二硝酰胺铵(ADN)球形化技术研究进展
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摘要
对二硝酰胺铵(ADN)的球形化技术进行了比较详细的综述。从乳液球形化、喷雾球形化、喷射研磨球形化、超声波球形化、微反应球形化技术及膜乳化结晶新技术等几方面介绍了ADN球形化技术的研究现状,对比了各种技术的优缺点,提出了超声波球形化技术、微反应球形化技术和膜乳化结晶技术是ADN球形化制备技术发展的趋势,并指出了我国ADN球形化技术的发展方向。
Ammonium dinitramide( ADN) spherical technology were reviewed in detail. The research status of ADN spheroidization technology was introduced from aspects of emulsion spheroidization,spray spheroidization,spray grinding sphericity,ultrasonic spheroidization,micro reaction spheroidization and new technology of membrane emulsification and crystallization. Advantages and disadvantages of various technologies were compared. Spheroidization of microspheres,micro-spheres and membrane-emulsified spherulites are the development trend of ADN spheroidization technology.And the development direction of ADN spheroidization technology in China was also proposed.
Ammonium dinitramide( ADN) spherical technology were reviewed in detail. The research status of ADN spheroidization technology was introduced from aspects of emulsion spheroidization,spray spheroidization,spray grinding sphericity,ultrasonic spheroidization,micro reaction spheroidization and new technology of membrane emulsification and crystallization. Advantages and disadvantages of various technologies were compared. Spheroidization of microspheres,micro-spheres and membrane-emulsified spherulites are the development trend of ADN spheroidization technology.And the development direction of ADN spheroidization technology in China was also proposed.
引文
[1]HEINTZ T,PONTIUS H,ANIOL J,et al.Ammonium dinitramide(ADN)-prilling,coating,and characterization[J].Propellants,Explosives,Pyrotechnics,2009,34(3):231-238.
[2]LARSSON A,WINGBORG N.Green propellants based on ammonium dinitramide(ADN)[J].Advances in Spacecraft Technologies,2011:139-156.
[3]HEINTZ T,FUCHS A.Continuous production of spherical ammonium dinitramide particles(ADN-prills)by microreaction technology[C]//The 41st International Annual Conference of ICT.Karlsruhe,Germany,2010.
[4]SKIFS H.Properties regarding handling of ADN[C]//New Energetics Conference.Stockholm,Sweden,2014.
[5]TALAWAR M B.SIVABALAN R,ANNIYAPPAN M,et al.Emerging trends in advanced high energy materials[J].Combustion,Explosion,and Shock Waves,2007,43(1):62-72.
[6]ELDSATER C,DE FLON J,HOLMGREN E,et al.ADN prills:production,characterisation and formulation[C]//The 40th International Annual Conference of ICT.Karlsruhe,Germany,2009.
[7]NAGAMACHI M Y,OLIVEIRA J I S,KAWAMOTO AM,et al.ADN-the new oxidizer around the corner for an environmentally friendly smokeless propellant[J].Journal of Aerospace Technology and Management,2009,1(2):153-160.
[8]TEIPEL U,HEINTZ T,KRAUSE H H.Crystallization of spherical ammonium dinitramide(ADN)particles[J].Propellants,Explosives,Pyrotechnics,2000,25(2):81-85.
[9]LANGLET A,WINGBORG N,OSTMARK H.ADN:a new high performance oxidizer for solid propellants[J].International Journal of Energetic Materials&Chemical Propulsion,1997,4(1/2/3/4/5/6):616-626.
[10]HEINTZ T,PONTIUS H,ANIOL J,et al.ADN-prilling,coating and characterization[C]//The 39th International Annual Conference of ICT.Karlsruhe,Germany:2008.
[11]GUIMONT J.Process for preparing spherical energetic compounds:5801453[P].1998-09-01.
[12]王伯周,张志忠,刘愆,等.ADN合成及应用研究进展[C]//ADN合成与应用研讨会论文集.北京,2006:11-33.WANG B Z,ZHANG Z Z,LIU Q,et al.ADN synthesis and application of research progress[C]//ADN Synthesis and Application Symposium Proceedings.Beijing,2006:11-33.
[13]刘波,刘少武,于慧芳,等.二硝酰胺铵防吸湿技术研究进展[J].化学推进剂与高分子材料,2011,9(6):57-60.LIU B,LIU S W,YU H F,et al.Research progress in anti-hygroscopicity of ammonium dinitramide[J].Chemical Propellants&Polymeric Materials,2011,9(6):57-60.
