Properties and corrosion behavior of Al based nanocomposite foams produced by the sintering-dissolution process
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摘要
The properties of Al based nanocomposite metal foams and their corrosion behaviors were investigated in this study. For this, the composite metal foams with different relative densities(porosity) reinforced with alumina nanoparticles were prepared using a powder metallurgy-based sintering-dissolution process(SDP) and Na Cl particles were used as space holders. Then, the effect of nanoparticle reinforcement and different amounts of Na Cl space holders(corresponding porosity) on the microstructure, morphology, density, hardness, and electrochemical specifications of the samples were investigated. It was found that as the relative density increased from 60% to 70%, the wall thickness increased from about 200 to 300 μm, which led to a decrease in pore size. Also, the addition of nanoparticle reinforcement and the increased relative density result in increasing metal foam hardness. Moreover, electrochemical test results indicated that increasing the Al_2O_3 content reduced the corrosion rate, but increasing the porosity enhanced it.
The properties of Al based nanocomposite metal foams and their corrosion behaviors were investigated in this study. For this, the composite metal foams with different relative densities(porosity) reinforced with alumina nanoparticles were prepared using a powder metallurgy-based sintering-dissolution process(SDP) and Na Cl particles were used as space holders. Then, the effect of nanoparticle reinforcement and different amounts of Na Cl space holders(corresponding porosity) on the microstructure, morphology, density, hardness, and electrochemical specifications of the samples were investigated. It was found that as the relative density increased from 60% to 70%, the wall thickness increased from about 200 to 300 μm, which led to a decrease in pore size. Also, the addition of nanoparticle reinforcement and the increased relative density result in increasing metal foam hardness. Moreover, electrochemical test results indicated that increasing the Al_2O_3 content reduced the corrosion rate, but increasing the porosity enhanced it.
The properties of Al based nanocomposite metal foams and their corrosion behaviors were investigated in this study. For this, the composite metal foams with different relative densities(porosity) reinforced with alumina nanoparticles were prepared using a powder metallurgy-based sintering-dissolution process(SDP) and Na Cl particles were used as space holders. Then, the effect of nanoparticle reinforcement and different amounts of Na Cl space holders(corresponding porosity) on the microstructure, morphology, density, hardness, and electrochemical specifications of the samples were investigated. It was found that as the relative density increased from 60% to 70%, the wall thickness increased from about 200 to 300 μm, which led to a decrease in pore size. Also, the addition of nanoparticle reinforcement and the increased relative density result in increasing metal foam hardness. Moreover, electrochemical test results indicated that increasing the Al_2O_3 content reduced the corrosion rate, but increasing the porosity enhanced it.
引文
[1]X.Fang and Z.Fan,A novel approach to produce Al-alloy foams,J.Mater.Sci.,42(2007),No.18,p.7894.
[2]M.Amirjan and H.Khorsand,On the microstructure and properties of Al-Al2O3 nanocomposites hollow sphere structures,[in]Proceedings of the 5th International Congress on Nanoscience&Nanotechnology(ICNN2014),Tehran,2014,p.1441.
[3]D.X.Sun and Y.Y.Zhao,Static and dynamic energy absorption of al foams produced by a sintering and dissolution process,Metall.Mater.Trans.B,34(2003),No.1,p.69.
[4]I.Jeon,K.Katou,T.Sonoda,T.Asahina,and K.J.Kang,Cell wall mechanical properties of closed-cell Al foam,Mech.Mater.,41(2009),No.1,p.60.
[5]L.C.Zhang and H.Attar,Selective laser melting of titanium alloys and titanium matrix composites for biomedical applications:A review,Adv.Eng.Mater.,18(2016),No.4,p.463.
[6]Z.Razavi Hesabi,A.Simch,and S.M.Seyed Reihani,Structural evolution during mechanical milling of nanometric and micrometric Al2O3 reinforced Al matrix composites,Mater.Sci.Eng.A,428(2006),No.1-2,p.159.
