饲料及畜产品中激素残留检测方法研究进展
|
摘要
随着养殖业与畜牧业的快速发展,各种激素、饲料添加剂被广泛使用,而饲料及畜产品中激素残留会对环境和人体健康产生影响。因此,对饲料及畜产品中激素残留检测方法的研究尤为重要。文章综述了饲料及畜产品中激素残留检测技术。
With the fast development of livestock and animal husbandry,a variety of hormones and feed additives were widely used,and harmful to public health and environment. Therefore,it was particularly important that the detection methods of hormone residues were established in feeds and animal products. This paper reviewed the detection methods of hormone in feeds and animal products.
With the fast development of livestock and animal husbandry,a variety of hormones and feed additives were widely used,and harmful to public health and environment. Therefore,it was particularly important that the detection methods of hormone residues were established in feeds and animal products. This paper reviewed the detection methods of hormone in feeds and animal products.
引文
[1]孙英,王晓玲.西宁市畜产品质量安全检验检测体系的现状及对策[J].上海畜牧兽医通讯,2010(1):90-91.
[2]张华.动物性产品中兽药残留的危害及控制措施概述[J].贵州畜牧兽医,2003,27(6):6-9.
[3]张宏伟,王喆,刘伟.动物性食品中兽药和饲料添加剂残留及其对人体的危害[J].兽药与饲料添加剂,2004,9(4):1-3.
[4]杨春林,李佳峻,胡强,等.高效液相色谱法同时测定饲料中多种酚类抗氧化剂和尼泊金酯类防腐剂[J].中国饲料,2013(1):39-42.
[5]白梓静.高效液相色谱法测定中药复方制剂中有效成分含量的研究[D].陕西:延安大学,2012.
[6]李歆,李小玲.高效液相色谱技术在饲料安全生产中的应用[J].畜牧与饲料科学,2009,30(1):92-94.
[7]李雪,牟光庆,陈历俊,等.高效液相色谱-串联质谱法测定饲料和卧床土中的环境雌激素[J].色谱,2013,31(9):908-913.
[8]Sun H W,Kang Z S,Li H.Determination of nine steroid hormone residues in beef samples by gel permeation chromatography-solid phase extraction-rapid resolution Liquid Chromatography-Mass Spectrometry tandem Mass spectrometry[J].Chinese Journal of Analytical Chemistry,2010,38(9):1 272-1 276.
[9]E Van der H,Bolck Y J C,Beumer B.Full-scan accurate mass selectivity of ultra-performance liquid chromatography combined with time-of-flight and orbitrap mass spectrometry in hormone and veterinary drug residue analysis[J].Journal of the American Society for Mass Spectrometry,2009,20(3):451-463.
[10]曾东平,林翠萍,曾振灵.气相色谱-质谱法检测猪肌肉中8种性激素的残留[J].中国农业科学,2008,41(9):2 776-2 782.
[11]Zeng D P,Lin C P,Zeng Z L.Multi-Residue Determination of Eight Anabolic Steroids by GC-MS in Muscle Tissues from Pigs[J].Agricultural Sciences in China,2010,9(2):306-312.
[12]庞军,刘文红,宋合兴.高效毛细管电泳法同时检测饲料中六种抗氧化剂[J].中国饲料,2013(8):40-42.
[13]唐建设,项丽.毛细管电泳在农药残留检测上的应用[J].分析测试技术与仪器,2005(3):215-220.
[14]王宇,沈玉栋,雷红涛,等.免疫分析标记技术研究进展[J].食品工业科技,2007,28(10):221-225.
[15]刘红菊,闫冲,刘宏果.反相高效液相色谱法同时测定饲料中的10种性激素[J].中国饲料,2010(18):34-36.
[16]李兰,索德成,杜洪鸽.高效液相色谱法同时测定饲料中5种糖皮质激素方法研究[J].农产品质量与安全,2010(2):35-37.
[17]卢艳芬,周莹,丑亚琴,等.固相萃取-高效液相色谱法测定畜禽肉中氯霉素残留量[J].中国卫生检验杂志,2008(1):57-59.
[18]Fan Y B,Yin Y M,Jiang W B,et al.Simultaneous determination of ten steroid hormones in animal origin food by matrix solidphase dispersion and liquid chromatography-electrospray tandemass spectrometry[J].Food Chemistry,2014,142(1):170-177.
[19]张毅,蓝芳,张峰,等.液相色谱-串联质谱法测定谷物类饲料中的41种激素[J].色谱,2011,29(6):523-534.
[20]张文刚,李丹妮,严凤,等.高效液相色谱-串联质谱法测定饲料中玉米赤霉醇类药物[J].分析实验室,2010(29):250-253.
[21]潘云山,聂建荣,朱铭立,等.高效液相色谱串联三重四极杆质谱检测饲料中10种β-受体激动剂[J].广东农业科学,2010(11):252-254,270.
[22]Kaklamanos G,Theodoridis G A,Dabalis T.Determination of anabolic steroids in bovine serum by liquid chromatography-tandem mass spectrometry[J].Journal of Chromatography B,2011,879(2):225-229.
