溶剂/非溶剂结晶技术制备纳米含能材料综述
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摘要
纳米含能材料具有诸多优异性能而受到专家学者的高度重视,发展了多种制备技术和方法;针对国内外溶剂/非溶剂结晶技术制备纳米含能材料的方法进行了综述,分析了影响纳米含能材料粒径和形貌的各种因素;溶剂/非溶剂技术具有很好的实际应用前景,已成为纳米含能材料制备的主流方法,同时指出了该方法还存在的不足和未来发展方向。
Nanoenergetic material has been highly attended by many researchers for its many excellent and desirable properties,multifarious preparation techniques and methods have been developed.The recent progress of preparation method of nanoenergetic materials through solvent/nonsolvent crystalltion route was reviewed in this work,and various factors which affect the particle size and morphology of nanoenergetic materials' were analyzed.The solvent/non-solvent technology has a good prospect of practical application and has become the mainstream method for nanoenergetic materials ' preparation.The shortcome and future research direction of this method were also pointed out.
Nanoenergetic material has been highly attended by many researchers for its many excellent and desirable properties,multifarious preparation techniques and methods have been developed.The recent progress of preparation method of nanoenergetic materials through solvent/nonsolvent crystalltion route was reviewed in this work,and various factors which affect the particle size and morphology of nanoenergetic materials' were analyzed.The solvent/non-solvent technology has a good prospect of practical application and has become the mainstream method for nanoenergetic materials ' preparation.The shortcome and future research direction of this method were also pointed out.
引文
[1]曾贵玉,聂福德.微纳米含能材料[M].北京:国防工业出版社,2015.
[2]ARMSTRONG R W.Dual Advantages of Ultrafine Crystalsized Energetic/Reactive Material Formulations[C]//Advancement in Energetic Materials&Chemical Propulsion,New York,2006.
[3]NARGES Z,MOHAMMAD H K,SEYED A S.The Advantages and Shortcomings of Using Nano-sized Energetic Materials[J].Central European Journal of Energetic Materials,2013,10(1):135-147.
[4]CHEN T,JIANG W,DU P,et al.Facile preparation of 1,3,5,7-tetranitro-1,3,5,7-tetrazocane/glycidylazide Polymer Energetic Nanocomposites with Enhanced Thermolysis Activity and Low Impact Sensitivity[J].RSC Advances,2017,7(10):5957-5965.
[5]KHASAINOV B A,ERMOLAEV B S,PRESLES H N,et al.On the Effect of Grain Size on Shock Sensitivity of Heterogeneous High Explosives[J].Shock Waves,1997(7):89-105.
[6]AN C,XU S,ZHANG Y,et al.Nano-HNS Particles:Mechanochemical Preparation and Properties Investigation[J].Journal of Nanomaterials,2018(1):1-7.
[7]SETCHELL R E.Grain-size Effects on the Shock Sensitivity of Hexanitrostilbene(HNS)Explosive[J].Combustion and flame,1984,56(3):343-345.
[8]SPITZER D,COMET M,BARAS C,et al.Energetic Nanomaterials:Opportunities for Enhanced Performances[J].Journal Physics Chemistry Solids,2010,71(2):100-108.
[9]WILLAM R F,THOMAS A.Recrystalization of HNS for the Preparation of Detonator Grade Explosive Material[R].DE88012862,1990.
[10]THORPE R,FAEIRHELLER W R.Development of Process for Reliable Detonator Grade Very Fine Secondary Explosive Powders[R].DE88012863,1990.
[11]GONTHIER K A.Modeling and Analysis of Reactive Compaction for Granular Energetic Materials[C]//NRC/AFOSR Summer Faculty Fellowship Report,Eglin Air Force Base,2001.
[12]YANG Z,GONG F,HE G,et al.Perfect Energetic Crystals with Improved Performances Obtained by Thermally Metastable Interfacial Self-Assembly of Corresponding Nanocrystals[J].Crystal Growth&Design,2018,18(3):1657-1665.
[13]MERCURI F,BALDONI M,SGAMELLOTTI A.Towards Nano-Organic Chemistry:Perspectives for a Bottom-up Approach to the Synthesis of Low-dimensional Carbon Nanostructures[J].Nanoscale,2012,4(2):369-379.
[14]叶毓鹏,曹欣茂,叶玲,等.炸药结晶工艺学及其应用[M].北京:国防工业出版社,1995.
[15]劳允亮.起爆药化学与工艺学[M].北京:北京理工大学出版社,2004.