[14]马跃,张海林.二硝酰胺铵(ADN)球形化工艺研究[J].固体火箭技术,2002,25(2):59-62.MA Y,ZHANG H L.Study on prilling process of ammonium dinitramide(ADN)[J].Journal of Solid Rocket Technology,2002,25(2):59-62.
[15]马跃,张海林.球形二硝酰胺铵研究[J].固体火箭技术,2002,25(1):29-32.MA Y,ZHANG H L.Study on prilled ammonium dinitramide(ADN)[J].Journal of Solid Rocket Technology,2002,25(1):29-32.
[16]黄洪勇.高能氧化剂二硝酰胺铵研究进展[J].上海航天,2005(4):31-35.HUANG H Y.Study progress of ammonium dinitramide[J].Aerospace Shanghai,2005(4):31-35.
[17]RAMASWAMY A L.Energetic-material combustion experiments on propellant formulations containing prilled ammonium dinitramide[J].Combustion,Explosion,and Shock Waves,2000,36(1):119-124.
[18]HIGHSMITH T K,MCLEOD C S,WARDIE R B,et al.Manufacture of thermally-stabilized prilled ammonium dinitramide particles,and process for making the same:US6136115[P].2000-10-24.
[19]WINGBORG N,ANDREASSON S,FLON J D,et al.Development of ADN-based minimum smoke propellants[C]//The 46th AIAA/ASME/SAE/ASEE Joint Propulsion Conference&Exhibit.Nashville,US,2010.
[20]JOHANSSON M,FLON JD,PETTERSON,et al.Spray prilling of ADN and testing of ADN-based solid propellants[C]//The 3rd International Conference on Green Propellants for Space Propulsion.Poitiers,France,2006.
[21]HEINTZ T,REINHARD W,BIRKE C,et al.Particle size adjustment of spherical ammonium dinitramide particles(ADN-prills)produced by emulsion crystallization[C]//The 45th International Annual Conference of ICT.Karlsruhe,Germany,2014.
[22]LANGLET A,JOHANSSON M.Method of producing ADN prills suitable for use in a polymer system:WO99/21794[P].1999-05-06.
[23]LILJEDAHL M,SKARSTIND M,LINDBORG A.Processing of ADN particles[C]//The 46th International Annual Conference of ICT.Karlsruhe,Germany,2015.
[24]LINDBORQ A,LILJEDAHL M,PETERSSON A,et al.Jet Milling of ADN and FOX-12[C]//The 44th International Annual Conference of ICT.Karlsruhe,Germany,2013.
[25]LANGLET A,JOHANSSON M.Method of producing prills of ammonium dinitramide(ADN):WO 99/21793[P].1999-05-06.
[26]HEINTZ T,FUCHS A.Continuous production of spherical ammonium dinitramide particles(ADN-prills)by microreaction technology[C]//The 41st International Annual Conference of ICT.Karlsruhe,Germany,2010.
[27]彭翠枝,郑斌,张培,等.国外二硝酰胺铵的发展现状[J].火炸药学报,2014,37(3):1-5.PENG C Z,ZHENG B,ZHANG P,et al.Current situation of foreign ammonium dinitramide development[J].Chinese Journal of Explosives&Propellants,2014,37(3):1-5.
[28]MANSELL E,EVANS S,MYATT R,et al.Development of the Roxel emulsion mediated spheroidisation technique for ammonium dinitramide(ADN)[C]//The46th International Annual Conference of ICT,Karlsruhe,Germany,2015.
[29]YUAN Q,ARYANTI N,GUTIRREZ G,et al.Enhancing the throughput of membrane emulsification techniques to manufacture functional particles[J].Industrial&Engineering Chemistry Research,2009,48(19):8872-8880.
[30]EGIDI E,GASPARINI G,HOLDICH R G,et al.Membrane emulsification using membranes of regular pore spacing:droplet size and uniformity in the presence of surface shear[J].Journal of Membrane Science,2008,323(2):414-420.
[31]JOHANSSON M,WINGBORG N,JOHANSSON J,et al.ADN is more than particles and formulations-it is a part of future missile propellants[C]//The NDIA Insensitive Munitions&Energetic Materials Technology Symposium.San Diego,US,2013.
[32]HIGHSNITH T K.ADN maunfactory technoiogy[C]//Proceedings 29th International Conference of ICT.Karisruhe,Germany,1998.
[33]CERRI S,BOHN M A.Ageing behaviour of rocket propellant formulations with ADN as oxidizer investigated by DMA,DSC and SEM[C]//The 42th International Annual Conference of ICT.Karlsruhe,Germany,2011.