[23]Yang Y,Shao B,Zhang J.Determination of the residues of 50 anabolic hormones in muscle,milk and liver by very-high-pressure liquid chromatography-electrospray ionization tandem mass spectrometry[J].Journal of Chromatography B,2009,877(5):489-496.
[24]李胜,贺利民,陈建新.气相色谱-质谱法测定饲料中莱克多巴胺[J].广东轻工职业技术学院学报,2006(2):11-13.
[25]杨柳,路苹,杨凯.乳牛饲料中邻苯二甲酸酯类环境激素的测定方法研究[J].中国畜牧兽医,2009,36(12):181-186.
[26]林维宣,田苗,董伟峰.固相萃取-气相色谱/质谱法同时检测动物组织中多种β-兴奋剂残留量的研究[J].动物医学进展,2010,31(1):1-4.
[27]Zeng D P,Lin C P,Zeng Z L,et al.Multi-residue determination of eight anabolic steroids by GC-MS in muscle tissues from pigs[J].Agricultural Sciences in China,2010,9(2):306-312.
[28]张敬敬,曹小妹,高文惠.高效毛细管电泳法分离分析畜产品中β-受体激动剂残留[J].畜牧与兽医,2012(9):60-62.
[29]段建平,陈红青,陈颖,等.毛细管区带电泳法同时测定饲料中西马特罗、盐酸克伦特罗和沙丁胺醇[J].色谱,2005,23(3):261-263.
[30]林杰,黄晓蓉,郑晶,等.放射免疫法快速检测饲料中磺胺类药物残留[J].中国饲料,2006(10):32-33.
[31]周浩,李俊霞,杨红,等.饲料中四环素类抗生素的放射免疫分析[J].中国饲料,2011(11):29-31.
[32]李瑞园,毛丽莎,刘红河,等.饲料中己烯雌酚定量的酶联免疫吸附测定法[J].职业与健康,2011(9):990-991.
[33]徐新慧,晏猛,符锋,等.郑州某粮库小麦中玉米赤霉烯酮含量的检测[J].动物医学进展,2012,33(4):59-62.
[34]贾涛,魏秀莲,王有月.酶联免疫法检测饲料中莱克多巴胺[J].饲料研究,2008(4):39-42.
[35]何明祥.沙丁胺醇时间分辨荧光免疫分析检测技术的研究[J].长江大学学报(自然科学版)农学卷,2009(1):33-37,111-112.
[36]王超,李志雄,林冠峰,等.时间分辨荧光免疫分析法测定莱克多巴胺[J].中国食品卫生杂志,2011,23(5):438-441.
[37]Shen J Z,Zhang Z,Yao Y,et al.Time-resolved fluoroimmunoassay for ractopamine in swine tissue[J].Analytical and Bioanalytical Chemistry.2007,38(4):1 561-1 564.
[38]李细芬.盐酸克伦特罗化学发光酶免疫分析方法的研究[D].天津:天津科技大学,2010.
[39]卢江,许杨,楚金申,等.化学发光酶免疫法检测玉米中玉米赤霉烯酮[J].食品与发酵工业,2011,37(5):160-165.
[2]张华.动物性产品中兽药残留的危害及控制措施概述[J].贵州畜牧兽医,2003,27(6):6-9.
[3]张宏伟,王喆,刘伟.动物性食品中兽药和饲料添加剂残留及其对人体的危害[J].兽药与饲料添加剂,2004,9(4):1-3.
[4]杨春林,李佳峻,胡强,等.高效液相色谱法同时测定饲料中多种酚类抗氧化剂和尼泊金酯类防腐剂[J].中国饲料,2013(1):39-42.
[5]白梓静.高效液相色谱法测定中药复方制剂中有效成分含量的研究[D].陕西:延安大学,2012.
[6]李歆,李小玲.高效液相色谱技术在饲料安全生产中的应用[J].畜牧与饲料科学,2009,30(1):92-94.
[7]李雪,牟光庆,陈历俊,等.高效液相色谱-串联质谱法测定饲料和卧床土中的环境雌激素[J].色谱,2013,31(9):908-913.
[8]Sun H W,Kang Z S,Li H.Determination of nine steroid hormone residues in beef samples by gel permeation chromatography-solid phase extraction-rapid resolution Liquid Chromatography-Mass Spectrometry tandem Mass spectrometry[J].Chinese Journal of Analytical Chemistry,2010,38(9):1 272-1 276.
[9]E Van der H,Bolck Y J C,Beumer B.Full-scan accurate mass selectivity of ultra-performance liquid chromatography combined with time-of-flight and orbitrap mass spectrometry in hormone and veterinary drug residue analysis[J].Journal of the American Society for Mass Spectrometry,2009,20(3):451-463.
[10]曾东平,林翠萍,曾振灵.气相色谱-质谱法检测猪肌肉中8种性激素的残留[J].中国农业科学,2008,41(9):2 776-2 782.
[11]Zeng D P,Lin C P,Zeng Z L.Multi-Residue Determination of Eight Anabolic Steroids by GC-MS in Muscle Tissues from Pigs[J].Agricultural Sciences in China,2010,9(2):306-312.