[16]MULLIN J W.Crystallization,4th ED[M].Oxford:Butterworth-Heineman,2001.
[17]王相元,李伟明,周小伟,等.重结晶工艺对太安撞击感度的影响[J].火炸药学报,2009,32(2):37-40.
[18]RIGDON L P,MOODY GORDON L,RAYMOND R.Preparation of 1,3,5-Triamino-2,4,6-Trinitrobenzene of Submicron Particle Size[P].US 6310253,2001.
[19]KUMAR R,SIRIL P F,SONI P.Tuning the Particle Size and Morphology of High Energetic Material Nanocrystals[J].Defence Technology,2015,11(4):382-389.
[20]SZCZYGIELSKA J,CHLEBNA S.Friction Sensitivity of the Epsilon-CL-20 Crystals Obtained in Precipitation Process[J].Central European Journal of Energetic Materials,2011,8(2):117-130.
[21]GUPTA S,KUMAR P D,SHARMA S,et al.Pressurized Nozzle-Based Solvent/Anti-Solvent Process for Making Ultrafineε-CL-20 Explosive[J].Propellants,Explosives,Pyrotechnics,2017,42(7):773-783.
[22]THORPE R,FEAIRHELLER W R.Development of Processes for Reliable Detonator Grade Very Fine Secondary Explosives Powders[R].DE88-012863,1990.
[23]LEE J E,KIM J W,HAN S K,et al.Production of Submicron Sized Hexahydro-1,3,5-trinitro-1,3,5-triazine by Drowning-Out[J].Industrial&Engineering Chemistry Research,2014,53(12):4739-4747.
[24]NANDIA A K,KASARA S M,THANIGAIVELANA U,et al.Synthesis and Characterization of Ultrafine TATB[J].Journal of Energetic Materials,2007,25(4):213-231.
[25]BAYAT Y,EGHDAMTALAB M,ZEYNALI V.Control of the Particle Size of Submicron HMX Explosive by Spraying in Non-solvent[J].Journal of Energetic Materials,2010,28(4):272-284.
[26]KUMAR R,SIRIL P F,SONI P.Optimized Synthesis of HMX Nanoparticles using Antisolvent Precipitation method[J].Journal of Energetic Materials,2015,33(4):277-287.
[27]曾贵玉,聂福德,刘晏,等.超细BTF粒子的制备[J].火炸药学报,2002(3):20-22.
[28]王平,秦德新,聂福德,等.HNS的微纳化工艺研究[J].含能材料,2001(4):153-155.
[29]王智洁,王晶禹.国内外超细炸药制备技术的发展概况[J].山西化工,2006,26(2):50-52.
[30]ZHANG Y X,LIU D B,LV C X.Preparation and Characterization of Reticular Nano-HMX[J].Propellants,Explosives,Pyrotechnics,2005,30(6):438-441.
[31]ZHANG X,WEEKS B L.Preparation of Sub-micron Nitrocellulose Particles for Improved Combustion Behavior[J].Journal of Hazardous Materials,2014,268(11):224-228.
[32]LEE KY,MOORE D S,ASAY B W,et al.Submicron-Sized Gamma-HMX:Preparation and Initial Characterization[J].Journal of Energetic Materials,2007,25(3):161-171.
[33]曾贵玉,聂福德,尹莉莎,等.冲击结晶技术制备亚微米TATB粒子的研究[J].火炸药学报,2001(4):12-14.
[34]Yang G C,Nie F D,Li J S,et al.Preparation and Characterization of Nano-NTO Explosive[J].Journal of Energetic Materials,2007,25(1):35-47.
[35]YANG G C,NIE F D,HUANG H,et al.Preparation and Characterization of Nano-TATB Explosive[J].Propellants,Explosives,Pyrotechnics,2006,31(5):390-394.
[36]HUANG H,WANG J Y,XU W Z,et al.Effect of Habit Modifiers on Morphology and Properties of Nano-HNS Explosive in Prefilming Twin-fluid Nozzle-assisted Precipitation[J].Propellants,Explosives,Pyrotechnics,2009,34(1):78-83.
[37]谯志强.不同形貌超细RDX的制备[D].绵阳:中国工程物理研究院,2005.
[38]刘杰,王龙祥,李青,等.钝感纳米RDX的制备与表征[J].火炸药学报,2013,35(6):46-50.
[39]王平,秦德新,陈娅,等.HNS-IV的纯化与防聚集研究[C].//2002年火炸药技术及钝感弹药学术研讨会论文集.珠海,2002.