[7]H.Mahboob,S.A.Sajjadi,and S.M.Zebarjad,Synthesis of Al-Al2O3 nano-composite by mechanical alloying and evaluation of the effect of ball milling time on the microstructure and mechanical properties,[in]Proceedings of the International Conference on MEMS and Nanotechnology(IC-MN'08),Kuala Lumpur,2008,Malaysia,p.240.
[8]D.Poirier,R.A.L.Drew,M.L.Trudeau,and R.Gauvin,Fabrication and properties of mechanically milled alumina/aluminium nanocomposites,Mater.Sci.Eng.A,527(2010),No.29-30,p.7605.
[9]M.Tabandeh Khorshid,S.A.Jenabali Jahromi,and M.M.Moshksar,Mechanical properties of tri-Modal Al matrix composites reinforced by nano-and submicron-sized Al2O3particulates developed by wet attrition milling and hot extrusion,Mater.Des.,31(2010),No.8,p.1.
[10]Y.J.Liu,S.J.Li,H.L.Wang,W.T.Hou,Y.L.Hao,R.Yang,T.B.Sercombe,and L.C.Zhang,Microstructure,defects and mechanical behavior of beta-type titanium porous structures manufactured by electron beam melting and selective laser melting,Acta Mater.,113(2016),p.56.
[11]Y.J.Liu,S.J.Li,W.T.Hou,S.G.Wang,Y.L.Hao,R.Yang,T.B.Sercombe,and L.C.Zhang,Electron beam melted beta-type Ti-24Nb-4Zr-8Sn porous structures with high strength-to-modulus ratio,J.Mater.Sci..Technol.,32(2016),No.6,p.505.
[12]D.X.Sun and Y.Y.Zhao,Phase changes in sintering of Al/Mg/Na Cl compacts for manufacturing Al foams by the sintering and dissolution process,Mater.Lett.,59(2005),No.1,p.6.
[13]Y.Y.Zhao and D.X.Sun,A novel sintering-dissolusion process for manufacturing Al foams,Scripta Mater.,44(2001),p.105.
[14]H.I.Suarez Andrade,M.E.Hernández Rojas,M.E.Palomar Pardavé,and S.Báez Pimiento,Manufacturing of aluminum foams using the sintering dissolution process,Rev.Colomb.Mater.,5(2013),p.292.
[15]Y.Y.Zhao,Stochastic modelling of removability of Na Cl in sintering and dissolution process to produce Al foams,J.Porous Mater.,10(2003),No.2,p.105.
[16]Z.Hussain and N.S.A.Suffin,Microstructure and mechanical behaviour of aluminium foam produced by sintering dissolution process using Na Cl space holder,J.Eng.Sci.,7(2011),p.37.
[17]A.Yavuz,?.Yavuz,M.S.Ba?p?nar,and H.Bayrak?eken,Effect of dissolving agent shape for the microstructural tailoring of sdp processed aluminum foams,[in]Proceeding of the 6th International Advanced Technologies Symposium(IATS’11),Elaz??,2011,p.22.
[18]E.Aghion and Y.Perez,Effects of porosity on corrosion resistance of Mg alloy foam produced by powder metallurgy technology,Mater.Charact.,96(2014),p.78.
[19]M.Rahimian,N.Parvin,and N.Ehsani,Investigation of particle size and amount of alumina on microstructure and mechanical properties of Al matrix composite made by powder metallurgy,Mater.Sci.Eng.A,527(2010),No.4-5,p.1031.
[20]A.B.Radwan,R.A.Shakoor,and A.Popelka,Improvement in properties of Ni-B coatings by the addition of mixed oxide nanoparticles,Int.J.Electrochem.Sci.,10(2015),p.7548.
[21]T.S.Mahmoud,El-Sayed Y.El-Kady,and A.S.Merzen Al-Shihiri,Corrosion behaviour of Al/Si C and Al/Al2O3nanocomposites,Mater.Res.,15(2012),No.6,p.903.