[34]GETTWERT V,FISCHER S.Aluminized ADN/GAP propellants-formulation and properties[C]//The 44th International Annual Conference of ICT.Karlsruhe,Germany,2013.
[35]李上文,赵风起,高红旭,等.ADN及其推进剂研制的进展[C]//ADN合成与应用研讨会论文集.北京,2006:1-10.LI S W,ZHAO F Q,GAO H X,et al.Development of ADN and its propellant[C]//ADN Synthesis and Application Symposium Proceedings.Beijing,2006:1-10.
[36]任晓雪,赵凤起,郑斌.ADN推进剂的研究发展[J].飞航导弹,2007(12):53-55.
[37]LANDSEM E,TOMAS L.Mechanical properties of smokeless composite rocket propellants based on prilled ammonium dinitramide[J].Propellants,Explosives,Pyrotechnics,2012,37(6):691-698.
[2]LARSSON A,WINGBORG N.Green propellants based on ammonium dinitramide(ADN)[J].Advances in Spacecraft Technologies,2011:139-156.
[3]HEINTZ T,FUCHS A.Continuous production of spherical ammonium dinitramide particles(ADN-prills)by microreaction technology[C]//The 41st International Annual Conference of ICT.Karlsruhe,Germany,2010.
[4]SKIFS H.Properties regarding handling of ADN[C]//New Energetics Conference.Stockholm,Sweden,2014.
[5]TALAWAR M B.SIVABALAN R,ANNIYAPPAN M,et al.Emerging trends in advanced high energy materials[J].Combustion,Explosion,and Shock Waves,2007,43(1):62-72.
[6]ELDSATER C,DE FLON J,HOLMGREN E,et al.ADN prills:production,characterisation and formulation[C]//The 40th International Annual Conference of ICT.Karlsruhe,Germany,2009.
[7]NAGAMACHI M Y,OLIVEIRA J I S,KAWAMOTO AM,et al.ADN-the new oxidizer around the corner for an environmentally friendly smokeless propellant[J].Journal of Aerospace Technology and Management,2009,1(2):153-160.
[8]TEIPEL U,HEINTZ T,KRAUSE H H.Crystallization of spherical ammonium dinitramide(ADN)particles[J].Propellants,Explosives,Pyrotechnics,2000,25(2):81-85.
[9]LANGLET A,WINGBORG N,OSTMARK H.ADN:a new high performance oxidizer for solid propellants[J].International Journal of Energetic Materials&Chemical Propulsion,1997,4(1/2/3/4/5/6):616-626.
[10]HEINTZ T,PONTIUS H,ANIOL J,et al.ADN-prilling,coating and characterization[C]//The 39th International Annual Conference of ICT.Karlsruhe,Germany:2008.
[11]GUIMONT J.Process for preparing spherical energetic compounds:5801453[P].1998-09-01.
[12]王伯周,张志忠,刘愆,等.ADN合成及应用研究进展[C]//ADN合成与应用研讨会论文集.北京,2006:11-33.WANG B Z,ZHANG Z Z,LIU Q,et al.ADN synthesis and application of research progress[C]//ADN Synthesis and Application Symposium Proceedings.Beijing,2006:11-33.
[13]刘波,刘少武,于慧芳,等.二硝酰胺铵防吸湿技术研究进展[J].化学推进剂与高分子材料,2011,9(6):57-60.LIU B,LIU S W,YU H F,et al.Research progress in anti-hygroscopicity of ammonium dinitramide[J].Chemical Propellants&Polymeric Materials,2011,9(6):57-60.
[14]马跃,张海林.二硝酰胺铵(ADN)球形化工艺研究[J].固体火箭技术,2002,25(2):59-62.MA Y,ZHANG H L.Study on prilling process of ammonium dinitramide(ADN)[J].Journal of Solid Rocket Technology,2002,25(2):59-62.
[15]马跃,张海林.球形二硝酰胺铵研究[J].固体火箭技术,2002,25(1):29-32.MA Y,ZHANG H L.Study on prilled ammonium dinitramide(ADN)[J].Journal of Solid Rocket Technology,2002,25(1):29-32.
[16]黄洪勇.高能氧化剂二硝酰胺铵研究进展[J].上海航天,2005(4):31-35.HUANG H Y.Study progress of ammonium dinitramide[J].Aerospace Shanghai,2005(4):31-35.
[17]RAMASWAMY A L.Energetic-material combustion experiments on propellant formulations containing prilled ammonium dinitramide[J].Combustion,Explosion,and Shock Waves,2000,36(1):119-124.