[40]BAYAT Y,MOUSAVI S H,BAYAT F,et al.Preparation Nano-sized HMX by Using Ultrasonic Waves[C]//The2011 International Autumn Seminar on Propellants,Explosives and Pyrotechnics.Nanjing,2011.
[41]MIKONSAARI I,LEISINGER K,HARTLIEB K,et al.Size Reduction of Crystalline Energetic Material Using Ultrasonic[C]//33th International Annual Conferece of ICT.Karlsruhe,2002:49-1.
[42]王平,秦德新,辛芳,等.超声波在超细炸药制备中的应用[J].含能材料,2003,2:107-109.
[43]PATIL M N,GORE G M,PANDIT A B.Ultrasonically Controlled Particle Size Distribution of Explosives:A safe Method[J].Ultrasonics Sonochemistry,2008,1:177-187.
[44]BAYAT Y,ZEYNALI V.Preparation and Characterization of Nano-CL-20 Explosive[J].Journal of Energetic Materials,2011,29(4):281-291.
[45]杨光成,聂福德.超细HMX的制备与表征研究[J].含能材料,2004(6):350-352.
[46]YANG G C,HU H L,ZHOU Y,et al.Synthesis of One Molecule-thick Single-crystalline Nanosheets of Energetic Material for High Sensitive Force Sensor[R].Scientific Reports,2012(2):698.
[47]HUANG B,QIAO Z Q,NIE F D,et al.Fabrication of FOX-7 Quasi-three-dimensional Grids of One-dimensional Nanostructures via a Spray Freeze-drying Technique and Size-dependence of Thermal Properties[J].Journal of Hazardous Materials,2010,184(10):561-566.
[48]CHEN J,QIAO Z Q,WANG L L,et al.Fabrication of Rectangular 2,6-diamino-3,5-dinitropyrazine-1-oxide Microtubes[J].Materials Letters,2011,65(8):1018-1021.
[49]WANG J Y,LI J L,AN C W,et al.Study on Ultrasoundand Spray-assisted Precipitation of CL-20[J].Propellants,Explosives,Pyrotechnics,2012,37(6):670-675.
[50]SALONI J,WALKER K,HILL JR G.Theoretical Investigation on Monomer and Solvent Selection for Molecular Imprinting of Nitrocompounds[J].The Journal of Physical Chemistry A,2013,117(7):1531-1534.
[51]AN C,HEQUN L,BINSHUO Y,et al.Preparation and Characterization of Ultrafine-Hexanitrohexaazaisowurtzitane Particles[J].International Journal of Energetic Materials and Chemical Propulsion.2015,14(4):295-306.
[52]HUANG B,CAO M,NIE F,et al.Construction and Properties of Structure-and Size-controlled Micro/Nano-energetic Materials[J].Defence Technology,2013,9(2):59-79.
[53]宋杉,向斌,张朝阳,等.基于自组装方法制备纳米含能材料的研究进展[J].含能材料,2014,22(1):108-115.
[2]ARMSTRONG R W.Dual Advantages of Ultrafine Crystalsized Energetic/Reactive Material Formulations[C]//Advancement in Energetic Materials&Chemical Propulsion,New York,2006.
[3]NARGES Z,MOHAMMAD H K,SEYED A S.The Advantages and Shortcomings of Using Nano-sized Energetic Materials[J].Central European Journal of Energetic Materials,2013,10(1):135-147.
[4]CHEN T,JIANG W,DU P,et al.Facile preparation of 1,3,5,7-tetranitro-1,3,5,7-tetrazocane/glycidylazide Polymer Energetic Nanocomposites with Enhanced Thermolysis Activity and Low Impact Sensitivity[J].RSC Advances,2017,7(10):5957-5965.
[5]KHASAINOV B A,ERMOLAEV B S,PRESLES H N,et al.On the Effect of Grain Size on Shock Sensitivity of Heterogeneous High Explosives[J].Shock Waves,1997(7):89-105.
[6]AN C,XU S,ZHANG Y,et al.Nano-HNS Particles:Mechanochemical Preparation and Properties Investigation[J].Journal of Nanomaterials,2018(1):1-7.
[7]SETCHELL R E.Grain-size Effects on the Shock Sensitivity of Hexanitrostilbene(HNS)Explosive[J].Combustion and flame,1984,56(3):343-345.
