香烟潜香物质——β-环己烯基异噁唑的合成

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英文篇名：Cigarette Potential Aroma Substance——Synthesis of β-Cyclohexenyl Isoxazole 作者：冯银茂 ; 吴启童 ; 李有桂 英文作者：FENG Yin-mao;WU Qi-tong;LI You-gui;School of Chemistry and Chemical Engineering,Hefei Univercity of Technology; 关键词：β-紫罗兰酮 ; β-环己烯基异噁唑 ; 香烟潜香物质 英文关键词：β-ionone;;β-cyclohexenyl isoxazole;;cigarette potential aroma substance 中文刊名：AHHG 英文刊名：Anhui Chemical Industry 机构：合肥工业大学化学与化工学院; 出版日期：2019-02-15 出版单位：安徽化工 年：2019 期：v.45;No.217 语种：中文; 页：AHHG201901012 页数：2 CN：01 ISSN：34-1114/TQ 分类号：47-48

摘要

以β-紫罗兰酮和羟胺为原料,在温和的条件下合成了香烟潜香物质β-环己烯基异噁唑,优化了反应条件。中间体及产物结构通过~1H-NMR、~(13)C-NMR、HRMS进行了表征。
        At the mind reaction conditions, cigarette potential aroma substance——β-cyclohexenyl isoxazole was synthesized by using β-ionone and hydroxylamine as starting material, and the reaction conditions were optimized. The structures of the intermediate and product were characterized with ~1H-NMR,~(13)H-NMR and HRMS spectras.

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