X射线衍射技术在炭材料研究中的应用
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摘要
X射线衍射(XRD)是一种快速有效的研究炭材料微观结构的分析方法,近年来,得到越来越广泛的应用。简要介绍了XRD分析技术应用于炭材料中的物相分析、晶体结构及取向分析、残余应力分析及小角散射分析的基本原理,并综述了国内外学者采用这种分析技术对炭材料的研究应用。
X-ray diffraction(XRD) technology is shown as a fast, reliable and suitable method for investigating microstructure of carbon materials and has been widely used in the study of carbon materials in recent years. The principle of phase analysis, structure and orientation analysis of crystals, residual stress analysis and small-angle scattering analysis based on XRD are briefly introduced. The extensive applications of XRD related to carbon materials were summarized.
X-ray diffraction(XRD) technology is shown as a fast, reliable and suitable method for investigating microstructure of carbon materials and has been widely used in the study of carbon materials in recent years. The principle of phase analysis, structure and orientation analysis of crystals, residual stress analysis and small-angle scattering analysis based on XRD are briefly introduced. The extensive applications of XRD related to carbon materials were summarized.
引文
[1] W.L布喇格,杨润殷译.X射线分析的发展[M].北京:科学出版社,1988. 1-20.
[2] Quanlin Shi, Botao Qin, Qiang Bi, et al. An experimental study on the effect of igneous intrusions on chemical structure and combustion characteristics of coal in Daxing Mine, China[J]. Fuel, 2018, 226:307-315.
[3] H.Takagi, K.Maruyama, N.Yoshizawa, et al. XRD analysis of carbon stacking structure in coal during heat treatment[J].Fuel, 2004, 83:2427-2433.
[4] AAXiaodong Zhang, Shuo Zhang, Pengpeng Li,et al. Investigation on solubility of multicomponents from semianthracite coal and its effect on coal structure by Fourier transform infrared spectroscopy and X-ray diffraction[J].Fuel Processing Technology,2018,174:123-131.
[5] Qing-an Xiong, Jiazhou Li, Shuai Guo, et al. Ash fusion characteristics during co-gasification of biomass and petroleum coke[J].Bioresource Technology,2018,257:1-6.
[6] Firuze Okyay O.ner, AlpYürüm, YudaYürüm. Structural characterization of semicokes produced from the pyrolysis of petroleum pitches[J]. Journal of Analytical and Applied Pyrolysis,2015,111:15-26.
[7]樊文克. KOH对煤及石油焦碳微晶结构和气化活性影响研究[D].上海:华东理工大学,2017.
[8] Tamás Ungár,JenO.. Gubicza,Gábor Ribárik,et al.Microstructure of carbon blacks determined by X-ray diffraction profile analysis[J].Carbon, 2002, 40:929-937.
[9] Alok P.S. Chauhan, Komal Chawla. Comparative studies onGraphiteandCarbonBlackpowders,andtheir dispersions[J].JournalofMolecularLiquids,2016,221:292-297.
[10] HuiZhu, XuankeLi, ZhijunDong, et al. Effect of carbon fiber crystallite size on the formation of hafnium carbide coating and the mechanism of the reaction of hafnium with carbon fibers[J].Carbon,2017,115:640-648.
[11]易静,袁观明,李轩科,等.大直径沥青基炭纤维/ABS树脂高导热复合材料的制备与表征[J].新型炭材料,2015,30(1):63-69.
[12] Yi Li, Chun Li, Hui Qi. Mesoporous activated carbon from corn stalk core for lithium ion batteries[J]. Chemical Physics, 2018,506:10-16.
[13] AndreavLazzarini, Andrea Piovano, Riccardo Pellegrini,et al. Graphitization of activated carbons:a molecularlevel investigation by INS, DRIFT, XRD and Raman techniques[J]. Physics Procedia,2016,85:20-26.
[14]S.B.Lyubchik,L.Ya.Galushko,A.M.Rego,etal.Intercalation as an approach to the activated carbon preparation from Ukrainian anthracites[J].Journal of Physics and Chemistry of Solids. 2004, 65:127-132.
[15] Hassan Soleimani, Mirza Khurram Baig, NoorhanaYahyaa,et al. Impact of carbon nanotubes based nanofluid on oil recovery efficiency using core flooding[J]. Results in Physics,2018,9:39-48.
