Nb-16Si-22Ti-2Cr-2Al-2Hf-xFe合金热加工性能研究
|
摘要
通过对真空非自耗电弧炉制备的Nb-16Si-22Ti-2Cr-2Al-2Hf-xFe(x=0, 1,2, 3, 5, at%) 5种铌硅合金的热变形行为进行探索和研究,分别绘制了5种铌硅合金的热加工图,并分析了不同变形参数下合金显微组织的变化,确定了各合金的最佳变形工艺范围,为后续铌硅合金的设计及热加工研究提供了理论依据。合金耗散效率因子η的最大值出现在低应变速率及高温区域;最小值则出现在低温和高应变速率区域。不同Fe含量合金的热加工图中均存在失稳变形区,主要分布区域与低耗散效率因子区重合,同时,失稳区晶粒明显拉长,晶界出现弯曲扭折现象,晶粒大小分布不均匀,发生了局部塑性流动。稳定变形区存在链状的动态再结晶组织,细小的再结晶晶粒沿晶界分布,随着变形温度的升高和应变速率的降低,动态再结晶晶粒的尺寸增大。
Through the research of hot deformation behavior of Nb-16Si-22Ti-2Cr-2Al-2Hf-xFe(x=0, 1,2,3, 5) alloys, the hot working diagrams of these alloys were made, which would provide a theoretical basis for subsequent design and hot working study of Nb-Si alloys.The maximum dissipative efficiency factor η appears in the region of low strain rate and high temperature; the minimum appears in low temperature and high strain rate region. There are unstable regions in the thermal processing map of the alloys with different Fe contents,mainly distributed in the regions with high strain rate and low temperature, coinciding with the low dissipative efficiency factor regions.The grains in the unstable regions are obviously elongated and the grain boundaries are curved. The grain size is uneven and local plastic flow occurs. The dynamic recrystallization structure exists in the stable deformation zone as well as the fine recrystallized grain is distributed along the grain boundary. With the increase of the deformation temperature and the decrease of the strain rate, the size of the dynamic recrystallization grain increases.
Through the research of hot deformation behavior of Nb-16Si-22Ti-2Cr-2Al-2Hf-xFe(x=0, 1,2,3, 5) alloys, the hot working diagrams of these alloys were made, which would provide a theoretical basis for subsequent design and hot working study of Nb-Si alloys.The maximum dissipative efficiency factor η appears in the region of low strain rate and high temperature; the minimum appears in low temperature and high strain rate region. There are unstable regions in the thermal processing map of the alloys with different Fe contents,mainly distributed in the regions with high strain rate and low temperature, coinciding with the low dissipative efficiency factor regions.The grains in the unstable regions are obviously elongated and the grain boundaries are curved. The grain size is uneven and local plastic flow occurs. The dynamic recrystallization structure exists in the stable deformation zone as well as the fine recrystallized grain is distributed along the grain boundary. With the increase of the deformation temperature and the decrease of the strain rate, the size of the dynamic recrystallization grain increases.
引文
[1]BewlayBP,JacksonMR,ZhaoJCetal.Metallurgicaland Material Transaction A[J], 2003, 34A:2044
[2] Zhao J C. MRS Bulletin[J]. 2003, 28(9):622
[3] Zhang Xiaoming(张小明). Materials China(中国材料进展)[J],2005, 24(2):3
[4]QuShiyu(曲士昱).ThesisforDoctorate(博士论文)[D].Beijing:AVICBeijingInstituteofAeronauticalMaterials,1998
[5] Miura S, Ohkubo K, Mohri T. Intermetallics[J], 2007, 15(5-6):783
[6]GaoLimei(高丽梅),GuoXiping(郭喜平).ThesisforMaster Degree(硕士论文)[D].Xi’an:NorthwesternPolytechnical University, 2005
[7] Huang Youlin(黄有林), Wang Jianbo(王建波), Ling Xueshi(凌学士)etal.MaterialsReview(材料导报)[J],2008,22(S3):173
[8]ZengWeidong(曾卫东),ZhouYigang(周义刚),ZhouJun(周军)et al. Rare Metal Materials and Engineering(稀有金属材料与工程)[J], 2006, 35(5):673
[9] Bao Ruqiang(鲍如强), Huang Xu(黄旭), Cao Chunxiao(曹春晓)et al. Materials Review(材料导报)[J], 2004, 18(7):26
[10]PrasadYV,GegelHL,DoraiveluSMetal.Metallurgical and Materials Transactions A[J], 1984, 15(10):1883
[11] Ma Xiong(马雄), Zeng Weidong(曾卫东), Sun Yu(孙宇)et al.RareMetalMaterialsandEngineering(稀有金属材料与工程)[J], 2010, 39(5):756
[12]YouLi(尤力),SongXiping(宋西平).ActaMetallurgica Sinica(金属学报)[J], 2008, 44(11):1310
[13]MuSiguo(慕思国).ThesisforDoctorate(博士论文)[D].Changsha:Central South University, 2008
[14]SivakesavamO,RAOIS,PrasadYV.MaterialsScience&Technology[J], 1993, 9(9):805
[2] Zhao J C. MRS Bulletin[J]. 2003, 28(9):622
[3] Zhang Xiaoming(张小明). Materials China(中国材料进展)[J],2005, 24(2):3
[4]QuShiyu(曲士昱).ThesisforDoctorate(博士论文)[D].Beijing:AVICBeijingInstituteofAeronauticalMaterials,1998
[5] Miura S, Ohkubo K, Mohri T. Intermetallics[J], 2007, 15(5-6):783
[6]GaoLimei(高丽梅),GuoXiping(郭喜平).ThesisforMaster Degree(硕士论文)[D].Xi’an:NorthwesternPolytechnical University, 2005
[7] Huang Youlin(黄有林), Wang Jianbo(王建波), Ling Xueshi(凌学士)etal.MaterialsReview(材料导报)[J],2008,22(S3):173
[8]ZengWeidong(曾卫东),ZhouYigang(周义刚),ZhouJun(周军)et al. Rare Metal Materials and Engineering(稀有金属材料与工程)[J], 2006, 35(5):673
[9] Bao Ruqiang(鲍如强), Huang Xu(黄旭), Cao Chunxiao(曹春晓)et al. Materials Review(材料导报)[J], 2004, 18(7):26
[10]PrasadYV,GegelHL,DoraiveluSMetal.Metallurgical and Materials Transactions A[J], 1984, 15(10):1883
[11] Ma Xiong(马雄), Zeng Weidong(曾卫东), Sun Yu(孙宇)et al.RareMetalMaterialsandEngineering(稀有金属材料与工程)[J], 2010, 39(5):756
[12]YouLi(尤力),SongXiping(宋西平).ActaMetallurgica Sinica(金属学报)[J], 2008, 44(11):1310
[13]MuSiguo(慕思国).ThesisforDoctorate(博士论文)[D].Changsha:Central South University, 2008
[14]SivakesavamO,RAOIS,PrasadYV.MaterialsScience&Technology[J], 1993, 9(9):805