响应面法优化玄武岩陶瓷纤维分散的工艺参数
|
摘要
利用响应面设计法(RSM),对分散玄武岩陶瓷纤维的工艺参数进行了研究。选择纤维分散剂、分散剂添加量、纤维浓度作为三个影响因素,分别建立了以MATLAB软件进行图像分析得到的均方差和沉降试验得到的分散度作为响应值的二次多项式模型,分析了各因素交互作用对纤维分散性的影响。两组试验进行相互验证,实验数据结果一致。研究表明,纤维高分散性的最佳工艺条件为:纤维分散剂选用羧甲基纤维素,分散剂添加量为10wt%,纤维浓度为1. 17 g/L,得到的均方差为34. 1883,分散度为75. 14%。
The parameters for dispersing basalt ceramic fibers were optimized by response surface method( RSM). The dispersant,its amount and concentration of fiber were selected as three influencing factors.A quadratic polynomial model was established. The mean square error obtained by image analysis with MATLAB software and the dispersion obtained by the sedimentation test were used as response values.The effects of the interaction of various factors on the fibers dispersibility were analyzed. The two experiments were mutually verified and the results were consistent. The research results show that the optimal process conditions for high fibers dispersibility are carboxymethyl cellulose as the dispersant( added 10 wt%) and concentration of fiber of 1. 17 g/L. The mean square error is 34. 1883 and the dispersion is 75. 14%.
The parameters for dispersing basalt ceramic fibers were optimized by response surface method( RSM). The dispersant,its amount and concentration of fiber were selected as three influencing factors.A quadratic polynomial model was established. The mean square error obtained by image analysis with MATLAB software and the dispersion obtained by the sedimentation test were used as response values.The effects of the interaction of various factors on the fibers dispersibility were analyzed. The two experiments were mutually verified and the results were consistent. The research results show that the optimal process conditions for high fibers dispersibility are carboxymethyl cellulose as the dispersant( added 10 wt%) and concentration of fiber of 1. 17 g/L. The mean square error is 34. 1883 and the dispersion is 75. 14%.
引文
[1]Raimondo M,Dondi M,Zanelli C.Processing and properties of large-sized ceramic slabs[J].Bol.Soc.Esp.Ceram.V,2010,49:289-296.
[2]段先湖,刘幼红,王博,等.陶瓷砖薄型减量化生产符合科学发展观的要求[J].陶瓷,2009(9):15-19.
[3]白战英,张卫星.关于陶瓷砖薄型化推进的几点建议[J].陶瓷,2012(7):45-48.
[4]Andre L S,Jucilene F,Marcelo D B.Effect of reduction of thickness on microstructure and properties of porcelain stoneware tiles[J].Ceramics International,2014,40:14693-14699.
[5]Li L B.Synergistic Effects of fiber debonding and fracture on matrix cracking in fiber-reinforced ceramic-matrix composites[J].Materials Science&Engineering A,2017,682:482-490.
[6]Hua Z S,Yao G C,Ma J F,et al.Fabrication and mechanical properties of short Zr O2fiber reinforced Ni Fe2O4matrix composites[J].Ceramics International,2013,39:3699-3708.
[7]华晓青,萧礼标,薛群虎,等.陶瓷基功能材料载体纤维增强效果及机理[J].人工晶体学报,2018,47(8):1542-1546.
[8]曾令可,胡动力.陶瓷纤维分散性能的研究[J].陶瓷学报,2008,29(4):324-328.
[9]王晶晶,赵传山,姜亦飞.硅酸铝纤维分散性的影响因素及提高方法[J].造纸化学品,2010,22(1):21-24.
[10]杨杰,张文苑,隋学叶,等.分散剂在陶瓷纤维分散过程中的应用[J].现代技术陶瓷,2014(4):58-60.
[11]Wang C,Jiao G S,Li B L,et al.Dispersion of carbon fibers and conductivity of carbon fiber-reinforced cement-based composites[J].Ceramics International,2017,43:15122-15132.
[12]冯云龙.莫来石基刚性多孔隔热材料的制备与性能研究[D].哈尔滨:哈尔滨工业大学,2012.
[13]Muhammad Y,Norlaili A,Faiz A,et al.Effect of basalt fibers dispersion on steel fire protection performance of epoxy-based intumescent coatings[J].Progress in Organic Coatings,2018,122:229-238.
[14]边宇,朱亚琪,王辉,等.响应面法优化Cu-BiVO4可见光催化降解扑热息痛污染物工艺研究[J].南水北调与水利科技,2014,12(6):22-25.
[15]崔佳丽,高利珍,高永华.响应面法优化MWCNTs-TiO2纳米颗粒深度降解焦化废水[J].太原理工大学学报,2013,44(6):713-717.
[16]Qiu T S,Yan H S,Li J F,et al.Response surface method for optimization of leaching of a low-grade ionic rare earth ore[J].Powder Technology,2018,330:330-338.
[17]Srdjan P,Ljiljana R,Vesna J,et al.Optimization of a nanoparticle ball milling process parameters using the response surface method[J].Advanced Powder Technology,2018,29:2129-2139.
