Fingerprints Analysis of the Chemical Components of Chloroform Parts of Renqing Mangjue Compatibility with Zuota or Not
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摘要
[Objectives] To research the fingerprints of chemical components of chloroform parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota),and to identify Renqing Mangjue compatibility with Zuota or not. [Methods]High-performance liquid chromatography was adopted. Chromatographic column was DIKMA diamonsil( 4. 6 mm × 250 mm,5 μm); flow rate was 1 mL / min; column temperature was 30 ℃; mobile phase was methanol-water with gradient elution. [Results] A total of 18 common fingerprint peaks were obtained. As for the petroleum ether parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota),eight characteristic peaks were obtained. [Conclusions] Characteristic fingerprints of chloroform parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota) could be obtained by the high-performance liquid chromatography. Therefore,the Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota) could be identified according to their characteristic peaks.
[Objectives] To research the fingerprints of chemical components of chloroform parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota),and to identify Renqing Mangjue compatibility with Zuota or not. [Methods]High-performance liquid chromatography was adopted. Chromatographic column was DIKMA diamonsil( 4. 6 mm × 250 mm,5 μm); flow rate was 1 mL / min; column temperature was 30 ℃; mobile phase was methanol-water with gradient elution. [Results] A total of 18 common fingerprint peaks were obtained. As for the petroleum ether parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota),eight characteristic peaks were obtained. [Conclusions] Characteristic fingerprints of chloroform parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota) could be obtained by the high-performance liquid chromatography. Therefore,the Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota) could be identified according to their characteristic peaks.
[Objectives] To research the fingerprints of chemical components of chloroform parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota),and to identify Renqing Mangjue compatibility with Zuota or not. [Methods]High-performance liquid chromatography was adopted. Chromatographic column was DIKMA diamonsil( 4. 6 mm × 250 mm,5 μm); flow rate was 1 mL / min; column temperature was 30 ℃; mobile phase was methanol-water with gradient elution. [Results] A total of 18 common fingerprint peaks were obtained. As for the petroleum ether parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota),eight characteristic peaks were obtained. [Conclusions] Characteristic fingerprints of chloroform parts of Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota) could be obtained by the high-performance liquid chromatography. Therefore,the Renqing Mangjue and Renqing Mangjue powder( compatibility without Zuota) could be identified according to their characteristic peaks.
引文
[1]ZHAN D,ZHAO JN.Modern research on Tibetan medicine prescription preparation and its clinical application[M].Chengdu:Sichuan Science and Technology Press,2009:470-471.(in Chinese).
[2]Pharmacopoeia Commission of the People’s Republic of China.Chinese Pharmacopoeia[M].Beijing:Chemical Industry Press,2010.(in Chinese).
[3]ZHAN D,ZHAO JN.Modern research on Tibetan medicine prescription preparation and its clinical application[M].Chengdu:Sichuan Science and Technology Press,2009:470-471.(in Chinese).
[4]ZHU JB,SHI YB,LI XY.Modern study on Tibetan drug-"zuo ta"[J].Asia-Pacific Traditional Medicine,2014,10(9):8-9.(in Chinese).
[5]LAN K.Observation on the curative effect of 70 ingredients pearl pills on102 cases of nerve and cardiovascular disease[J].Journal of Medicine&Pharmacy of Chinese Minorities,1996,2(3):20-21.(in Chinese).
[6]ZHANG SS,LI B,HUANG ZJ,et al.Fingerprints analysis of the chemical components petroleum ether parts of Renqing Mangjue and Renqing Mangjue Compatible with Zouta[J].Medicinal Plant,2015,6(11-12):7-10.
[7]SUN M,YANG ZM,LI B,et al.Comparison of the content changes of strychnine and brucine in Renqingmangjue combined with or without Zuota by UPLC[J].Medicinal Plant,2013,5(1):33-36.
[2]Pharmacopoeia Commission of the People’s Republic of China.Chinese Pharmacopoeia[M].Beijing:Chemical Industry Press,2010.(in Chinese).
[3]ZHAN D,ZHAO JN.Modern research on Tibetan medicine prescription preparation and its clinical application[M].Chengdu:Sichuan Science and Technology Press,2009:470-471.(in Chinese).
[4]ZHU JB,SHI YB,LI XY.Modern study on Tibetan drug-"zuo ta"[J].Asia-Pacific Traditional Medicine,2014,10(9):8-9.(in Chinese).
[5]LAN K.Observation on the curative effect of 70 ingredients pearl pills on102 cases of nerve and cardiovascular disease[J].Journal of Medicine&Pharmacy of Chinese Minorities,1996,2(3):20-21.(in Chinese).
[6]ZHANG SS,LI B,HUANG ZJ,et al.Fingerprints analysis of the chemical components petroleum ether parts of Renqing Mangjue and Renqing Mangjue Compatible with Zouta[J].Medicinal Plant,2015,6(11-12):7-10.
[7]SUN M,YANG ZM,LI B,et al.Comparison of the content changes of strychnine and brucine in Renqingmangjue combined with or without Zuota by UPLC[J].Medicinal Plant,2013,5(1):33-36.