[16] Rajveer Singh Rajaura, Subodh Srivastava, Preetam Kumar Sharma,et al. Structural and surface modification of carbon nanotubes for enhanced hydrogen storage density[J]. NanoStructures&Nano-Objects.2018,14:57-65.
[17] L.Stobinski, B.Lesiak, A.Malolepszy, et al. Graphene oxide and reduced graphene oxide studied by the XRD, TEM and electron spectroscopy methods[J]. Journal of Electron Spectroscopy and Related Phenomena,2014,195:145-154.
[18]XianjueChen,XiaomeiDeng,NaYeonKim,etal.Graphitization of graphene oxide films under pressure[J].Carbon,2018,132:294-303.
[19]杨于兴.X射线衍射分析[M].上海:上海交通大学出版社,1994.105.
[20]钱湛芬.炭素工艺学[M].北京:冶金工业出版社,1996. 165-166.
[21]王曾辉,高晋生.碳素材料[M].上海:华东工学院出版社,1991.54
[22]贾琨,李克训,张泽奎等.石墨烯/碳纳米管复合材料的微波吸收性能研究[J].功能材料,2018, 49(2):2136-2140.
[23] Wangjia Tang, Jianbo Wu, Xiuli Wang, et al. Integrated carbonnanospheresarraysasanodematerialsfor boostedsodiumionstorage[J].GreenEnergy&Environment,2018,3:50-55.
[24] J.Díaz-Terán, D.M.Nevskaia, J.L.G.Fierro, et al. Study of a lignocellulosic material with KOH by XPS and XRD.Microporous and Mesoporous Materials[J]. 2003,60:173-181.
[25]王培铭,许乾慰.材料研究方法[M].北京:科学出版社,2005.98.
[26]刘粤惠,刘平安.X射线衍射分析原理与应用[M].北京:化学工业出版社,2003.122.
[27] Andréda S. Machado,AndréS. Mexias, Antonio C.F.Vilela, et al. Study of coal, char and coke fines structures and their proportions in the off-gas blast furnace samples by X-ray diffraction[J].Fuel,2013,114:224-228.
[28]SeungHunHuh.X-raydiffractionofmulti-layer graphenes:Instant measurement and determination of the number of layers[J]. Carbon,2014,78:617-628.
[29]朱亚明,赵雪飞,高丽娟,等.煤系针状焦微晶结构的XRD与Raman分峰拟合定量研究[J].光谱学与光谱分析, 2017, 37(6):1919-1924.
[30]汪树军.X射线衍射法对树脂炭微观结构测试分析[J].炭素技术, 2000, 111(6):8-12.
[31] Hishiyama.Y and Nakamura.M, X-ray diffraction in orientedcarbonfilmswithturbostraticstructure[J]. Carbon,1995, 33:1399-1403.
[32]张硕,张小东,杨延辉等.溶剂萃取下构造煤的XRD结构演化特征[J].光谱学与光谱分析, 2017,37(10):3220-3224.
[33]李树棠.晶体X射线衍射基础[M].北京:冶金工业出版社,1990.91.
[34] L.Dobiaásˇová, V.Stary, P.Glogar, et al, Analysisi of carbon fibers and carbon composites by asymmetric X-ray diffraction technique[J]. Carbon,1999, 37:421-425.
[35]宋俊凯,黄小波,高玉魁.残余应力测试分析技术[J].表面技术, 2016, 45(4):75-82.
[36] Sam Zhang,Hong Xie, Xianting Zeng, et al, Residual stress characterization of diamond-like carbon coatings by an X-ray diffraction method[J]. Surface and Coatings Technology, 1999,122:219-224
[37] Yongqing Fu, Hejun, Du, Chang Q. Sun. Interfacial structure,residualstressandadhesionofdiamond coatingsdepositedontitanium[J].ThinSolid Films,2003,424:107-114.
[38]孟昭富.小角X射线散射理论及应用[M].吉林:吉林科学技术出版社,1995.
[39]朱卫华,丁万平,林建伟,等.柔性石墨微孔孔径分布X射线小角散射实验测定[J].江西科学,2005,23(5):552-558
[40]李志宏,吴东,孙予罕,等.小角X射线散射模糊数据解析方法[J].煤炭转化,2001,24(1):11-14.
[41]魏彦茹.小角X射线散射若干方法研究[D].安徽大学,2017.