[8]SPITZER D,COMET M,BARAS C,et al.Energetic Nanomaterials:Opportunities for Enhanced Performances[J].Journal Physics Chemistry Solids,2010,71(2):100-108.
[9]WILLAM R F,THOMAS A.Recrystalization of HNS for the Preparation of Detonator Grade Explosive Material[R].DE88012862,1990.
[10]THORPE R,FAEIRHELLER W R.Development of Process for Reliable Detonator Grade Very Fine Secondary Explosive Powders[R].DE88012863,1990.
[11]GONTHIER K A.Modeling and Analysis of Reactive Compaction for Granular Energetic Materials[C]//NRC/AFOSR Summer Faculty Fellowship Report,Eglin Air Force Base,2001.
[12]YANG Z,GONG F,HE G,et al.Perfect Energetic Crystals with Improved Performances Obtained by Thermally Metastable Interfacial Self-Assembly of Corresponding Nanocrystals[J].Crystal Growth&Design,2018,18(3):1657-1665.
[13]MERCURI F,BALDONI M,SGAMELLOTTI A.Towards Nano-Organic Chemistry:Perspectives for a Bottom-up Approach to the Synthesis of Low-dimensional Carbon Nanostructures[J].Nanoscale,2012,4(2):369-379.
[14]叶毓鹏,曹欣茂,叶玲,等.炸药结晶工艺学及其应用[M].北京:国防工业出版社,1995.
[15]劳允亮.起爆药化学与工艺学[M].北京:北京理工大学出版社,2004.
[16]MULLIN J W.Crystallization,4th ED[M].Oxford:Butterworth-Heineman,2001.
[17]王相元,李伟明,周小伟,等.重结晶工艺对太安撞击感度的影响[J].火炸药学报,2009,32(2):37-40.
[18]RIGDON L P,MOODY GORDON L,RAYMOND R.Preparation of 1,3,5-Triamino-2,4,6-Trinitrobenzene of Submicron Particle Size[P].US 6310253,2001.
[19]KUMAR R,SIRIL P F,SONI P.Tuning the Particle Size and Morphology of High Energetic Material Nanocrystals[J].Defence Technology,2015,11(4):382-389.
[20]SZCZYGIELSKA J,CHLEBNA S.Friction Sensitivity of the Epsilon-CL-20 Crystals Obtained in Precipitation Process[J].Central European Journal of Energetic Materials,2011,8(2):117-130.
[21]GUPTA S,KUMAR P D,SHARMA S,et al.Pressurized Nozzle-Based Solvent/Anti-Solvent Process for Making Ultrafineε-CL-20 Explosive[J].Propellants,Explosives,Pyrotechnics,2017,42(7):773-783.
[22]THORPE R,FEAIRHELLER W R.Development of Processes for Reliable Detonator Grade Very Fine Secondary Explosives Powders[R].DE88-012863,1990.
[23]LEE J E,KIM J W,HAN S K,et al.Production of Submicron Sized Hexahydro-1,3,5-trinitro-1,3,5-triazine by Drowning-Out[J].Industrial&Engineering Chemistry Research,2014,53(12):4739-4747.
[24]NANDIA A K,KASARA S M,THANIGAIVELANA U,et al.Synthesis and Characterization of Ultrafine TATB[J].Journal of Energetic Materials,2007,25(4):213-231.
[25]BAYAT Y,EGHDAMTALAB M,ZEYNALI V.Control of the Particle Size of Submicron HMX Explosive by Spraying in Non-solvent[J].Journal of Energetic Materials,2010,28(4):272-284.
[26]KUMAR R,SIRIL P F,SONI P.Optimized Synthesis of HMX Nanoparticles using Antisolvent Precipitation method[J].Journal of Energetic Materials,2015,33(4):277-287.
[27]曾贵玉,聂福德,刘晏,等.超细BTF粒子的制备[J].火炸药学报,2002(3):20-22.
[28]王平,秦德新,聂福德,等.HNS的微纳化工艺研究[J].含能材料,2001(4):153-155.
[29]王智洁,王晶禹.国内外超细炸药制备技术的发展概况[J].山西化工,2006,26(2):50-52.
[30]ZHANG Y X,LIU D B,LV C X.Preparation and Characterization of Reticular Nano-HMX[J].Propellants,Explosives,Pyrotechnics,2005,30(6):438-441.
[31]ZHANG X,WEEKS B L.Preparation of Sub-micron Nitrocellulose Particles for Improved Combustion Behavior[J].Journal of Hazardous Materials,2014,268(11):224-228.
