SAPO-11分子筛合成方法与改性技术
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摘要
对SAPO-11分子筛的合成方法、改性技术及应用的最新研究进展进行了综述,并对SAPO-11分子筛的改性技术及其应用进行了展望。认为今后合成SAPO-11分子筛的发展趋势是催化剂晶粒小尺寸化,并具有优良的孔道结构和较大外比表面积。
The advances in synthetic methods,modification technology and application of SAPO-11 molecular sieve were summarized with 52 references,and its modification technology and application were prospected. It was pointed out that the development trend of SAPO-11 molecular sieve was smaller particle size,better pore structure,and larger external specific surface area.
The advances in synthetic methods,modification technology and application of SAPO-11 molecular sieve were summarized with 52 references,and its modification technology and application were prospected. It was pointed out that the development trend of SAPO-11 molecular sieve was smaller particle size,better pore structure,and larger external specific surface area.
引文
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[5]Fan W,Snyder M A,Kumar S,et al.Hierarchical nanofabrication of microporous crystals with ordered mesoporosity[J].Nature materials,2008,7(12):984-991.
[6]Chen H,Wydra J,Zhang X,et al.Hydrothermal synthesis of zeolites with three-dimensionally ordered mesoporous-imprinted structure[J].Journal of the American Chemical Society,2011,133(32):12390-12393.
[7]Gola A,Rebours B,Milazzo E,et al.Effect of leaching agent in the dealumination of stabilized Y zeolites[J].Microporous&Mesoporous Materials,2000,40(1/3):73-83.
[8]Ogura M,Shinomiya S,Tateno J,et al.Formation of uniform mesopores in ZSM-5 zeolite through treatment in alkaline solution[J].Chemistry Letters,2000,29(8):882-883.
[9]Groen J C,Moulijn J A,Pérez-Ramírez J.Alkaline posttreatment of MFI zeolites.From accelerated screening to scale-up[J].Industrial&Engineering Chemistry Research,2007,46(12):4193-4201.
[10]赵莺,杨潍嘉,杨凯旭,等.微波辅助水热条件对二乙胺合成SAPO-11晶体结构与性质的影响[J].人工晶体学报,2017,46(1):1-7.
[11]王琼.微波辅助高效水热合成SAPO-11分子筛[J].无机盐工业,2014,46(2):74-78.
[12]Liu Y,Xu L,LüY,et al.Regulating acidity,porosity,and morphology of hierarchical SAPO-11 zeolite by aging treatment[J].Journal of Colloid&Interface Science,2016(479):55-63.
[13]韩磊,崔晓,刘欣梅.SAPO-11分子筛粒度调控[J].无机化学学报,2013,29(3):565-570.
[14]刘作磊,张宝川,张进,等.空心玻璃微球制备的研究进展[J].材料导报,2011,25(17):451-453.
[15]Cheng Y X,Song J F,Chen L W,et al.Silic hybrid xerogel Incorporating(R)-2,2'-bis(methoxyethoxymethyloxy-1,1'-binaphthyl unit via sol-gel process[J].Chinese Journal of Inorganic Chemistry,2005,4(4):561-564.
[16]Song C M,Feng Y,Ma L L.Characterization and hydroisomerization performance of SAPO-11 molecular sieves synthesized by dry gel conversion[J].Microporous&Mesoporous Materials,2012,147(1):205-211.
[17]Song C M,Yang H,Wang Y,et al.Dry-gel conversion synthesis of SAPO-11 molecular sieves and their use in hydroisodewaxing of hydrocracking recycle oil[J].Asia-Pacific Journal of Chemical Engineering,2016,11(6):846-854.
[18]Cui X,Liu Y,Liu X.Controlling acidic sites to improve hydro isomerization performance of Pt/SAPO-11 catalysts[J].Catalysis Letters,2015,145(7):1464-1473.
[19]孙丽媛,张亚飞,巩雁军.微孔-微孔复合分子筛的结构特征及应用[J].物理化学学报,2016,32(5):1105-1122.
[20]杨秀娜,姜阳,齐慧敏.多级孔ZSM-5分子筛的制备及其催化甲醇芳构化反应性能[J].化工进展,2016,35(11):3536-3541.
