无机晶须的制备及应用进展
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摘要
综述了无机晶须的制备方法和一些常见晶须如碳化硅、硼酸铝、氧化锌、钛酸钾、莫来石、硫酸钙、硫酸镁的结构、性能及其应用情况。同时,从结构型材料转向功能型材料是现在研究的重点,也是未来高新材料研究的发展方向。
This paper mainly focus on the preparation methods of inorganic whiskers,and the structure,properties and application of some common whiskers such as silicon carbide,aluminum borate,zinc oxide,potassium titanate,mullite,calcium sulfate and magnesium sulfate.At the same time,the transition from structural materials to functional materials is not only the major focus of current research,but also the future development direction of high-tech materials.
This paper mainly focus on the preparation methods of inorganic whiskers,and the structure,properties and application of some common whiskers such as silicon carbide,aluminum borate,zinc oxide,potassium titanate,mullite,calcium sulfate and magnesium sulfate.At the same time,the transition from structural materials to functional materials is not only the major focus of current research,but also the future development direction of high-tech materials.
引文
[1] Brenner S S.Facters Influencing the Strength of Whiskers in Fiber Composite Materials[M].New York:American Society for Metals,1965.
[2] Erker L.Tretise on Ores and Assaying[M].2nd ed.Chicago:University of Chicago,1951:177-183.
[3] 潘金生,陈永华.晶须及其应用[J].复合材料学报,1995,12(4):1-7.
[4] 袁建君,方琪,刘智恩.晶须的研究进展[J].材料科学与工程,1996,14(4):1-7.
[5] 李广宇,李子东,叶进.晶须的性能及其应用进展[J].热固性树脂,2000,15(2):48-51.
[6] 刘玲,殷宁,亢茂青,等.晶须增韧复合材料机理的研究[J].材料科学与工程,2000,18(2):116-119.
[7] Evans C C.Whiskers[M].London:Mills Boon Limited,1972.
[8] Parvizi-Majidi Azar.Ullmann’s Encyclopedia of Industrial Chemistry:Whiskers[M].Wiley-VCH Verlag GmbH & Co KGaA,2000.
[9] 李武,靳治良,张志宏.无机晶须材料的合成与应用[J].化学进展,2003,15(4):264-273.
[10] Geng L,Zhang J.A study of the crystal structure of a commercial-SiC whisker by high-resolution TEM[J].Materials Chemistry and Physics,2004,84:243-246.
[11] Geng L,Ochiai S,Hu J Q,et al.Compression testing of SiCw/Al composite at tempreture close to and above the solidus of the matrix alloy[J].Material Science and Engeneering,1998,246A:302-305.
[12] Ye F,Le T Q,Zhou Y.Interface structure and mechanical properties of Al2O3 20%SiCw ceramic matrix composite[J].Material Science and Engineering,2000,281A:305-309.
[13] Brennan J J,Nutt S R.SiC-Whisker-reinforced glass-ceramic composites:Interfaces and properties[J].Journal of the American Ceramics Society,1992,75:1205-1216.
[14] Hua Y F,Zhang L T,Cheng Laifei,et al.Silicon carbide whisker reinforced silicon carbide composites by chemical vapor infiltration[J].Material Science and Engeneering,2006,428:346-350.
[15] Ogawa J,Takeoki R.Granular aggregate of aluminum borate whisker:JP,07330499[P].1995-12-19.
[16] 隗学礼,赵宽放.硼酸铝晶须制备方法:中国,1093065A[P].1994-10-05.
[17] Ma R,Bando Y,Sato T.Single-crystal Al18B4O33 microtube[J].Journal of the American Chemical Society,2002,124(36):10668-10669.
[18] Li J X,Narita T,Ogawa J,et al.In situ synthesis of porous ceramics with a framework structure of aluminium borate whisker[J].Journal of Materials Science,1998,33(10):2601-2605.
[19] Wada H,Sakane K,Kitamura T,et al.Synthesis of aluminum borate whiskers in potassium-sulfate flux[J].Journal of Materials Science Letters,1991,10(18):1076-1077.
[20] Hu J Q,Ma X L,Xie Z Y,et al.Characterization of zinc oxide crystal whiskers grown by thermal evaporation[J].Chemical Physics Letters,2001,344:97-100.
[21] Fuller M L.Twining in zinc oxide[J].Journal of Applied Physics,1944,15:164-170.
[22] Pan Z W,Daiand Z R,Wang Z L.Nanobelts of semiconducting oxides[J].Science,2001,291:1947-1949.
[23] Huang M H,Wu Y,Feiek H,et al.Catalytic growth of zinc oxide nanowires by vapor transport[J].Advanced Materials,2001,13(2):113-116.