[22]N.W.Dai,L.C.Zhang,J.X.Zhang,X.Zhang,Q.Z.Ni,Y.Chen,M.L.Wu,and C.Yang,Distinction in corrosion resistance of selective laser melted Ti-6Al-4V alloy on different planes,Corros.Sci.,111(2016),p.703.
[23]M.Kuruvilla,S.John,and A.Joseph,Electrochemical studies on the interaction of L-cysteine with metallic copper in sulfuric acid,Res.Chem.Intermed.,39(2013),No.8,p.3531.
[24]L.O.Olasunkanmi,M.M.Kabanda,and E.E.Ebenso,Quinoxaline derivatives as corrosion inhibitors for mild steel in hydrochloric acid medium:Electrochemical and quantum chemical studies,Physica E,76(2016),p.109.
[25]N.W.Dai,L.C.Zhang,J.X.Zhang,Q.M.Chen,and M.L.Wu,Corrosion behavior of selective laser melted Ti-6Al-4 V alloy in Na Cl solution,Corros.Sci.,102(2016),p.484.
[26]M.Bozorg,T.S.Farahani,J.Neshati,Z.Chaghazardi,and G.M.Ziarani,Myrtus communis as green inhibitor of copper corrosion in sulfuric acid,Ind.Eng.Chem.Res.,53(2014),No.11,p.4295.
[2]M.Amirjan and H.Khorsand,On the microstructure and properties of Al-Al2O3 nanocomposites hollow sphere structures,[in]Proceedings of the 5th International Congress on Nanoscience&Nanotechnology(ICNN2014),Tehran,2014,p.1441.
[3]D.X.Sun and Y.Y.Zhao,Static and dynamic energy absorption of al foams produced by a sintering and dissolution process,Metall.Mater.Trans.B,34(2003),No.1,p.69.
[4]I.Jeon,K.Katou,T.Sonoda,T.Asahina,and K.J.Kang,Cell wall mechanical properties of closed-cell Al foam,Mech.Mater.,41(2009),No.1,p.60.
[5]L.C.Zhang and H.Attar,Selective laser melting of titanium alloys and titanium matrix composites for biomedical applications:A review,Adv.Eng.Mater.,18(2016),No.4,p.463.
[6]Z.Razavi Hesabi,A.Simch,and S.M.Seyed Reihani,Structural evolution during mechanical milling of nanometric and micrometric Al2O3 reinforced Al matrix composites,Mater.Sci.Eng.A,428(2006),No.1-2,p.159.
[7]H.Mahboob,S.A.Sajjadi,and S.M.Zebarjad,Synthesis of Al-Al2O3 nano-composite by mechanical alloying and evaluation of the effect of ball milling time on the microstructure and mechanical properties,[in]Proceedings of the International Conference on MEMS and Nanotechnology(IC-MN'08),Kuala Lumpur,2008,Malaysia,p.240.
[8]D.Poirier,R.A.L.Drew,M.L.Trudeau,and R.Gauvin,Fabrication and properties of mechanically milled alumina/aluminium nanocomposites,Mater.Sci.Eng.A,527(2010),No.29-30,p.7605.
[9]M.Tabandeh Khorshid,S.A.Jenabali Jahromi,and M.M.Moshksar,Mechanical properties of tri-Modal Al matrix composites reinforced by nano-and submicron-sized Al2O3particulates developed by wet attrition milling and hot extrusion,Mater.Des.,31(2010),No.8,p.1.
[10]Y.J.Liu,S.J.Li,H.L.Wang,W.T.Hou,Y.L.Hao,R.Yang,T.B.Sercombe,and L.C.Zhang,Microstructure,defects and mechanical behavior of beta-type titanium porous structures manufactured by electron beam melting and selective laser melting,Acta Mater.,113(2016),p.56.