[21]Chen Z,Song W,Zhu S,et al.Synthesis of a multi-branched dandelion-like SAPO-11 by an in situ inoculating seed-induced-steam-assisted conversion method(SISAC)as a highly effective hydroisomerization support[J].RSC Advances,2017,7(8):4656-4666.
[22]Wu Q,Oduro I N,Huang Y,et al.Synthesis of hierarchical SA-PO-11 via seeded crystallization[J].Microporous and Mesoporous Materials,2015(218):24-32.
[23]陈铁红,袁忠勇,王敬中.气固相法合成β沸石分子筛[J].石油学报(石油加工),1999,15(5):77-80.
[24]唐建君,许云书.微孔材料的研究进展[J].材料导报,2010,24(16):20-23.
[25]Jin Y,Sun Q,Qi G,et al.Solvent-free synthesis of silicoaluminophosphate zeolites[J].Angewandte Chemie International Edition,2013,52(35):9172-9175.
[26]Jin Y,Chen X,Sun Q,et al.Solvent-free syntheses of hierarchically porous aluminophosphate-based zeolites with AEL and AFI structures[J].Chemistry A European Journal,2014,20(52):16-23.
[27]谭可心,栾国颜,裴东寒.ZSM-5分子筛的合成及改性研究进展[J].人工晶体学报,2016,45(12):2895-2901.
[28]吴会军,朱冬生,向兰.有机溶剂热法合成纳米材料的研究与发展[J].化工新型材料,2005,33(8):1-4.
[29]孙剑,王金泉,王蕾,等.基于离子液体的绿色催化过程[J].中国科学(化学),2014,44(1):100-113.
[30]管国锋,万辉,王磊.介孔分子筛固载离子液体的制备及应用研究进展[J].石油化工,2014,43(3):241-248.
[31]金银樱.固相合成磷铝沸石分子筛及其应用[D].杭州:浙江大学,2014.
[32]Razavian M,Halladj R,Askari S.Recent advances in silicoalumino phosphate nanocatalysts synthesis techniques and their effects on particle size distribution[J].Rev Adv Mater Sci,2011(29):83-99.
[33]Han L,Liu Y,Subhan F,et al.Particle effect of SAPO-11 promoter on isomerization reaction in FCC units[J].Microporous and Mesoporous Materials,2014,194(8):90-96.
[34]肖寒,于海斌,刘红光,等.晶种硅烷化合成小粒径SAPO-11分子筛表征及其临氢异构化催化性能评价[J].石油炼制与化工,2014,45(1):28-34.
[35]张胜振,陈胜利,董鹏,等.小晶粒SAPO-11分子筛的合成及其催化异构化性能[J].催化学报,2007,28(10):857-864.
[36]Chen Z,Dong Y,Jiang S,et al.Low-temperature synthesis of hierarchical architectures of SAPO-11 zeolite as a good hydroisomerization support[J].Journal of Materials Science,2017,52(8):1-12.
[37]Fan Y,Xiao H,Shi G,et al.Alkylphosphonic acid-and small amine-templated synthesis of hierarchical silicoaluminophosphate molecular sieves with high isomerization selectivity to dibranched paraffins[J].Journal of Catalysis,2012,285(1):251-259.
[38]孙娜,王海彦,李浩,等.剑麻纤维素合成多级孔SAPO-11分子筛及其临氢异构化性能[J].硅酸盐学报,2018,46(1):108-115.
[39]Liu Y,Liu X,Zhao L,et al.Effect of lanthanum species on the physicochemical properties of La/SAPO-11 molecular sieve[J].Journal of Catalysis,2017(347):170-184.
[40]Yang Zhichao,Liu Yunqi,Zhao Jinchong,et al.Zinc-modified Pt/SAPO-11 for improving the isomerization selectivity to dibranched alkanes[J].Chinese Journal of Catalysis,2017,38(3):509-517.
[41]魏晓鸣,柳云骐,刘晨光.Ni W/SAPO-11催化剂孔结构性质对其柴油异构降凝性能的影响[J].石油学报(石油加工),2015,31(6):1394-1401.