[42]周怡然,肖瑛阁,何烨,等.聚丙烯腈原丝预氧化过程中长周期结构的生成[J].材料导报:纳米与新材料专辑,2017(1):305-308.
[43] Jienan Pan, Qinghe Niu, Kai Wang, et al. The closed pores of tectonically deformed coal studied by small-angle X-ray scattering and liquid nitrogen adsorption[J].Microporous&Mesoporous Materials, 2016, 224:245-252.
[44]戚威,夏汇浩,张灿,等.基于SAXS方法的核石墨微孔结构的温度影响[J].核技术, 2017, 40(10):13-19.
[2] Quanlin Shi, Botao Qin, Qiang Bi, et al. An experimental study on the effect of igneous intrusions on chemical structure and combustion characteristics of coal in Daxing Mine, China[J]. Fuel, 2018, 226:307-315.
[3] H.Takagi, K.Maruyama, N.Yoshizawa, et al. XRD analysis of carbon stacking structure in coal during heat treatment[J].Fuel, 2004, 83:2427-2433.
[4] AAXiaodong Zhang, Shuo Zhang, Pengpeng Li,et al. Investigation on solubility of multicomponents from semianthracite coal and its effect on coal structure by Fourier transform infrared spectroscopy and X-ray diffraction[J].Fuel Processing Technology,2018,174:123-131.
[5] Qing-an Xiong, Jiazhou Li, Shuai Guo, et al. Ash fusion characteristics during co-gasification of biomass and petroleum coke[J].Bioresource Technology,2018,257:1-6.
[6] Firuze Okyay O.ner, AlpYürüm, YudaYürüm. Structural characterization of semicokes produced from the pyrolysis of petroleum pitches[J]. Journal of Analytical and Applied Pyrolysis,2015,111:15-26.
[7]樊文克. KOH对煤及石油焦碳微晶结构和气化活性影响研究[D].上海:华东理工大学,2017.
[8] Tamás Ungár,JenO.. Gubicza,Gábor Ribárik,et al.Microstructure of carbon blacks determined by X-ray diffraction profile analysis[J].Carbon, 2002, 40:929-937.
[9] Alok P.S. Chauhan, Komal Chawla. Comparative studies onGraphiteandCarbonBlackpowders,andtheir dispersions[J].JournalofMolecularLiquids,2016,221:292-297.
[10] HuiZhu, XuankeLi, ZhijunDong, et al. Effect of carbon fiber crystallite size on the formation of hafnium carbide coating and the mechanism of the reaction of hafnium with carbon fibers[J].Carbon,2017,115:640-648.
[11]易静,袁观明,李轩科,等.大直径沥青基炭纤维/ABS树脂高导热复合材料的制备与表征[J].新型炭材料,2015,30(1):63-69.
[12] Yi Li, Chun Li, Hui Qi. Mesoporous activated carbon from corn stalk core for lithium ion batteries[J]. Chemical Physics, 2018,506:10-16.
[13] AndreavLazzarini, Andrea Piovano, Riccardo Pellegrini,et al. Graphitization of activated carbons:a molecularlevel investigation by INS, DRIFT, XRD and Raman techniques[J]. Physics Procedia,2016,85:20-26.
[14]S.B.Lyubchik,L.Ya.Galushko,A.M.Rego,etal.Intercalation as an approach to the activated carbon preparation from Ukrainian anthracites[J].Journal of Physics and Chemistry of Solids. 2004, 65:127-132.
[15] Hassan Soleimani, Mirza Khurram Baig, NoorhanaYahyaa,et al. Impact of carbon nanotubes based nanofluid on oil recovery efficiency using core flooding[J]. Results in Physics,2018,9:39-48.
[16] Rajveer Singh Rajaura, Subodh Srivastava, Preetam Kumar Sharma,et al. Structural and surface modification of carbon nanotubes for enhanced hydrogen storage density[J]. NanoStructures&Nano-Objects.2018,14:57-65.
[17] L.Stobinski, B.Lesiak, A.Malolepszy, et al. Graphene oxide and reduced graphene oxide studied by the XRD, TEM and electron spectroscopy methods[J]. Journal of Electron Spectroscopy and Related Phenomena,2014,195:145-154.
[18]XianjueChen,XiaomeiDeng,NaYeonKim,etal.Graphitization of graphene oxide films under pressure[J].Carbon,2018,132:294-303.