[24] Guo M,Diao P,Cai S M.Hydrothermal growth of well-aligned ZnO nanorod arrays:Dependence of morphology and alignment ordering upon preparing conditions[J].Journal of Solid State Chemistry,2005,178:1864-1873.
[25] 刘红霞,周圣明,李抒智,等.柱状ZnO阵列薄膜的生长及其发光特性[J].物理学报,2006,55(3):1398-1401.
[26] 景晓明,卢佳美,马晨,等.钛酸钾晶须研究现状及发展前景[J].西南民族大学学报:自然科学版,2008,34(3):539-544.
[27] Peng P,Chris S.Preparation of mullite whiskers from topaz decomposition[J].Material Letters,2004,58(7/8):1288-1291.
[28] Agathopoulos S,Fernanders H,Tulyaganov D.Preparetion of mullite whiskers from kaolinite using CuSO4 as fluxing agent[J].Materials Science Forum,2004,455/456:818-821.
[29] Kim B M,Yang T Y,Yoon S Y,et al.Processing of mullite whiskers from Kaolin[J].Advanced Materials Research,2007,29:203-206.
[30] 朱伯铨,郝瑞,李雪冬.在硫酸钠熔盐中合成莫来石晶须[J].耐火材料,2006,40(3):165-168.
[31] 聂建华,张寒,徐满,等.熔盐法合成莫来石晶须[J].稀有金属材料与工程,2009,38(S2):1154-1157.
[32] Hashimoto S,Yamaguchi A.Synthesis of mullite whiskers using Na2SO4 flux[J].Journal of the Ceramic Society of Japan,2004,112(2):104-109.
[33] Ismail M,Arai H,Nakai Z,et al.Mullite whiskers from precursor gel powdes[J].Journal of the American Ceramic Society,1990,73(9):2736-2739.
[34] 袁建君,刘智恩,韩玉.溶胶-凝胶法制备莫来石晶须[J].硅酸盐学报,1996,24(3):342-346.
[35] Kong L B,Huang H,Zhang T S,et al.Growth of mullite whiskers in mechanochemically activated oxides doped with WO3[J].Journal of the European Ceramic Society,2003,23(13):2257-2264.
[36] Kong L B,Chen Y Z,Zhang T S.Effect of alkaline-earth oxides on phase formation and morphology development of mulite ceramics[J].Ceramics International,2004,30(7):1319-1323.
[37] 袁致涛,王泽红,韩跃新,等.用石膏合成超细硫酸钙晶须的研究[J].中国矿业,2005,14(11):30-33.
[38] 吕通建,于洋,范平,等.碱式硫酸镁晶须增强阻燃聚丙烯的研究[J].中国塑料,2001,15(9):66-68.
[39] 陶国良,龚方红,丁家红.镁盐晶须填充改性聚丙烯材料研究[J].中国塑料,2003,17(12):45-48.
[2] Erker L.Tretise on Ores and Assaying[M].2nd ed.Chicago:University of Chicago,1951:177-183.
[3] 潘金生,陈永华.晶须及其应用[J].复合材料学报,1995,12(4):1-7.
[4] 袁建君,方琪,刘智恩.晶须的研究进展[J].材料科学与工程,1996,14(4):1-7.
[5] 李广宇,李子东,叶进.晶须的性能及其应用进展[J].热固性树脂,2000,15(2):48-51.
[6] 刘玲,殷宁,亢茂青,等.晶须增韧复合材料机理的研究[J].材料科学与工程,2000,18(2):116-119.
[7] Evans C C.Whiskers[M].London:Mills Boon Limited,1972.
[8] Parvizi-Majidi Azar.Ullmann’s Encyclopedia of Industrial Chemistry:Whiskers[M].Wiley-VCH Verlag GmbH & Co KGaA,2000.
[9] 李武,靳治良,张志宏.无机晶须材料的合成与应用[J].化学进展,2003,15(4):264-273.
[10] Geng L,Zhang J.A study of the crystal structure of a commercial-SiC whisker by high-resolution TEM[J].Materials Chemistry and Physics,2004,84:243-246.
[11] Geng L,Ochiai S,Hu J Q,et al.Compression testing of SiCw/Al composite at tempreture close to and above the solidus of the matrix alloy[J].Material Science and Engeneering,1998,246A:302-305.
[12] Ye F,Le T Q,Zhou Y.Interface structure and mechanical properties of Al2O3 20%SiCw ceramic matrix composite[J].Material Science and Engineering,2000,281A:305-309.