[42]魏晓鸣,柳云骐,赵亮,等.Ni W/SAPO-11催化剂制备方法对柴油异构降凝性能的影响[J].燃料化学学报,2014,42(12):1500-1505.
[43]高善彬,迟克彬,杨晓东,等.正构烷烃在Pt/SAPO-11催化剂上加氢异构反应性能[J].化工学报,2016,67(12):5024-5030.
[44]杨娜,王红英,柳云骐,等.不同链长正构烷烃在Pt/SAPO-11催化剂上的临氢转化规律研究[J].燃料化学学报,2016,44(1):91-98.
[45]Chen N,Ren Y,Qian E W.Elucidation of the active phase in Pt Sn/SAPO-11 for hydrodeoxygenation of methyl palmitate[J].Journal of Catalysis,2016,334(3):79-88.
[46]Chen N,Gong S,Shirai H,et al.Effects of Si/Al ratio and Pt loading on Pt/SAPO-11 catalysts in hydroconversion of Jatropha oil[J].Applied Catalysis A General,2013,466(36):105-115.
[47]Rabaev M,Landau M V,Vidruk N R,et al.Improvement of hydrothermal stability of Pt/SAPO-11 catalyst in hydrodeoxygenation isomerization aromatization of vegetable oil[J].Journal of Catalysis,2015(332):164-176.
[48]Liu X Q,Li S H,Sun M T,et al.Preparation,characterization and low-temperature NH3-SCR activity of MnOx/SAPO-11catalysts[J].Acta Physico-Chimica Sinica,2016,32(5):1236-1246.
[49]Wang X,Guo F,Wei X,et al.The catalytic performance of methylation of naphthalene with methanol over SAPO-11 zeolites synthesized with different Si content[J].Korean Journal of Chemical Engineering,2016,33(7):2034-2041.
[50]温健,王桂云,张晔,等.SAPO-11分子筛择形催化萘甲基化反应[J].石油化工,2010,39(5):487-491.
[51]刘国柱,韩立军,师亚威,等.Pt/SAPO-11催化费托合成油选择性加氢异构化制备替代喷气燃料[J].石油化工,2015,44(2):144-149.
[52]赵昱,刘红星.不同模板剂合成SAPO-11分子筛及其甲醇制烯烃催化性能[J].天然气化工(化学与化工),2013,38(5):5-8.
[2]梁君,王福平.烷烃加氢异构化反应[J].化学进展,2008,20(4):457-463.
[3]Jacobsen C J H,Madsen C,Houzvicka J,et al.Mesoporous zeolite single crystals[J].Journal of the American Chemical Society,2000,122(29):7116-7117.
[4]Cho H S,Ryoo R.Synthesis of ordered mesoporous MFI zeolite using CMK carbon templates[J].Microporous and Mesoporous Materials,2012(151):107-112.
[5]Fan W,Snyder M A,Kumar S,et al.Hierarchical nanofabrication of microporous crystals with ordered mesoporosity[J].Nature materials,2008,7(12):984-991.
[6]Chen H,Wydra J,Zhang X,et al.Hydrothermal synthesis of zeolites with three-dimensionally ordered mesoporous-imprinted structure[J].Journal of the American Chemical Society,2011,133(32):12390-12393.
[7]Gola A,Rebours B,Milazzo E,et al.Effect of leaching agent in the dealumination of stabilized Y zeolites[J].Microporous&Mesoporous Materials,2000,40(1/3):73-83.
[8]Ogura M,Shinomiya S,Tateno J,et al.Formation of uniform mesopores in ZSM-5 zeolite through treatment in alkaline solution[J].Chemistry Letters,2000,29(8):882-883.
[9]Groen J C,Moulijn J A,Pérez-Ramírez J.Alkaline posttreatment of MFI zeolites.From accelerated screening to scale-up[J].Industrial&Engineering Chemistry Research,2007,46(12):4193-4201.
[10]赵莺,杨潍嘉,杨凯旭,等.微波辅助水热条件对二乙胺合成SAPO-11晶体结构与性质的影响[J].人工晶体学报,2017,46(1):1-7.
[11]王琼.微波辅助高效水热合成SAPO-11分子筛[J].无机盐工业,2014,46(2):74-78.
