茅苍术饮片的制备工艺研究
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摘要
目的优选茅苍术饮片的最佳制备工艺。方法采用正交试验法,以水分、灰分、苍术素及挥发油含量等多种指标进行综合评价,优选茅苍术净制、干燥最佳工艺参数。结果茅苍术饮片的最佳水处理工艺参数为:加水量10倍,水洗1次,转速45r/min、水洗时间60s;干燥工艺参数为:干燥温度50℃,时间4h,厚度2cm,翻动2次。结论本研究制定的茅苍术饮片生产工艺稳定可行,为其饮片规范化生产奠定了良好基础。
Objective To optimize the preparation technology of Areactylodis Lanceae Rhizoma. Methods Using the orthogonal test method,with water,ash,Atractylodin and volatile oil content and other indicators to conduct comprehensive evaluation,we can optimize the best processing parameters for the purification and drying of the Areactylodis Lanceae Rhizoma.Results The optimum water treatment parameters of Areactylodis Lanceae Rhizoma were as follows: 10 times water addition,once washing,45r/min speed,60s washing time; drying parameters were as follows: drying temperature 50℃,time 4h,thickness 2cm,turning twice. Conclusion The preparation technology of Areactylodis Lanceae Rhizoma is stable and feasible,which lays a good foundation for standardized production of Chinese herbal medicines.
Objective To optimize the preparation technology of Areactylodis Lanceae Rhizoma. Methods Using the orthogonal test method,with water,ash,Atractylodin and volatile oil content and other indicators to conduct comprehensive evaluation,we can optimize the best processing parameters for the purification and drying of the Areactylodis Lanceae Rhizoma.Results The optimum water treatment parameters of Areactylodis Lanceae Rhizoma were as follows: 10 times water addition,once washing,45r/min speed,60s washing time; drying parameters were as follows: drying temperature 50℃,time 4h,thickness 2cm,turning twice. Conclusion The preparation technology of Areactylodis Lanceae Rhizoma is stable and feasible,which lays a good foundation for standardized production of Chinese herbal medicines.
引文
[1]国家药典委员会.中华人民共和国药典[M].一部.北京:化学工业出版社,2015:161.
[2]邓爱平,李颖,吴志涛,等.苍术化学成分和药理的研究进展[J].中国中药杂志,2016,41(21):3904-3913.
[3]刘晓宁,侯芳洁,谷巍,等.不同产地苍术挥发油特征性成分分析[J].南京中医药大学学报,2009,25(1):51-53.
[4]王鸣,肖超成,陈雨,等.不同产地茅苍术水溶性成分的HPLC指纹图谱研究[J].植物资源与环境学报,2009,18(1):12-15.
[5]许俊华,巢建国,谷巍,等.不同产地茅苍术药材无机元素测定及分析[J].南京中医药大学学报,2010,26(4):294-295.
[6]黄新平,熊娟,许腊英,等.湖北贝母的净制工艺研究[J].湖北中医药大学学报,2011,13(2):28-30.
[7]叶丛进,赵宏伟,王文杰,等.不同加工方法对湖北大别山地区茅苍术挥发油的影响[J].湖北中医学院学报,2005,7(1):51-52.
[8]国家药典委员会.中华人民共和国药典[M].四部.北京:化学工业出版社,2015:104,203-204.
[9]黄瑞平,孙敏宁,潘红玲.茅苍术与北苍术中苍术素含量的比较[J].中国中医药科技,2015,22(04):398-399.
[10]史周华.中医药统计学[M].北京:科学出版社,2009:76-78.
[2]邓爱平,李颖,吴志涛,等.苍术化学成分和药理的研究进展[J].中国中药杂志,2016,41(21):3904-3913.
[3]刘晓宁,侯芳洁,谷巍,等.不同产地苍术挥发油特征性成分分析[J].南京中医药大学学报,2009,25(1):51-53.
[4]王鸣,肖超成,陈雨,等.不同产地茅苍术水溶性成分的HPLC指纹图谱研究[J].植物资源与环境学报,2009,18(1):12-15.
[5]许俊华,巢建国,谷巍,等.不同产地茅苍术药材无机元素测定及分析[J].南京中医药大学学报,2010,26(4):294-295.
[6]黄新平,熊娟,许腊英,等.湖北贝母的净制工艺研究[J].湖北中医药大学学报,2011,13(2):28-30.
[7]叶丛进,赵宏伟,王文杰,等.不同加工方法对湖北大别山地区茅苍术挥发油的影响[J].湖北中医学院学报,2005,7(1):51-52.
[8]国家药典委员会.中华人民共和国药典[M].四部.北京:化学工业出版社,2015:104,203-204.
[9]黄瑞平,孙敏宁,潘红玲.茅苍术与北苍术中苍术素含量的比较[J].中国中医药科技,2015,22(04):398-399.
[10]史周华.中医药统计学[M].北京:科学出版社,2009:76-78.