[13] Brennan J J,Nutt S R.SiC-Whisker-reinforced glass-ceramic composites:Interfaces and properties[J].Journal of the American Ceramics Society,1992,75:1205-1216.
[14] Hua Y F,Zhang L T,Cheng Laifei,et al.Silicon carbide whisker reinforced silicon carbide composites by chemical vapor infiltration[J].Material Science and Engeneering,2006,428:346-350.
[15] Ogawa J,Takeoki R.Granular aggregate of aluminum borate whisker:JP,07330499[P].1995-12-19.
[16] 隗学礼,赵宽放.硼酸铝晶须制备方法:中国,1093065A[P].1994-10-05.
[17] Ma R,Bando Y,Sato T.Single-crystal Al18B4O33 microtube[J].Journal of the American Chemical Society,2002,124(36):10668-10669.
[18] Li J X,Narita T,Ogawa J,et al.In situ synthesis of porous ceramics with a framework structure of aluminium borate whisker[J].Journal of Materials Science,1998,33(10):2601-2605.
[19] Wada H,Sakane K,Kitamura T,et al.Synthesis of aluminum borate whiskers in potassium-sulfate flux[J].Journal of Materials Science Letters,1991,10(18):1076-1077.
[20] Hu J Q,Ma X L,Xie Z Y,et al.Characterization of zinc oxide crystal whiskers grown by thermal evaporation[J].Chemical Physics Letters,2001,344:97-100.
[21] Fuller M L.Twining in zinc oxide[J].Journal of Applied Physics,1944,15:164-170.
[22] Pan Z W,Daiand Z R,Wang Z L.Nanobelts of semiconducting oxides[J].Science,2001,291:1947-1949.
[23] Huang M H,Wu Y,Feiek H,et al.Catalytic growth of zinc oxide nanowires by vapor transport[J].Advanced Materials,2001,13(2):113-116.
[24] Guo M,Diao P,Cai S M.Hydrothermal growth of well-aligned ZnO nanorod arrays:Dependence of morphology and alignment ordering upon preparing conditions[J].Journal of Solid State Chemistry,2005,178:1864-1873.
[25] 刘红霞,周圣明,李抒智,等.柱状ZnO阵列薄膜的生长及其发光特性[J].物理学报,2006,55(3):1398-1401.
[26] 景晓明,卢佳美,马晨,等.钛酸钾晶须研究现状及发展前景[J].西南民族大学学报:自然科学版,2008,34(3):539-544.
[27] Peng P,Chris S.Preparation of mullite whiskers from topaz decomposition[J].Material Letters,2004,58(7/8):1288-1291.
[28] Agathopoulos S,Fernanders H,Tulyaganov D.Preparetion of mullite whiskers from kaolinite using CuSO4 as fluxing agent[J].Materials Science Forum,2004,455/456:818-821.
[29] Kim B M,Yang T Y,Yoon S Y,et al.Processing of mullite whiskers from Kaolin[J].Advanced Materials Research,2007,29:203-206.
[30] 朱伯铨,郝瑞,李雪冬.在硫酸钠熔盐中合成莫来石晶须[J].耐火材料,2006,40(3):165-168.
[31] 聂建华,张寒,徐满,等.熔盐法合成莫来石晶须[J].稀有金属材料与工程,2009,38(S2):1154-1157.
[32] Hashimoto S,Yamaguchi A.Synthesis of mullite whiskers using Na2SO4 flux[J].Journal of the Ceramic Society of Japan,2004,112(2):104-109.
[33] Ismail M,Arai H,Nakai Z,et al.Mullite whiskers from precursor gel powdes[J].Journal of the American Ceramic Society,1990,73(9):2736-2739.
[34] 袁建君,刘智恩,韩玉.溶胶-凝胶法制备莫来石晶须[J].硅酸盐学报,1996,24(3):342-346.
[35] Kong L B,Huang H,Zhang T S,et al.Growth of mullite whiskers in mechanochemically activated oxides doped with WO3[J].Journal of the European Ceramic Society,2003,23(13):2257-2264.
[36] Kong L B,Chen Y Z,Zhang T S.Effect of alkaline-earth oxides on phase formation and morphology development of mulite ceramics[J].Ceramics International,2004,30(7):1319-1323.
[37] 袁致涛,王泽红,韩跃新,等.用石膏合成超细硫酸钙晶须的研究[J].中国矿业,2005,14(11):30-33.
[38] 吕通建,于洋,范平,等.碱式硫酸镁晶须增强阻燃聚丙烯的研究[J].中国塑料,2001,15(9):66-68.
[39] 陶国良,龚方红,丁家红.镁盐晶须填充改性聚丙烯材料研究[J].中国塑料,2003,17(12):45-48.