[12]Liu Y,Xu L,LüY,et al.Regulating acidity,porosity,and morphology of hierarchical SAPO-11 zeolite by aging treatment[J].Journal of Colloid&Interface Science,2016(479):55-63.
[13]韩磊,崔晓,刘欣梅.SAPO-11分子筛粒度调控[J].无机化学学报,2013,29(3):565-570.
[14]刘作磊,张宝川,张进,等.空心玻璃微球制备的研究进展[J].材料导报,2011,25(17):451-453.
[15]Cheng Y X,Song J F,Chen L W,et al.Silic hybrid xerogel Incorporating(R)-2,2'-bis(methoxyethoxymethyloxy-1,1'-binaphthyl unit via sol-gel process[J].Chinese Journal of Inorganic Chemistry,2005,4(4):561-564.
[16]Song C M,Feng Y,Ma L L.Characterization and hydroisomerization performance of SAPO-11 molecular sieves synthesized by dry gel conversion[J].Microporous&Mesoporous Materials,2012,147(1):205-211.
[17]Song C M,Yang H,Wang Y,et al.Dry-gel conversion synthesis of SAPO-11 molecular sieves and their use in hydroisodewaxing of hydrocracking recycle oil[J].Asia-Pacific Journal of Chemical Engineering,2016,11(6):846-854.
[18]Cui X,Liu Y,Liu X.Controlling acidic sites to improve hydro isomerization performance of Pt/SAPO-11 catalysts[J].Catalysis Letters,2015,145(7):1464-1473.
[19]孙丽媛,张亚飞,巩雁军.微孔-微孔复合分子筛的结构特征及应用[J].物理化学学报,2016,32(5):1105-1122.
[20]杨秀娜,姜阳,齐慧敏.多级孔ZSM-5分子筛的制备及其催化甲醇芳构化反应性能[J].化工进展,2016,35(11):3536-3541.
[21]Chen Z,Song W,Zhu S,et al.Synthesis of a multi-branched dandelion-like SAPO-11 by an in situ inoculating seed-induced-steam-assisted conversion method(SISAC)as a highly effective hydroisomerization support[J].RSC Advances,2017,7(8):4656-4666.
[22]Wu Q,Oduro I N,Huang Y,et al.Synthesis of hierarchical SA-PO-11 via seeded crystallization[J].Microporous and Mesoporous Materials,2015(218):24-32.
[23]陈铁红,袁忠勇,王敬中.气固相法合成β沸石分子筛[J].石油学报(石油加工),1999,15(5):77-80.
[24]唐建君,许云书.微孔材料的研究进展[J].材料导报,2010,24(16):20-23.
[25]Jin Y,Sun Q,Qi G,et al.Solvent-free synthesis of silicoaluminophosphate zeolites[J].Angewandte Chemie International Edition,2013,52(35):9172-9175.
[26]Jin Y,Chen X,Sun Q,et al.Solvent-free syntheses of hierarchically porous aluminophosphate-based zeolites with AEL and AFI structures[J].Chemistry A European Journal,2014,20(52):16-23.
[27]谭可心,栾国颜,裴东寒.ZSM-5分子筛的合成及改性研究进展[J].人工晶体学报,2016,45(12):2895-2901.
[28]吴会军,朱冬生,向兰.有机溶剂热法合成纳米材料的研究与发展[J].化工新型材料,2005,33(8):1-4.
[29]孙剑,王金泉,王蕾,等.基于离子液体的绿色催化过程[J].中国科学(化学),2014,44(1):100-113.
[30]管国锋,万辉,王磊.介孔分子筛固载离子液体的制备及应用研究进展[J].石油化工,2014,43(3):241-248.
[31]金银樱.固相合成磷铝沸石分子筛及其应用[D].杭州:浙江大学,2014.
[32]Razavian M,Halladj R,Askari S.Recent advances in silicoalumino phosphate nanocatalysts synthesis techniques and their effects on particle size distribution[J].Rev Adv Mater Sci,2011(29):83-99.
[33]Han L,Liu Y,Subhan F,et al.Particle effect of SAPO-11 promoter on isomerization reaction in FCC units[J].Microporous and Mesoporous Materials,2014,194(8):90-96.
