牛乳中硝基呋喃代谢物检测技术研究进展
摘要
本文对牛乳中硝基呋喃类抗生素及其代谢物的残留危害和检测方法进行综述。介绍了样品前处理和仪器测定方法,包括高效液相色谱、液相色谱质谱联用、液相色谱串联质谱和酶联免疫吸附分析。同时综述了我国现有的关于硝基呋喃代谢物的检测方法,比较了各种方法的工作原理、适用范围以及各自的特点。
引文
[1]徐一平,胥传来.动物源食品中硝基呋喃类物质及其代谢物残留的检测技术研究[J].食品科学,2007,28(10):590-593.
[2]郑淑容.牛奶中抗生素残留的危害及对策[J].中国畜禽种业,2010,1:29-30.
[3]蒙君丽,周鑫,郑百芹,等.UPLC-MS/MS检测牛奶中硝基呋喃类代谢物残留[J].食品工业,2016,37(7):278-280.
[4]宋阳威.呋喃类药物检验检疫现状及对策[J].中国动物检疫,2003,20(3):37-39.
[5]柳毅.动物源性食品硝基呋喃类代谢物残留量的测定与分析[J].现代畜牧科技,2017,3(27):159.
[6]祝伟霞,刘亚风,梁炜.动物性食品中硝基呋喃类药物残留检测研究进展[J].动物医学进展,2010,31(2):99-102.
[7]李芳,陈莹,李献刚,等.动物源性食品中硝基呋喃及其代谢产物检测方法研究进展[J].食品安全质量检测学报,2016,7(6):2321-2327.
[8]郭德华,汪国权,王东辉,等.高效液相色谱-串联质谱法测定动物源性食品中硝基呋喃类代谢物残留量[J].化学分析计量,2005,14(4):16-18.
[9]Athikomrattanakul U,Katterle M,Gajovic-Eichelmann N,et al.Development of molecularly imprinted polymers for the binding ofnitrofurantoin[J].Biosens Bioelectr,2009,25(1):82-87.
[10]Freitas A,Barbosa J,Ramos F.Multi-residue and multi-class method for the determination of antibiotics in bovine muscle by ultra-high-performance liquid chromatography tandem mass spectrometry[J].Meat Sci,2014,98:58-64.
[11]Storey JM,Clark SB,Johnson AS,et al.Analysis of sulfonamides,trimethoprim,fluoroquinolones,quinolones,triphenylmethane dyes and methyltestosterone in fish and shrimp using liquid chromatography-mass spectrometry[J].J Chromatogr B,2014,972:38-47.
[12]丁涛,徐锦忠,沈崇钰,等.高效液相色谱-串联质谱联用测定蜂王浆中的四种硝基呋喃类药物的代谢物[J].色谱,2006,24(5):432-435.
[13]Angelini N M,Rampini O D,Mugica H.Liquid chromatographic determination of nitrofuran residues in bovine muscle tissues[J].Journal of AOAC International.,1997,80(3):481-485.
[14]郭德华,汪国权.高效液相色谱-串联质谱法测定动物源性食品中硝基呋喃类代谢物残留量[J].化学分析计量,2005,14(4):16-18.
[15]郭桢,连瑾,吴淑君.动物源性食品中呋喃唑酮及其代谢物的检测[J].广东农业科学,2005,5:57-59.
[16]Conneely A,Nugent A,Keefe MO.Use of solid phase extraction for the isolation and clean-up of a derivatised furazolidone metabolite fromanimal tissues[J].Analyst,2002,127:705-709.
[17]余建新,胡小钟,林雁飞,等.液相色谱-串联质谱联用法测定蜂蜜及水产品中硝基呋喃类抗生素代谢物残留量[J].分析科学学报,2004,20(4):382-384.
[18]翟艳,王卉.化学发光免疫分析及其进展[J].长春中医药大学2009,25(4):619-621.
