Microstructure Evolution of Extruded Mg-6Gd Alloy Under 175 ℃ and 150 MPa
|
摘要
The tensile creep behavior of extruded Mg-6 Gd alloy,having the tensile yield strength of～ 110 MPa at 175 ℃,has been investigated under 175 ℃ and 150 MPa. In this study, the extruded Mg-6 Gd sample exhibits the total tensile strain of ～10.5% after the creep time of 1100 h,and the fast plastic strain of ～4.6% at the beginning of the creep test. The microstructure result suggests that the dislocation deformation is the main deformation mode during creep, and the grains with orientation close to(0001) II ED disappear after creep. The creep process containing a low creep strain has no effective promotion for the precipitation compared with the aging process without strain. The origination of creep crack is related to the formation of precipitate-free zone during creep. The work offers an important implication to research the microstructure evolution under an applied stress in a weak aging response Mg alloy.
The tensile creep behavior of extruded Mg-6 Gd alloy,having the tensile yield strength of～ 110 MPa at 175 ℃,has been investigated under 175 ℃ and 150 MPa. In this study, the extruded Mg-6 Gd sample exhibits the total tensile strain of ～10.5% after the creep time of 1100 h,and the fast plastic strain of ～4.6% at the beginning of the creep test. The microstructure result suggests that the dislocation deformation is the main deformation mode during creep, and the grains with orientation close to(0001) II ED disappear after creep. The creep process containing a low creep strain has no effective promotion for the precipitation compared with the aging process without strain. The origination of creep crack is related to the formation of precipitate-free zone during creep. The work offers an important implication to research the microstructure evolution under an applied stress in a weak aging response Mg alloy.
The tensile creep behavior of extruded Mg-6 Gd alloy,having the tensile yield strength of～ 110 MPa at 175 ℃,has been investigated under 175 ℃ and 150 MPa. In this study, the extruded Mg-6 Gd sample exhibits the total tensile strain of ～10.5% after the creep time of 1100 h,and the fast plastic strain of ～4.6% at the beginning of the creep test. The microstructure result suggests that the dislocation deformation is the main deformation mode during creep, and the grains with orientation close to(0001) II ED disappear after creep. The creep process containing a low creep strain has no effective promotion for the precipitation compared with the aging process without strain. The origination of creep crack is related to the formation of precipitate-free zone during creep. The work offers an important implication to research the microstructure evolution under an applied stress in a weak aging response Mg alloy.