[34]肖寒,于海斌,刘红光,等.晶种硅烷化合成小粒径SAPO-11分子筛表征及其临氢异构化催化性能评价[J].石油炼制与化工,2014,45(1):28-34.
[35]张胜振,陈胜利,董鹏,等.小晶粒SAPO-11分子筛的合成及其催化异构化性能[J].催化学报,2007,28(10):857-864.
[36]Chen Z,Dong Y,Jiang S,et al.Low-temperature synthesis of hierarchical architectures of SAPO-11 zeolite as a good hydroisomerization support[J].Journal of Materials Science,2017,52(8):1-12.
[37]Fan Y,Xiao H,Shi G,et al.Alkylphosphonic acid-and small amine-templated synthesis of hierarchical silicoaluminophosphate molecular sieves with high isomerization selectivity to dibranched paraffins[J].Journal of Catalysis,2012,285(1):251-259.
[38]孙娜,王海彦,李浩,等.剑麻纤维素合成多级孔SAPO-11分子筛及其临氢异构化性能[J].硅酸盐学报,2018,46(1):108-115.
[39]Liu Y,Liu X,Zhao L,et al.Effect of lanthanum species on the physicochemical properties of La/SAPO-11 molecular sieve[J].Journal of Catalysis,2017(347):170-184.
[40]Yang Zhichao,Liu Yunqi,Zhao Jinchong,et al.Zinc-modified Pt/SAPO-11 for improving the isomerization selectivity to dibranched alkanes[J].Chinese Journal of Catalysis,2017,38(3):509-517.
[41]魏晓鸣,柳云骐,刘晨光.Ni W/SAPO-11催化剂孔结构性质对其柴油异构降凝性能的影响[J].石油学报(石油加工),2015,31(6):1394-1401.
[42]魏晓鸣,柳云骐,赵亮,等.Ni W/SAPO-11催化剂制备方法对柴油异构降凝性能的影响[J].燃料化学学报,2014,42(12):1500-1505.
[43]高善彬,迟克彬,杨晓东,等.正构烷烃在Pt/SAPO-11催化剂上加氢异构反应性能[J].化工学报,2016,67(12):5024-5030.
[44]杨娜,王红英,柳云骐,等.不同链长正构烷烃在Pt/SAPO-11催化剂上的临氢转化规律研究[J].燃料化学学报,2016,44(1):91-98.
[45]Chen N,Ren Y,Qian E W.Elucidation of the active phase in Pt Sn/SAPO-11 for hydrodeoxygenation of methyl palmitate[J].Journal of Catalysis,2016,334(3):79-88.
[46]Chen N,Gong S,Shirai H,et al.Effects of Si/Al ratio and Pt loading on Pt/SAPO-11 catalysts in hydroconversion of Jatropha oil[J].Applied Catalysis A General,2013,466(36):105-115.
[47]Rabaev M,Landau M V,Vidruk N R,et al.Improvement of hydrothermal stability of Pt/SAPO-11 catalyst in hydrodeoxygenation isomerization aromatization of vegetable oil[J].Journal of Catalysis,2015(332):164-176.
[48]Liu X Q,Li S H,Sun M T,et al.Preparation,characterization and low-temperature NH3-SCR activity of MnOx/SAPO-11catalysts[J].Acta Physico-Chimica Sinica,2016,32(5):1236-1246.
[49]Wang X,Guo F,Wei X,et al.The catalytic performance of methylation of naphthalene with methanol over SAPO-11 zeolites synthesized with different Si content[J].Korean Journal of Chemical Engineering,2016,33(7):2034-2041.
[50]温健,王桂云,张晔,等.SAPO-11分子筛择形催化萘甲基化反应[J].石油化工,2010,39(5):487-491.
[51]刘国柱,韩立军,师亚威,等.Pt/SAPO-11催化费托合成油选择性加氢异构化制备替代喷气燃料[J].石油化工,2015,44(2):144-149.
[52]赵昱,刘红星.不同模板剂合成SAPO-11分子筛及其甲醇制烯烃催化性能[J].天然气化工(化学与化工),2013,38(5):5-8.