气相色谱-质谱检测浓香型白酒氨基甲酸乙酯预处理方法的研究
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摘要
饮酒是摄入氨基甲酸乙酯的主要方式,通过实验比较液液萃取法和固相萃取法,确定更加高效的浓香型白酒氨基甲酸乙酯检测预处理方法。
Drinking is the main way of ethyl carbamate(EC) intake, we compae liquid-liquid extraction method(LLE) and solid phase extraction method(SPE) by experiment to determine the best efficient pretreatment method of the EC detection for the Luzhou-flavor liquor.
Drinking is the main way of ethyl carbamate(EC) intake, we compae liquid-liquid extraction method(LLE) and solid phase extraction method(SPE) by experiment to determine the best efficient pretreatment method of the EC detection for the Luzhou-flavor liquor.
引文
[1]沈怡方.白酒生产技术全书[M].中国轻工业出版社,1998.
[2]肖玉华.2012年11月中国白酒产量达1023.32万千升[J].中国酒,2013:82-82.
[3]Weber J V,Sharypov V I.Ethyl Carbamate in Foods and Beverages A Review[M].//Climate Change,Intercropping,Pest Control and Beneficial Microorganisms.Springer Netherlands,2009.
[4]吴世嘉,王洪新.发酵食品中氨基甲酸乙酯的研究进展[J].化学与生物工程,2009,26(9):15-19.
[5]Lachenmeier D W,Lima M C,Nóbrega I C,et al.Cancer risk assessment of ethyl carbamate in alcoholic beverages from Brazil with special consideration to the spirits cachaa and tiquira[J].Bmc Cancer,2010,10(1):266.
[6]Lee KG.Analysis and risk assessment of ethyl carbamate invarious fermented foods[J].European Food Res Technol,2013,236:891-898
[7]Huang Z,Pan XD,Wu PG,et al.Validation(in-house and collaboratory)of the quantification method for ethyl carbamate in alcoholic beverages and soy sauce by GC-MS[J].Food Chem,2013,141(4):4161-4165
[8]耿予欢,吕芬,黄伟雄,等.黄酒中氨基甲酸乙酯的分析与控制[J].现代食品科技,2013,29(9):2271-2274
[9]Nobrega ICC,Pereira GE,Silva M,et al.Improved sample preparation for GC-MS-SIM analysis of ethyl carbamate in wine[J].Food Chem,2015,177:23-28
[10]Ye CW,Zhang XN,Huang JY,et al.Multiple headspace solid-phase microextraction of ethyl carbamate from different alcoholic beverages employing drying agent based matrix modification[J].J Chromatogr A,2011,1218(31):5063-5070
[11]Zhang J,Liu GX,Zhang Y,et al.Simultaneous determination of ethyl carbamate and urea in alcoholic beverages by high-performance liquid chromatography coupled with fluorescence detection[J].J Agric Food Chem,2014,62(13):2797-2802
[12]王丽娟,柯润辉,王冰.超高效液相色谱-电喷雾串联质谱法直接测定黄酒和葡萄酒中氨基甲酸乙酯[J].色谱,2012,30(9):903-907
[13]SN/T 0285-2012出口酒中氨基甲酸乙酯残留量检测方法气相色谱-质谱法[S].
[14]AOAC Official Method 994.07.Ethyl carbamate in alcoholic beverages and soy sauce[S].
[15]Method OIV-MA-AS315-04.Compendium of international methods of analysis-OIV ethyl carbamate[S].
[2]肖玉华.2012年11月中国白酒产量达1023.32万千升[J].中国酒,2013:82-82.
[3]Weber J V,Sharypov V I.Ethyl Carbamate in Foods and Beverages A Review[M].//Climate Change,Intercropping,Pest Control and Beneficial Microorganisms.Springer Netherlands,2009.
[4]吴世嘉,王洪新.发酵食品中氨基甲酸乙酯的研究进展[J].化学与生物工程,2009,26(9):15-19.
[5]Lachenmeier D W,Lima M C,Nóbrega I C,et al.Cancer risk assessment of ethyl carbamate in alcoholic beverages from Brazil with special consideration to the spirits cachaa and tiquira[J].Bmc Cancer,2010,10(1):266.
[6]Lee KG.Analysis and risk assessment of ethyl carbamate invarious fermented foods[J].European Food Res Technol,2013,236:891-898
[7]Huang Z,Pan XD,Wu PG,et al.Validation(in-house and collaboratory)of the quantification method for ethyl carbamate in alcoholic beverages and soy sauce by GC-MS[J].Food Chem,2013,141(4):4161-4165
[8]耿予欢,吕芬,黄伟雄,等.黄酒中氨基甲酸乙酯的分析与控制[J].现代食品科技,2013,29(9):2271-2274
[9]Nobrega ICC,Pereira GE,Silva M,et al.Improved sample preparation for GC-MS-SIM analysis of ethyl carbamate in wine[J].Food Chem,2015,177:23-28
[10]Ye CW,Zhang XN,Huang JY,et al.Multiple headspace solid-phase microextraction of ethyl carbamate from different alcoholic beverages employing drying agent based matrix modification[J].J Chromatogr A,2011,1218(31):5063-5070
[11]Zhang J,Liu GX,Zhang Y,et al.Simultaneous determination of ethyl carbamate and urea in alcoholic beverages by high-performance liquid chromatography coupled with fluorescence detection[J].J Agric Food Chem,2014,62(13):2797-2802
[12]王丽娟,柯润辉,王冰.超高效液相色谱-电喷雾串联质谱法直接测定黄酒和葡萄酒中氨基甲酸乙酯[J].色谱,2012,30(9):903-907
[13]SN/T 0285-2012出口酒中氨基甲酸乙酯残留量检测方法气相色谱-质谱法[S].
[14]AOAC Official Method 994.07.Ethyl carbamate in alcoholic beverages and soy sauce[S].
[15]Method OIV-MA-AS315-04.Compendium of international methods of analysis-OIV ethyl carbamate[S].