[19]杨于兴.X射线衍射分析[M].上海:上海交通大学出版社,1994.105.
[20]钱湛芬.炭素工艺学[M].北京:冶金工业出版社,1996. 165-166.
[21]王曾辉,高晋生.碳素材料[M].上海:华东工学院出版社,1991.54
[22]贾琨,李克训,张泽奎等.石墨烯/碳纳米管复合材料的微波吸收性能研究[J].功能材料,2018, 49(2):2136-2140.
[23] Wangjia Tang, Jianbo Wu, Xiuli Wang, et al. Integrated carbonnanospheresarraysasanodematerialsfor boostedsodiumionstorage[J].GreenEnergy&Environment,2018,3:50-55.
[24] J.Díaz-Terán, D.M.Nevskaia, J.L.G.Fierro, et al. Study of a lignocellulosic material with KOH by XPS and XRD.Microporous and Mesoporous Materials[J]. 2003,60:173-181.
[25]王培铭,许乾慰.材料研究方法[M].北京:科学出版社,2005.98.
[26]刘粤惠,刘平安.X射线衍射分析原理与应用[M].北京:化学工业出版社,2003.122.
[27] Andréda S. Machado,AndréS. Mexias, Antonio C.F.Vilela, et al. Study of coal, char and coke fines structures and their proportions in the off-gas blast furnace samples by X-ray diffraction[J].Fuel,2013,114:224-228.
[28]SeungHunHuh.X-raydiffractionofmulti-layer graphenes:Instant measurement and determination of the number of layers[J]. Carbon,2014,78:617-628.
[29]朱亚明,赵雪飞,高丽娟,等.煤系针状焦微晶结构的XRD与Raman分峰拟合定量研究[J].光谱学与光谱分析, 2017, 37(6):1919-1924.
[30]汪树军.X射线衍射法对树脂炭微观结构测试分析[J].炭素技术, 2000, 111(6):8-12.
[31] Hishiyama.Y and Nakamura.M, X-ray diffraction in orientedcarbonfilmswithturbostraticstructure[J]. Carbon,1995, 33:1399-1403.
[32]张硕,张小东,杨延辉等.溶剂萃取下构造煤的XRD结构演化特征[J].光谱学与光谱分析, 2017,37(10):3220-3224.
[33]李树棠.晶体X射线衍射基础[M].北京:冶金工业出版社,1990.91.
[34] L.Dobiaásˇová, V.Stary, P.Glogar, et al, Analysisi of carbon fibers and carbon composites by asymmetric X-ray diffraction technique[J]. Carbon,1999, 37:421-425.
[35]宋俊凯,黄小波,高玉魁.残余应力测试分析技术[J].表面技术, 2016, 45(4):75-82.
[36] Sam Zhang,Hong Xie, Xianting Zeng, et al, Residual stress characterization of diamond-like carbon coatings by an X-ray diffraction method[J]. Surface and Coatings Technology, 1999,122:219-224
[37] Yongqing Fu, Hejun, Du, Chang Q. Sun. Interfacial structure,residualstressandadhesionofdiamond coatingsdepositedontitanium[J].ThinSolid Films,2003,424:107-114.
[38]孟昭富.小角X射线散射理论及应用[M].吉林:吉林科学技术出版社,1995.
[39]朱卫华,丁万平,林建伟,等.柔性石墨微孔孔径分布X射线小角散射实验测定[J].江西科学,2005,23(5):552-558
[40]李志宏,吴东,孙予罕,等.小角X射线散射模糊数据解析方法[J].煤炭转化,2001,24(1):11-14.
[41]魏彦茹.小角X射线散射若干方法研究[D].安徽大学,2017.
[42]周怡然,肖瑛阁,何烨,等.聚丙烯腈原丝预氧化过程中长周期结构的生成[J].材料导报:纳米与新材料专辑,2017(1):305-308.
[43] Jienan Pan, Qinghe Niu, Kai Wang, et al. The closed pores of tectonically deformed coal studied by small-angle X-ray scattering and liquid nitrogen adsorption[J].Microporous&Mesoporous Materials, 2016, 224:245-252.
[44]戚威,夏汇浩,张灿,等.基于SAXS方法的核石墨微孔结构的温度影响[J].核技术, 2017, 40(10):13-19.