[18]HIGHSMITH T K,MCLEOD C S,WARDIE R B,et al.Manufacture of thermally-stabilized prilled ammonium dinitramide particles,and process for making the same:US6136115[P].2000-10-24.
[19]WINGBORG N,ANDREASSON S,FLON J D,et al.Development of ADN-based minimum smoke propellants[C]//The 46th AIAA/ASME/SAE/ASEE Joint Propulsion Conference&Exhibit.Nashville,US,2010.
[20]JOHANSSON M,FLON JD,PETTERSON,et al.Spray prilling of ADN and testing of ADN-based solid propellants[C]//The 3rd International Conference on Green Propellants for Space Propulsion.Poitiers,France,2006.
[21]HEINTZ T,REINHARD W,BIRKE C,et al.Particle size adjustment of spherical ammonium dinitramide particles(ADN-prills)produced by emulsion crystallization[C]//The 45th International Annual Conference of ICT.Karlsruhe,Germany,2014.
[22]LANGLET A,JOHANSSON M.Method of producing ADN prills suitable for use in a polymer system:WO99/21794[P].1999-05-06.
[23]LILJEDAHL M,SKARSTIND M,LINDBORG A.Processing of ADN particles[C]//The 46th International Annual Conference of ICT.Karlsruhe,Germany,2015.
[24]LINDBORQ A,LILJEDAHL M,PETERSSON A,et al.Jet Milling of ADN and FOX-12[C]//The 44th International Annual Conference of ICT.Karlsruhe,Germany,2013.
[25]LANGLET A,JOHANSSON M.Method of producing prills of ammonium dinitramide(ADN):WO 99/21793[P].1999-05-06.
[26]HEINTZ T,FUCHS A.Continuous production of spherical ammonium dinitramide particles(ADN-prills)by microreaction technology[C]//The 41st International Annual Conference of ICT.Karlsruhe,Germany,2010.
[27]彭翠枝,郑斌,张培,等.国外二硝酰胺铵的发展现状[J].火炸药学报,2014,37(3):1-5.PENG C Z,ZHENG B,ZHANG P,et al.Current situation of foreign ammonium dinitramide development[J].Chinese Journal of Explosives&Propellants,2014,37(3):1-5.
[28]MANSELL E,EVANS S,MYATT R,et al.Development of the Roxel emulsion mediated spheroidisation technique for ammonium dinitramide(ADN)[C]//The46th International Annual Conference of ICT,Karlsruhe,Germany,2015.
[29]YUAN Q,ARYANTI N,GUTIRREZ G,et al.Enhancing the throughput of membrane emulsification techniques to manufacture functional particles[J].Industrial&Engineering Chemistry Research,2009,48(19):8872-8880.
[30]EGIDI E,GASPARINI G,HOLDICH R G,et al.Membrane emulsification using membranes of regular pore spacing:droplet size and uniformity in the presence of surface shear[J].Journal of Membrane Science,2008,323(2):414-420.
[31]JOHANSSON M,WINGBORG N,JOHANSSON J,et al.ADN is more than particles and formulations-it is a part of future missile propellants[C]//The NDIA Insensitive Munitions&Energetic Materials Technology Symposium.San Diego,US,2013.
[32]HIGHSNITH T K.ADN maunfactory technoiogy[C]//Proceedings 29th International Conference of ICT.Karisruhe,Germany,1998.
[33]CERRI S,BOHN M A.Ageing behaviour of rocket propellant formulations with ADN as oxidizer investigated by DMA,DSC and SEM[C]//The 42th International Annual Conference of ICT.Karlsruhe,Germany,2011.
[34]GETTWERT V,FISCHER S.Aluminized ADN/GAP propellants-formulation and properties[C]//The 44th International Annual Conference of ICT.Karlsruhe,Germany,2013.
[35]李上文,赵风起,高红旭,等.ADN及其推进剂研制的进展[C]//ADN合成与应用研讨会论文集.北京,2006:1-10.LI S W,ZHAO F Q,GAO H X,et al.Development of ADN and its propellant[C]//ADN Synthesis and Application Symposium Proceedings.Beijing,2006:1-10.
[36]任晓雪,赵凤起,郑斌.ADN推进剂的研究发展[J].飞航导弹,2007(12):53-55.
[37]LANDSEM E,TOMAS L.Mechanical properties of smokeless composite rocket propellants based on prilled ammonium dinitramide[J].Propellants,Explosives,Pyrotechnics,2012,37(6):691-698.