引文
[1]Y.M.Zhu,M.Z.Bian,J.F.Nie,Acta Mater.127,505(2017)
[2]R.G.Li,R.L.Xin,Q.Liu,J.A.Liu,G.Y.Fu,L.Zong,Y.M.Yu,S.G.Guo,Mater.Character.109,43(2015)
[3]J.Zheng,Z.Li,L.Tan,X.Xu,R.Luo,B.Chen,Mater.Character.117,76(2016)
[4]X.J.Wang,D.K.Xu,R.Z.Wu,X.B.Chen,Q.M.Peng,L.Jin,Y.C.Xin,Z.Q.Zhang,Y.Liu,X.H.Chen,G.Chen,K.K.Deng,H.Y.Wang,J.Mater.Sci.Technol.34,245(2018)
[5]P.J.Apps,H.Karimzadeh,J.F.King,G.W.Lorimer,Scr.Mater.48,1023(2003)
[6]J.F.Nie,X.Gao,S.M.Zhu,Scr.Mater.53,1049(2005)
[7]X.Gao,J.F.Nie,Enhanced precipitation-hardening in Mg-Gd alloys containing Ag and Zn.Scr.Mater.58,619(2008)
[8]K.Yamada,H.Hoshikawa,S.Maki,T.Ozaki,Y.Kuroki,S.Kamado,Y.Kojima,Scr.Mater.61,636(2009)
[9]Y.Hu,J.Deng,C.Zhao,F.Pan,J.Peng,J.Mater.Sci.46,5838(2011)
[10]Y.Hu,J.Deng,C.Zhao,J.Wang,F.Pan,Trans.Nonferrous Met.Soc.China 21,732(2011)
[11]J.F.Nie,Metall.Mater.Trans.A 43,3891(2012)
[12]Q.Peng,H.Dong,L.Wang,Y.Wu,L.Wang,Mater.Character.59,983(2008)
[13]G.Li,J.Zhang,R.Wu,Y.Feng,S.Liu,X.Wang,Y.Jiao,Q.Yang,J.Meng,J.Mater.Sci.Technol.34,1076(2018)
[14]A.P.Druzhkov,D.A.Perminov,Mater.Sci.Eng.A 527,3877(2010)
[15]J.Cˇ?′zˇek,I.Procha′zka,B.Smola,I.StulolaCˇ?′zˇek,J.Alloys Compd.430,92(2007)
[16]T.Honma,T.Ohkubo,S.Kamado,K.Hono,Acta Mater.55,4137(2007)
[17]H.Liu,W.F.Xu,L.M.Peng,W.J.Ding,J.F.Nie,Comput.Mater.Sci.130,152(2017)
[18]S.M.He,X.Q.Zeng,L.M.Peng,X.Gao,J.F.Nie,W.J.Ding,J.Alloys Compd.427,316(2007)
[19]R.G.Li,J.F.Nie,G.J.Huang,Y.C.Xin,Q.Liu,Scr.Mater.64,950(2011)
[20]K.Y.Zheng,J.Dong,X.Q.Zeng,W.J.Ding,Mater.Sci.Eng.A489,44(2008)
[21]W.H.Wang,D.Wu,R.S.Chen,X.N.Zhang,J.Mater.Sci.Technol.34,1236(2018)
[22]F.Guo,X.Luo,Y.Xin,G.Wu,Q.Liu,J.Alloys Compd.704,406(2017)
[23]M.Wang,R.Xin,B.Wang,Q.Liu,Mater.Sci.Eng.A 528,2941(2011)
[24]T.Homma,N.Kunito,S.Kamado,Scr.Mater.61,644(2009)
[25]N.Stanford,D.Atwell,M.R.Barnett,Acta Mater.58,6773(2010)
[26]H.Fu,B.Ge,Y.Xin,R.Wu,C.Fernandez,J.Huang,Q.Peng,Nano Lett.17,6117(2017)
[27]B.Jiang,C.H.Zhang,T.Wang,Z.Qu,R.Wu,M.Zhang,Mater.Des.34,863(2012)
[28]R.Wu,Y.Yan,G.Wang,L.E.Murr,W.Han,Z.Zhang,M.Zhang,Int.Mater.Rev.60,65(2015)
[29]Y.Xin,X.Zhou,Y.Wu,H.Yu,Q.Liu,Mater.Sci.Eng.A 640,118(2015)
[30]Y.Xin,L.Lv,H.Chen,C.He,H.Yu,Q.Liu,Mater.Sci.Eng.A662,95(2016)
[31]A.Chapuis,Q.Liu,Comput.Mater.Sci.97,121(2015)