[19]Chang C,Peng D P,Wu J E,et al.Development of an indirect competitive ELISA for the detection of furazotidone rDnrker residue in animal edible tissues[J].J Agric Food Chem,2007,56:1525-1531.
[20]谢世红,谢世涛,欧阳敏.水产品中4种硝基呋喃类代谢物残留快检方法的研究[J].江西农业学报,2014,26(8):61-64.
[2]郑淑容.牛奶中抗生素残留的危害及对策[J].中国畜禽种业,2010,1:29-30.
[3]蒙君丽,周鑫,郑百芹,等.UPLC-MS/MS检测牛奶中硝基呋喃类代谢物残留[J].食品工业,2016,37(7):278-280.
[4]宋阳威.呋喃类药物检验检疫现状及对策[J].中国动物检疫,2003,20(3):37-39.
[5]柳毅.动物源性食品硝基呋喃类代谢物残留量的测定与分析[J].现代畜牧科技,2017,3(27):159.
[6]祝伟霞,刘亚风,梁炜.动物性食品中硝基呋喃类药物残留检测研究进展[J].动物医学进展,2010,31(2):99-102.
[7]李芳,陈莹,李献刚,等.动物源性食品中硝基呋喃及其代谢产物检测方法研究进展[J].食品安全质量检测学报,2016,7(6):2321-2327.
[8]郭德华,汪国权,王东辉,等.高效液相色谱-串联质谱法测定动物源性食品中硝基呋喃类代谢物残留量[J].化学分析计量,2005,14(4):16-18.
[9]Athikomrattanakul U,Katterle M,Gajovic-Eichelmann N,et al.Development of molecularly imprinted polymers for the binding ofnitrofurantoin[J].Biosens Bioelectr,2009,25(1):82-87.
[10]Freitas A,Barbosa J,Ramos F.Multi-residue and multi-class method for the determination of antibiotics in bovine muscle by ultra-high-performance liquid chromatography tandem mass spectrometry[J].Meat Sci,2014,98:58-64.
[11]Storey JM,Clark SB,Johnson AS,et al.Analysis of sulfonamides,trimethoprim,fluoroquinolones,quinolones,triphenylmethane dyes and methyltestosterone in fish and shrimp using liquid chromatography-mass spectrometry[J].J Chromatogr B,2014,972:38-47.
[12]丁涛,徐锦忠,沈崇钰,等.高效液相色谱-串联质谱联用测定蜂王浆中的四种硝基呋喃类药物的代谢物[J].色谱,2006,24(5):432-435.
[13]Angelini N M,Rampini O D,Mugica H.Liquid chromatographic determination of nitrofuran residues in bovine muscle tissues[J].Journal of AOAC International.,1997,80(3):481-485.
[14]郭德华,汪国权.高效液相色谱-串联质谱法测定动物源性食品中硝基呋喃类代谢物残留量[J].化学分析计量,2005,14(4):16-18.
[15]郭桢,连瑾,吴淑君.动物源性食品中呋喃唑酮及其代谢物的检测[J].广东农业科学,2005,5:57-59.
[16]Conneely A,Nugent A,Keefe MO.Use of solid phase extraction for the isolation and clean-up of a derivatised furazolidone metabolite fromanimal tissues[J].Analyst,2002,127:705-709.
[17]余建新,胡小钟,林雁飞,等.液相色谱-串联质谱联用法测定蜂蜜及水产品中硝基呋喃类抗生素代谢物残留量[J].分析科学学报,2004,20(4):382-384.
[18]翟艳,王卉.化学发光免疫分析及其进展[J].长春中医药大学2009,25(4):619-621.
[19]Chang C,Peng D P,Wu J E,et al.Development of an indirect competitive ELISA for the detection of furazotidone rDnrker residue in animal edible tissues[J].J Agric Food Chem,2007,56:1525-1531.
[20]谢世红,谢世涛,欧阳敏.水产品中4种硝基呋喃类代谢物残留快检方法的研究[J].江西农业学报,2014,26(8):61-64.