[17]国家质量监督检验检疫局发布.GB/T19143-2017《岩石有机质中碳、氢、氧元素分析方法》[S].
[18]国家能源局发布.SY/T5124-2012《沉积岩中镜质组反射率测定方法》[S].
[19]国家能源局发布.SY/T5163-1995《沉积岩黏土矿物相对含量X射线衍射分析方法》[S].
[20]国家能源局发布.SY/T6103-2004《岩石孔隙结构特征的测定图像分析法》[S].
[21]国家能源局发布.SY/T5162-2014《岩石样品扫描电子显微镜分析方法》[S].
[22]国家能源局发布.SY/T6385-2016《覆压下岩石孔隙度和渗透率测定方法》[S].
[23]国家质量监督检验检疫局发布.GB/T19959-2008《煤层气含量测定方法》[S].
[24]国家能源局发布.SY/T6132-2013《煤岩中甲烷等温吸附测定》[S].
[25]国家质量监督检验检疫局发布.GB/T 19560-2008《煤的高压等温吸附试验方法》[S]..HNIQUES FOR SHALE GAS
[2]帅琴,黄瑞成,高强,徐生瑞,邱海鸥,汤志勇.页岩气实验测试技术现状与研究进展[J].岩矿测试,2012,30(6):931~938.
[3]腾吉文,刘有山.中国页岩气成藏和潜在产能与环境的污染分析[J].中国地质,2013,13(1):1~11.
[4]RONALD J H,DANIEL M J,JOHN ZIMBERGE,et al Oil and gas geochemistry and petroleum systems of the Fort Worth Basin[J].AAPG Bulletin,2007,91(4):445~473.
[5]张金川,聂海宽,徐波,等.四川盆地页岩气成藏地质条件[J].天然气工业,2008,28(2):151~126.
[6]张金川,金之钧,袁明生.页岩气成藏机理和分布[J].天然气工业,2004,24(7):15~18.
[7]姜呈馥,王香增,张丽霞,万永平,雷裕红,孙建博,郭超.鄂尔多斯盆地东南延长组长7段陆相页岩气地质特征及勘查潜力评价[J].中国地质,2013,40(6):1884~1885.
[8]曾胜强,王剑,付修根,冯兴雷,孙伟.北羌塘盆地长蛇山油页岩剖面烃源岩生烃潜力及沉积环境[J].中国地质,2013,40(6):1864~1865.
[9]成海燕,李安龙,龚建明.陆相烃源岩评价参数浅析[J].海洋地质动态,2008,24(2):6~9.
[10]范昌育,王震亮.页岩气富集与高产的地质因素和过程[J].ADVANCES IN TESTING TEC石油实验地质.2010,32(5):465~469.
[11]董谦,刘小平,李武广,董清源.关于页岩含气量确定方法的探讨[J].天然气与石油.2012,30(5):34~35.
[12]唐颖,张金川,刘珠江,李乐忠.解析法测量页岩含气量及其方法的改进[J].天然气工业.2011,31(10):108~112.
[13]刘弋生,谢军,武浩宁.页岩气储层评价技术的方法--实验分析技术[J].内江科技.2012,31(3):101~102.
[14]国家能源局发布.SY/T 7550-2004《原油中蜡、胶质、沥青质含量测定法》[S].
[15]国家质量监督检验检疫局发布.GB/T 19145-2003《.沉积岩中总有机碳的测定》[S].
[16]国家能源局发布.SY/T 5125-1996《透射光-荧光干酪根显微组分鉴定及类型划分方法》[S].国家质量监督检验检疫局发布.GB/T18602-2012《岩石热解分析》[S].
[17]国家质量监督检验检疫局发布.GB/T19143-2017《岩石有机质中碳、氢、氧元素分析方法》[S].
[18]国家能源局发布.SY/T5124-2012《沉积岩中镜质组反射率测定方法》[S].
[19]国家能源局发布.SY/T5163-1995《沉积岩黏土矿物相对含量X射线衍射分析方法》[S].
[20]国家能源局发布.SY/T6103-2004《岩石孔隙结构特征的测定图像分析法》[S].
[21]国家能源局发布.SY/T5162-2014《岩石样品扫描电子显微镜分析方法》[S].
[22]国家能源局发布.SY/T6385-2016《覆压下岩石孔隙度和渗透率测定方法》[S].
[23]国家质量监督检验检疫局发布.GB/T19959-2008《煤层气含量测定方法》[S].
[24]国家能源局发布.SY/T6132-2013《煤岩中甲烷等温吸附测定》[S].
[25]国家质量监督检验检疫局发布.GB/T 19560-2008《煤的高压等温吸附试验方法》[S]..HNIQUES FOR SHALE GAS