[32]J.Sun,L.Jin,S.Dong,J.Dong,Z.Zhang,F.Wang,W.Ding,A.A.Luo,Mater.Des.122,164(2017)
[33]R.Li,R.Xin,A.Chapuis,Q.Liu,G.Fu,L.Zong,Y.Yu,B.Guo,S.Guo,Mater.Charact.112,81(2016)
[2]R.G.Li,R.L.Xin,Q.Liu,J.A.Liu,G.Y.Fu,L.Zong,Y.M.Yu,S.G.Guo,Mater.Character.109,43(2015)
[3]J.Zheng,Z.Li,L.Tan,X.Xu,R.Luo,B.Chen,Mater.Character.117,76(2016)
[4]X.J.Wang,D.K.Xu,R.Z.Wu,X.B.Chen,Q.M.Peng,L.Jin,Y.C.Xin,Z.Q.Zhang,Y.Liu,X.H.Chen,G.Chen,K.K.Deng,H.Y.Wang,J.Mater.Sci.Technol.34,245(2018)
[5]P.J.Apps,H.Karimzadeh,J.F.King,G.W.Lorimer,Scr.Mater.48,1023(2003)
[6]J.F.Nie,X.Gao,S.M.Zhu,Scr.Mater.53,1049(2005)
[7]X.Gao,J.F.Nie,Enhanced precipitation-hardening in Mg-Gd alloys containing Ag and Zn.Scr.Mater.58,619(2008)
[8]K.Yamada,H.Hoshikawa,S.Maki,T.Ozaki,Y.Kuroki,S.Kamado,Y.Kojima,Scr.Mater.61,636(2009)
[9]Y.Hu,J.Deng,C.Zhao,F.Pan,J.Peng,J.Mater.Sci.46,5838(2011)
[10]Y.Hu,J.Deng,C.Zhao,J.Wang,F.Pan,Trans.Nonferrous Met.Soc.China 21,732(2011)
[11]J.F.Nie,Metall.Mater.Trans.A 43,3891(2012)
[12]Q.Peng,H.Dong,L.Wang,Y.Wu,L.Wang,Mater.Character.59,983(2008)
[13]G.Li,J.Zhang,R.Wu,Y.Feng,S.Liu,X.Wang,Y.Jiao,Q.Yang,J.Meng,J.Mater.Sci.Technol.34,1076(2018)
[14]A.P.Druzhkov,D.A.Perminov,Mater.Sci.Eng.A 527,3877(2010)
[15]J.Cˇ?′zˇek,I.Procha′zka,B.Smola,I.StulolaCˇ?′zˇek,J.Alloys Compd.430,92(2007)
[16]T.Honma,T.Ohkubo,S.Kamado,K.Hono,Acta Mater.55,4137(2007)
[17]H.Liu,W.F.Xu,L.M.Peng,W.J.Ding,J.F.Nie,Comput.Mater.Sci.130,152(2017)
[18]S.M.He,X.Q.Zeng,L.M.Peng,X.Gao,J.F.Nie,W.J.Ding,J.Alloys Compd.427,316(2007)
[19]R.G.Li,J.F.Nie,G.J.Huang,Y.C.Xin,Q.Liu,Scr.Mater.64,950(2011)
[20]K.Y.Zheng,J.Dong,X.Q.Zeng,W.J.Ding,Mater.Sci.Eng.A489,44(2008)
[21]W.H.Wang,D.Wu,R.S.Chen,X.N.Zhang,J.Mater.Sci.Technol.34,1236(2018)
[22]F.Guo,X.Luo,Y.Xin,G.Wu,Q.Liu,J.Alloys Compd.704,406(2017)
[23]M.Wang,R.Xin,B.Wang,Q.Liu,Mater.Sci.Eng.A 528,2941(2011)
[24]T.Homma,N.Kunito,S.Kamado,Scr.Mater.61,644(2009)
[25]N.Stanford,D.Atwell,M.R.Barnett,Acta Mater.58,6773(2010)
[26]H.Fu,B.Ge,Y.Xin,R.Wu,C.Fernandez,J.Huang,Q.Peng,Nano Lett.17,6117(2017)
[27]B.Jiang,C.H.Zhang,T.Wang,Z.Qu,R.Wu,M.Zhang,Mater.Des.34,863(2012)
[28]R.Wu,Y.Yan,G.Wang,L.E.Murr,W.Han,Z.Zhang,M.Zhang,Int.Mater.Rev.60,65(2015)
[29]Y.Xin,X.Zhou,Y.Wu,H.Yu,Q.Liu,Mater.Sci.Eng.A 640,118(2015)
[30]Y.Xin,L.Lv,H.Chen,C.He,H.Yu,Q.Liu,Mater.Sci.Eng.A662,95(2016)
[31]A.Chapuis,Q.Liu,Comput.Mater.Sci.97,121(2015)
[32]J.Sun,L.Jin,S.Dong,J.Dong,Z.Zhang,F.Wang,W.Ding,A.A.Luo,Mater.Des.122,164(2017)
[33]R.Li,R.Xin,A.Chapuis,Q.Liu,G.Fu,L.Zong,Y.Yu,B.Guo,S.Guo,Mater.Charact.112,81(2016)