[18]陈清,陈照峰,李承东,等.分散剂对玻璃纤维浆料分散性的影响[J].宇航材料工艺,2014(2):29-33.
[19]Zheng G,Nie H,Luo M,et al.Parametric design and analysis on the landing gear of a planet lander using the response surface method[J].Acta Astronautica,2018,148:225-234.
[20]崔旭峰,杜尔登.响应面方法优化光催化降解抗生素类污染物过程研究[J].环境科学与管理,2010,35(7):70-74.
[21]Xu G Q,Zhang H C,Zou Q,et al.Predicting and analyzing interaction of the thermal cloaking performance through response surface method[J].International Journal of Heat and Mass Transfer,2017,109:746-754.
[22]刘俊华.国产对位芳纶纤维悬浮液体系的分散性及机理研究[D].西安:陕西科技大学,2014.
[23]王宁.玄武岩纤维及其改性沥青的性能研究[D].武汉:中国地质大学,2013.
[24]王闯,李克智,李贺军.短碳纤维在不同分散剂中的分散性[J].精细化工,2007,24(1):1-5.
[2]段先湖,刘幼红,王博,等.陶瓷砖薄型减量化生产符合科学发展观的要求[J].陶瓷,2009(9):15-19.
[3]白战英,张卫星.关于陶瓷砖薄型化推进的几点建议[J].陶瓷,2012(7):45-48.
[4]Andre L S,Jucilene F,Marcelo D B.Effect of reduction of thickness on microstructure and properties of porcelain stoneware tiles[J].Ceramics International,2014,40:14693-14699.
[5]Li L B.Synergistic Effects of fiber debonding and fracture on matrix cracking in fiber-reinforced ceramic-matrix composites[J].Materials Science&Engineering A,2017,682:482-490.
[6]Hua Z S,Yao G C,Ma J F,et al.Fabrication and mechanical properties of short Zr O2fiber reinforced Ni Fe2O4matrix composites[J].Ceramics International,2013,39:3699-3708.
[7]华晓青,萧礼标,薛群虎,等.陶瓷基功能材料载体纤维增强效果及机理[J].人工晶体学报,2018,47(8):1542-1546.
[8]曾令可,胡动力.陶瓷纤维分散性能的研究[J].陶瓷学报,2008,29(4):324-328.
[9]王晶晶,赵传山,姜亦飞.硅酸铝纤维分散性的影响因素及提高方法[J].造纸化学品,2010,22(1):21-24.
[10]杨杰,张文苑,隋学叶,等.分散剂在陶瓷纤维分散过程中的应用[J].现代技术陶瓷,2014(4):58-60.
[11]Wang C,Jiao G S,Li B L,et al.Dispersion of carbon fibers and conductivity of carbon fiber-reinforced cement-based composites[J].Ceramics International,2017,43:15122-15132.
[12]冯云龙.莫来石基刚性多孔隔热材料的制备与性能研究[D].哈尔滨:哈尔滨工业大学,2012.
[13]Muhammad Y,Norlaili A,Faiz A,et al.Effect of basalt fibers dispersion on steel fire protection performance of epoxy-based intumescent coatings[J].Progress in Organic Coatings,2018,122:229-238.
[14]边宇,朱亚琪,王辉,等.响应面法优化Cu-BiVO4可见光催化降解扑热息痛污染物工艺研究[J].南水北调与水利科技,2014,12(6):22-25.
[15]崔佳丽,高利珍,高永华.响应面法优化MWCNTs-TiO2纳米颗粒深度降解焦化废水[J].太原理工大学学报,2013,44(6):713-717.
[16]Qiu T S,Yan H S,Li J F,et al.Response surface method for optimization of leaching of a low-grade ionic rare earth ore[J].Powder Technology,2018,330:330-338.
[17]Srdjan P,Ljiljana R,Vesna J,et al.Optimization of a nanoparticle ball milling process parameters using the response surface method[J].Advanced Powder Technology,2018,29:2129-2139.
[18]陈清,陈照峰,李承东,等.分散剂对玻璃纤维浆料分散性的影响[J].宇航材料工艺,2014(2):29-33.
[19]Zheng G,Nie H,Luo M,et al.Parametric design and analysis on the landing gear of a planet lander using the response surface method[J].Acta Astronautica,2018,148:225-234.
[20]崔旭峰,杜尔登.响应面方法优化光催化降解抗生素类污染物过程研究[J].环境科学与管理,2010,35(7):70-74.
[21]Xu G Q,Zhang H C,Zou Q,et al.Predicting and analyzing interaction of the thermal cloaking performance through response surface method[J].International Journal of Heat and Mass Transfer,2017,109:746-754.
[22]刘俊华.国产对位芳纶纤维悬浮液体系的分散性及机理研究[D].西安:陕西科技大学,2014.
[23]王宁.玄武岩纤维及其改性沥青的性能研究[D].武汉:中国地质大学,2013.
[24]王闯,李克智,李贺军.短碳纤维在不同分散剂中的分散性[J].精细化工,2007,24(1):1-5.