活性炭复合滤嘴对卷烟中薄荷醇转移行为的影响
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摘要
【目的】筛选薄荷型卷烟的滤嘴材料。【方法】比较了接装纯醋纤滤嘴和活性炭醋纤滤嘴的薄荷型卷烟,检测其在存放和抽吸过程中烟丝、滤嘴和烟气部分中薄荷醇含量。【结果】1)存放过程中,活性炭复合滤嘴吸附烟丝薄荷醇的能力大于纯醋纤滤嘴,稳定期约为1.3倍;2)抽吸过程中,纯醋纤滤嘴样品薄荷醇向主流烟气的转移能力大于活性炭复合滤嘴样品,存放前转移率为1.9倍,中间平缓期转移率在1.2-1.7倍之间,但随着存放时间变化的幅度较大,转移率最大极差为3.7倍,稳定性较活性炭复合滤嘴差。【结论】对薄荷型卷烟滤嘴材料的选择和改进有指导意义。
To determine the effect of ?lter material on transfer rate of menthol in cigarette, content of menthol in cut tobacco, ?lter tip and mainstream smoke was measured at different storages. The comparison experiments were performed on pure cellulose acetate(CA) ?lter tip and active carbon ?lter tip. Results show that: 1) Adsorption capacity of menthol in active carbon composite ?lter is 1.3 times of that in pure CA ?lter in stable period. 2) The transfer rate of menthol from pure CA ?lter to mainstream smoke was 1.9 times of that from active carbon composite ?lter to mainstream smoke in the period before storage, and 1.2-1.7 times larger in stable period; with extended storage time, the number can be as much as 3.7 times larger. The absorption stability of menthol with active carbon ?lter tip is better than with pure CA ?lter tip. This result has signi?cance for choosing and improving mentholated cigarette ?lter material.
To determine the effect of ?lter material on transfer rate of menthol in cigarette, content of menthol in cut tobacco, ?lter tip and mainstream smoke was measured at different storages. The comparison experiments were performed on pure cellulose acetate(CA) ?lter tip and active carbon ?lter tip. Results show that: 1) Adsorption capacity of menthol in active carbon composite ?lter is 1.3 times of that in pure CA ?lter in stable period. 2) The transfer rate of menthol from pure CA ?lter to mainstream smoke was 1.9 times of that from active carbon composite ?lter to mainstream smoke in the period before storage, and 1.2-1.7 times larger in stable period; with extended storage time, the number can be as much as 3.7 times larger. The absorption stability of menthol with active carbon ?lter tip is better than with pure CA ?lter tip. This result has signi?cance for choosing and improving mentholated cigarette ?lter material.
引文
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[12]刘泽春,谢卫,刘加增,等.卷烟烟碱向主、测流烟气中的转移率[J].烟草科技,2006(11):35-36.LIU Zechun,XIE Wei,LIU Jiazeng,et al.Transfer Efficiency of Nicotine from Cigarette to Smoke[J].Tobacco Science&Technology,2006(11):35-36.
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[14]黄富,刘斌,王平军.特色薄荷型卷烟纸的开发与应用[J].中国造纸,2012(1):42-44.HUANG Fu,LIU Bin,WANG Pingjun.Manufacture of Menthol Cigarette Paper[J].China Pulp&Paper,2012(1):42-44.
[2]林文强,欧亚非,王瑞玲,等.薄荷型卷烟和主流烟气中薄荷醇分析及其转移的研究[J].化学研究与应用,2010,22(9):1122-1125.LIN Wenqiang,OU Yafei,WANG Ruiling,et al.Analysis of menthol in mentholated cigarettes and mainstream smoke and determination of transfer rate in smoke[J].Chemical Research and Applicationg,2010,22(9):1122-1125.
[3]黄泳彤,谢涛,徐畅.填充柱气相色谱法测定卷烟及烟气中的薄荷醇[J].烟草科技,2003(7):27229.HUANG Yongtong,XIE Tao,XU Chang.Determination of Menthol in Cigarette and Smoke by Packed Column GC Method[J].Tobacco Science&Technology,2003(7):27229.
[4]刘立全,王月霞,邵国泉,等.薄荷卷烟生产技术进展[J].烟草科技,1993(5):528.LIU Liquan,WANG Yuexia,SHAO Guoquan,et al.Progress in mint cigarettes production technology[J].Tobacco Science&Technology,1993(5):528.
[5]田书霞,白若石,杨振民,等.薄荷-茶香型卷烟香气风格的应用研究[J].香料香精化妆品,2015(1):23-27.TIAN Shuxia,BAI Ruoshi,YANG Zhenmin,et al.Study on the Aroma Profile of Menthol-Tea Cigarettes[J].Flavour Fragrance Cosmetics,2015(1):23-27.
[6]张悠金,金闻博.烟用香料香精[M].合肥:中国科技大学出版社,1996.ZHANG Youjin,JIN Wenbo.Cigarette flavour[M].Hefei:China university of science and technology press,1996.
[7]宋瑜冰,谢剑平,宗永立,等.薄荷醇在卷烟中转移行为的控制及检测研究综述[J].香料香精化妆品,2005(3):25-28.SONG Yubing XIE Jianping ZONG Yongl,et al.Summary of Transfer Control and Determination Research of Menthol in Cigarette[J].Flavour Fragrance Cosmetics,2005(3):25-28.
[8]Hee Jin Jang.A study on menthol migration patterns in different mentholated cigarettes[J].Journal of the Korea Society of Tobacco Science,2001,23(1):77281.
[9]Brozinski M,Doulbero U,Lipp G.Research into the distribution of menthol in the tobacco,filter and menthol cigarettes[J].Beitr.Tabakforsch,1972(3):124-130.
[10]宋瑜冰,宗永立,谢剑平,等.一些酯类香料在卷烟中的转移研究[J].烟草科技,2005(6):22-25.SONG Yubing,ZONG Yongli,XIE Jianping,et al.Transfer of some Ester Flavors in Cigarette[J].Tobacco Science&Technology,2005(6):22-25.
[11]宋瑜冰,宗永立,李炎强,等.一些酯类香料在卷烟加香后散失率研究[J].烟草科技,2007(6):1-6.SONG Yubing,ZONG Yongli,LI Yanqiang,et al.A study on dissipation rates of ester flavors in cigarettes[J].Tobacco Science&Technology,2007(6):1-6.
[12]刘泽春,谢卫,刘加增,等.卷烟烟碱向主、测流烟气中的转移率[J].烟草科技,2006(11):35-36.LIU Zechun,XIE Wei,LIU Jiazeng,et al.Transfer Efficiency of Nicotine from Cigarette to Smoke[J].Tobacco Science&Technology,2006(11):35-36.
[13]黄龙.卷烟及烟气中薄荷醇的毛细管色谱分析[J].烟草科技,2007(4):32-35.HUANG Long.Capillary Gas Chromatographic Determination of Menthol in Cigarette and Smoke[J].Tobacco Science&Technology,2007(4):32-35.
[14]黄富,刘斌,王平军.特色薄荷型卷烟纸的开发与应用[J].中国造纸,2012(1):42-44.HUANG Fu,LIU Bin,WANG Pingjun.Manufacture of Menthol Cigarette Paper[J].China Pulp&Paper,2012(1):42-44.