摘要
环境中的二氧化硫需要不间断监测,二氧化硫仪器的定期校准离不开气体标准物质,用重量法制备气体标准物质称量不确定度的准确计算是气体标准物质量值准确的保证。
Sulfur dioxide in the environment needs continuous monitoring. The regular calibration of sulfur dioxide instruments can not be separated from gas standard materials. The accurate calculation of the uncertainty of the standard weight of gas materials prepared by weight method is an accurate guarantee of the quality of gas standard materials.
引文
[1]韩永志,等.标准物质手册[G].北京:中国计量出版社,2016.
[2]GB/T 5274—2008气体分析校准用混合气体的制备称量法[S].
[3] ISO 6142-1:2015. Gas analysis-Preparation of calibration gas mixtures Part 1:Gravimetric method for Class I mixtures[S].
[4]GB/T 15000. 3—2008/ISO Guide 35:2006标准样品导则(3)标准样品定值的一般原则和统计方法[S].
[5]ISO/IEC Guide 98-3:2008 Guide to the Expression of Uncertainty in Measurement[S].
[6]ALINK A,VAN DER VEEN A M H. Uncertainty calculations for the preparation of primary gas mixtures[J].Metrologia,2000,37(6):641-650.
[7]JONES F E. The Air Density Equation and the Transfer of the Mass Unit[J]. J Res Nat Bur Stand,1978,83(5):419-428.
[8]GIACOMO P. Equation for the Determination of the Density of Moist Air(1981)[J]. Metrologia,1982,18(1):33-40.
[9]DAVIS R S. Equation for the Determination of the Density of Moist Air(1981/91)[J]. Metrologia,1992,29(1):67-70.