[12]庞军,刘文红,宋合兴.高效毛细管电泳法同时检测饲料中六种抗氧化剂[J].中国饲料,2013(8):40-42.
[13]唐建设,项丽.毛细管电泳在农药残留检测上的应用[J].分析测试技术与仪器,2005(3):215-220.
[14]王宇,沈玉栋,雷红涛,等.免疫分析标记技术研究进展[J].食品工业科技,2007,28(10):221-225.
[15]刘红菊,闫冲,刘宏果.反相高效液相色谱法同时测定饲料中的10种性激素[J].中国饲料,2010(18):34-36.
[16]李兰,索德成,杜洪鸽.高效液相色谱法同时测定饲料中5种糖皮质激素方法研究[J].农产品质量与安全,2010(2):35-37.
[17]卢艳芬,周莹,丑亚琴,等.固相萃取-高效液相色谱法测定畜禽肉中氯霉素残留量[J].中国卫生检验杂志,2008(1):57-59.
[18]Fan Y B,Yin Y M,Jiang W B,et al.Simultaneous determination of ten steroid hormones in animal origin food by matrix solidphase dispersion and liquid chromatography-electrospray tandemass spectrometry[J].Food Chemistry,2014,142(1):170-177.
[19]张毅,蓝芳,张峰,等.液相色谱-串联质谱法测定谷物类饲料中的41种激素[J].色谱,2011,29(6):523-534.
[20]张文刚,李丹妮,严凤,等.高效液相色谱-串联质谱法测定饲料中玉米赤霉醇类药物[J].分析实验室,2010(29):250-253.
[21]潘云山,聂建荣,朱铭立,等.高效液相色谱串联三重四极杆质谱检测饲料中10种β-受体激动剂[J].广东农业科学,2010(11):252-254,270.
[22]Kaklamanos G,Theodoridis G A,Dabalis T.Determination of anabolic steroids in bovine serum by liquid chromatography-tandem mass spectrometry[J].Journal of Chromatography B,2011,879(2):225-229.
[23]Yang Y,Shao B,Zhang J.Determination of the residues of 50 anabolic hormones in muscle,milk and liver by very-high-pressure liquid chromatography-electrospray ionization tandem mass spectrometry[J].Journal of Chromatography B,2009,877(5):489-496.
[24]李胜,贺利民,陈建新.气相色谱-质谱法测定饲料中莱克多巴胺[J].广东轻工职业技术学院学报,2006(2):11-13.
[25]杨柳,路苹,杨凯.乳牛饲料中邻苯二甲酸酯类环境激素的测定方法研究[J].中国畜牧兽医,2009,36(12):181-186.
[26]林维宣,田苗,董伟峰.固相萃取-气相色谱/质谱法同时检测动物组织中多种β-兴奋剂残留量的研究[J].动物医学进展,2010,31(1):1-4.
[27]Zeng D P,Lin C P,Zeng Z L,et al.Multi-residue determination of eight anabolic steroids by GC-MS in muscle tissues from pigs[J].Agricultural Sciences in China,2010,9(2):306-312.
[28]张敬敬,曹小妹,高文惠.高效毛细管电泳法分离分析畜产品中β-受体激动剂残留[J].畜牧与兽医,2012(9):60-62.
[29]段建平,陈红青,陈颖,等.毛细管区带电泳法同时测定饲料中西马特罗、盐酸克伦特罗和沙丁胺醇[J].色谱,2005,23(3):261-263.
[30]林杰,黄晓蓉,郑晶,等.放射免疫法快速检测饲料中磺胺类药物残留[J].中国饲料,2006(10):32-33.
[31]周浩,李俊霞,杨红,等.饲料中四环素类抗生素的放射免疫分析[J].中国饲料,2011(11):29-31.
[32]李瑞园,毛丽莎,刘红河,等.饲料中己烯雌酚定量的酶联免疫吸附测定法[J].职业与健康,2011(9):990-991.
[33]徐新慧,晏猛,符锋,等.郑州某粮库小麦中玉米赤霉烯酮含量的检测[J].动物医学进展,2012,33(4):59-62.
[34]贾涛,魏秀莲,王有月.酶联免疫法检测饲料中莱克多巴胺[J].饲料研究,2008(4):39-42.
[35]何明祥.沙丁胺醇时间分辨荧光免疫分析检测技术的研究[J].长江大学学报(自然科学版)农学卷,2009(1):33-37,111-112.
[36]王超,李志雄,林冠峰,等.时间分辨荧光免疫分析法测定莱克多巴胺[J].中国食品卫生杂志,2011,23(5):438-441.
[37]Shen J Z,Zhang Z,Yao Y,et al.Time-resolved fluoroimmunoassay for ractopamine in swine tissue[J].Analytical and Bioanalytical Chemistry.2007,38(4):1 561-1 564.
[38]李细芬.盐酸克伦特罗化学发光酶免疫分析方法的研究[D].天津:天津科技大学,2010.
[39]卢江,许杨,楚金申,等.化学发光酶免疫法检测玉米中玉米赤霉烯酮[J].食品与发酵工业,2011,37(5):160-165.