[32]LEE KY,MOORE D S,ASAY B W,et al.Submicron-Sized Gamma-HMX:Preparation and Initial Characterization[J].Journal of Energetic Materials,2007,25(3):161-171.
[33]曾贵玉,聂福德,尹莉莎,等.冲击结晶技术制备亚微米TATB粒子的研究[J].火炸药学报,2001(4):12-14.
[34]Yang G C,Nie F D,Li J S,et al.Preparation and Characterization of Nano-NTO Explosive[J].Journal of Energetic Materials,2007,25(1):35-47.
[35]YANG G C,NIE F D,HUANG H,et al.Preparation and Characterization of Nano-TATB Explosive[J].Propellants,Explosives,Pyrotechnics,2006,31(5):390-394.
[36]HUANG H,WANG J Y,XU W Z,et al.Effect of Habit Modifiers on Morphology and Properties of Nano-HNS Explosive in Prefilming Twin-fluid Nozzle-assisted Precipitation[J].Propellants,Explosives,Pyrotechnics,2009,34(1):78-83.
[37]谯志强.不同形貌超细RDX的制备[D].绵阳:中国工程物理研究院,2005.
[38]刘杰,王龙祥,李青,等.钝感纳米RDX的制备与表征[J].火炸药学报,2013,35(6):46-50.
[39]王平,秦德新,陈娅,等.HNS-IV的纯化与防聚集研究[C].//2002年火炸药技术及钝感弹药学术研讨会论文集.珠海,2002.
[40]BAYAT Y,MOUSAVI S H,BAYAT F,et al.Preparation Nano-sized HMX by Using Ultrasonic Waves[C]//The2011 International Autumn Seminar on Propellants,Explosives and Pyrotechnics.Nanjing,2011.
[41]MIKONSAARI I,LEISINGER K,HARTLIEB K,et al.Size Reduction of Crystalline Energetic Material Using Ultrasonic[C]//33th International Annual Conferece of ICT.Karlsruhe,2002:49-1.
[42]王平,秦德新,辛芳,等.超声波在超细炸药制备中的应用[J].含能材料,2003,2:107-109.
[43]PATIL M N,GORE G M,PANDIT A B.Ultrasonically Controlled Particle Size Distribution of Explosives:A safe Method[J].Ultrasonics Sonochemistry,2008,1:177-187.
[44]BAYAT Y,ZEYNALI V.Preparation and Characterization of Nano-CL-20 Explosive[J].Journal of Energetic Materials,2011,29(4):281-291.
[45]杨光成,聂福德.超细HMX的制备与表征研究[J].含能材料,2004(6):350-352.
[46]YANG G C,HU H L,ZHOU Y,et al.Synthesis of One Molecule-thick Single-crystalline Nanosheets of Energetic Material for High Sensitive Force Sensor[R].Scientific Reports,2012(2):698.
[47]HUANG B,QIAO Z Q,NIE F D,et al.Fabrication of FOX-7 Quasi-three-dimensional Grids of One-dimensional Nanostructures via a Spray Freeze-drying Technique and Size-dependence of Thermal Properties[J].Journal of Hazardous Materials,2010,184(10):561-566.
[48]CHEN J,QIAO Z Q,WANG L L,et al.Fabrication of Rectangular 2,6-diamino-3,5-dinitropyrazine-1-oxide Microtubes[J].Materials Letters,2011,65(8):1018-1021.
[49]WANG J Y,LI J L,AN C W,et al.Study on Ultrasoundand Spray-assisted Precipitation of CL-20[J].Propellants,Explosives,Pyrotechnics,2012,37(6):670-675.
[50]SALONI J,WALKER K,HILL JR G.Theoretical Investigation on Monomer and Solvent Selection for Molecular Imprinting of Nitrocompounds[J].The Journal of Physical Chemistry A,2013,117(7):1531-1534.
[51]AN C,HEQUN L,BINSHUO Y,et al.Preparation and Characterization of Ultrafine-Hexanitrohexaazaisowurtzitane Particles[J].International Journal of Energetic Materials and Chemical Propulsion.2015,14(4):295-306.
[52]HUANG B,CAO M,NIE F,et al.Construction and Properties of Structure-and Size-controlled Micro/Nano-energetic Materials[J].Defence Technology,2013,9(2):59-79.
[53]宋杉,向斌,张朝阳,等.基于自组装方法制备纳米含能材料的研究进展[J].含能材料,2014,22(1):108-115.