[11]Y.J.Liu,S.J.Li,W.T.Hou,S.G.Wang,Y.L.Hao,R.Yang,T.B.Sercombe,and L.C.Zhang,Electron beam melted beta-type Ti-24Nb-4Zr-8Sn porous structures with high strength-to-modulus ratio,J.Mater.Sci..Technol.,32(2016),No.6,p.505.
[12]D.X.Sun and Y.Y.Zhao,Phase changes in sintering of Al/Mg/Na Cl compacts for manufacturing Al foams by the sintering and dissolution process,Mater.Lett.,59(2005),No.1,p.6.
[13]Y.Y.Zhao and D.X.Sun,A novel sintering-dissolusion process for manufacturing Al foams,Scripta Mater.,44(2001),p.105.
[14]H.I.Suarez Andrade,M.E.Hernández Rojas,M.E.Palomar Pardavé,and S.Báez Pimiento,Manufacturing of aluminum foams using the sintering dissolution process,Rev.Colomb.Mater.,5(2013),p.292.
[15]Y.Y.Zhao,Stochastic modelling of removability of Na Cl in sintering and dissolution process to produce Al foams,J.Porous Mater.,10(2003),No.2,p.105.
[16]Z.Hussain and N.S.A.Suffin,Microstructure and mechanical behaviour of aluminium foam produced by sintering dissolution process using Na Cl space holder,J.Eng.Sci.,7(2011),p.37.
[17]A.Yavuz,?.Yavuz,M.S.Ba?p?nar,and H.Bayrak?eken,Effect of dissolving agent shape for the microstructural tailoring of sdp processed aluminum foams,[in]Proceeding of the 6th International Advanced Technologies Symposium(IATS’11),Elaz??,2011,p.22.
[18]E.Aghion and Y.Perez,Effects of porosity on corrosion resistance of Mg alloy foam produced by powder metallurgy technology,Mater.Charact.,96(2014),p.78.
[19]M.Rahimian,N.Parvin,and N.Ehsani,Investigation of particle size and amount of alumina on microstructure and mechanical properties of Al matrix composite made by powder metallurgy,Mater.Sci.Eng.A,527(2010),No.4-5,p.1031.
[20]A.B.Radwan,R.A.Shakoor,and A.Popelka,Improvement in properties of Ni-B coatings by the addition of mixed oxide nanoparticles,Int.J.Electrochem.Sci.,10(2015),p.7548.
[21]T.S.Mahmoud,El-Sayed Y.El-Kady,and A.S.Merzen Al-Shihiri,Corrosion behaviour of Al/Si C and Al/Al2O3nanocomposites,Mater.Res.,15(2012),No.6,p.903.
[22]N.W.Dai,L.C.Zhang,J.X.Zhang,X.Zhang,Q.Z.Ni,Y.Chen,M.L.Wu,and C.Yang,Distinction in corrosion resistance of selective laser melted Ti-6Al-4V alloy on different planes,Corros.Sci.,111(2016),p.703.
[23]M.Kuruvilla,S.John,and A.Joseph,Electrochemical studies on the interaction of L-cysteine with metallic copper in sulfuric acid,Res.Chem.Intermed.,39(2013),No.8,p.3531.
[24]L.O.Olasunkanmi,M.M.Kabanda,and E.E.Ebenso,Quinoxaline derivatives as corrosion inhibitors for mild steel in hydrochloric acid medium:Electrochemical and quantum chemical studies,Physica E,76(2016),p.109.
[25]N.W.Dai,L.C.Zhang,J.X.Zhang,Q.M.Chen,and M.L.Wu,Corrosion behavior of selective laser melted Ti-6Al-4 V alloy in Na Cl solution,Corros.Sci.,102(2016),p.484.
[26]M.Bozorg,T.S.Farahani,J.Neshati,Z.Chaghazardi,and G.M.Ziarani,Myrtus communis as green inhibitor of copper corrosion in sulfuric acid,Ind.Eng.Chem.Res.,53(2014),No.11,p.4295.