化学多维校正辅助色谱波谱联用技术开展精准定量分析研究
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摘要
<正>近年来,利用化学计量学方法所具有的数学分离功能辅助提高色谱联用技术及多维色谱的定性定量分析能力的相关工作时有报道,本实验室利用化学多维校正方法已有若干开创性探索,并取得了系列创新性成果。近期进展列举如下:1)运用交替三线性分解(ATLD)方法解析HPLC-DAD产生的三维响应数据,借助二阶校正方法所特有的二阶优势:即使包含有共流出组分和重叠光谱情况亦能获得复杂样本中感兴趣组分的准
引文
[1]Zhi Liu,Hai-Long Wu*,Yan-Mei Sun,Min Zhai,Xiao-Li Yin,Ru-Qin Yu.Rapid and simultaneous determination of five vinca alkaloids in catharanthus roseus and human serum using trilinear component modeling of liquid chromatography-diode array detection data.Journal of Chromatography B,2016,In Press,Corrected Proof,Available online 14 August 2015.
[2]Shou-Xia Xiang,Hai-Long Wu*,Chao Kang,Li-Xia Xie,Xiao-Li Yin,Hui-Wen Gu,Ru-Qin Yu.Fast quantitative analysis of four tyrosine kinase inhibitors in different human plasma samples using three-way calibration assisted liquid chromatography with diode array detection.Journal of Separation Science,2015,38:2781-2788.
[3]Hui-Wen Gu,Hai-Long Wu*,Xiao-Li Yin,Shan-Shan Li,Ya-Juan Liu,Hui Xia,Li-Xia Xie,Ru-Qin Yu,Peng-Yuan Yang**,Hao-Jie Lu.Solving signal instability to maintain the second-order advantage in the resolution and determination of multi-analytes in complex systems by modeling liquid chromatography-mass spectrometry data using alternating trilinear decomposition method assisted with piecewise direct standardization.Journal of Chromatography A,2015,1407:157-168.
[4]Chao Kang,Hai-Long Wu*,Jing-Jing Song,Hui Xu,Ya-Juan Liu,Yong-Jie Yu,Xiao-Hua Zhang,Ru-Qin Yu.A flexible trilinear decomposition algorithm for three-way calibration based on the trilinear component model and a theoretical extension of the algorithm to the multilinear component model.Analytica Chimica Acta,2015,878:63-77.
[5]Xiang-Dong Qing,Hai-Long Wu*,Xi-Hua Zhang,Yong Li,Hui-Wen Gu,Ru-Qin Yu.A novel fourth-order calibration method based on alternating quinquelinear decomposition algorithm for processing high performance liquid chromatography-diode array detection-kinetic-p H data of naptalam hydrolysis.Analytica Chimica Acta,2015,861:12-24.
[6]Hai-Long Wu,Yong Li,Chao Kang,Ru-Qin Yu*.Chapter 3.Multiway Calibration Based on Alternating Multilinear Decomposition.In:Alejandro C.Olivieri,Graciela M.Escandar,Héctor C.Goicoechea,Arsenio Mu?oz de la Pe?a,Eds.,Fundamentals and Analytical Applications of Multi-way Calibration.Elsevier,2015,pp83-166(ISBN 978-0-444-63527-3).
[7]Hai-Long Wu,Chao Kang,Yong Li,Ru-Qin Yu*.Chapter 4.Practical Analytical Applications of Multiway Calibration Methods Based on Alternating Multilinear Decomposition.In:Alejandro C.Olivieri,Graciela M.Escandar,Héctor C.Goicoechea,Arsenio Mu?oz de la Pe?a,Eds.,Fundamentals and Analytical Applications of Multi-way Calibration.Elsevier,2015,pp167-246(ISBN 978-0-444-63527-3).
[2]Shou-Xia Xiang,Hai-Long Wu*,Chao Kang,Li-Xia Xie,Xiao-Li Yin,Hui-Wen Gu,Ru-Qin Yu.Fast quantitative analysis of four tyrosine kinase inhibitors in different human plasma samples using three-way calibration assisted liquid chromatography with diode array detection.Journal of Separation Science,2015,38:2781-2788.
[3]Hui-Wen Gu,Hai-Long Wu*,Xiao-Li Yin,Shan-Shan Li,Ya-Juan Liu,Hui Xia,Li-Xia Xie,Ru-Qin Yu,Peng-Yuan Yang**,Hao-Jie Lu.Solving signal instability to maintain the second-order advantage in the resolution and determination of multi-analytes in complex systems by modeling liquid chromatography-mass spectrometry data using alternating trilinear decomposition method assisted with piecewise direct standardization.Journal of Chromatography A,2015,1407:157-168.
[4]Chao Kang,Hai-Long Wu*,Jing-Jing Song,Hui Xu,Ya-Juan Liu,Yong-Jie Yu,Xiao-Hua Zhang,Ru-Qin Yu.A flexible trilinear decomposition algorithm for three-way calibration based on the trilinear component model and a theoretical extension of the algorithm to the multilinear component model.Analytica Chimica Acta,2015,878:63-77.
[5]Xiang-Dong Qing,Hai-Long Wu*,Xi-Hua Zhang,Yong Li,Hui-Wen Gu,Ru-Qin Yu.A novel fourth-order calibration method based on alternating quinquelinear decomposition algorithm for processing high performance liquid chromatography-diode array detection-kinetic-p H data of naptalam hydrolysis.Analytica Chimica Acta,2015,861:12-24.
[6]Hai-Long Wu,Yong Li,Chao Kang,Ru-Qin Yu*.Chapter 3.Multiway Calibration Based on Alternating Multilinear Decomposition.In:Alejandro C.Olivieri,Graciela M.Escandar,Héctor C.Goicoechea,Arsenio Mu?oz de la Pe?a,Eds.,Fundamentals and Analytical Applications of Multi-way Calibration.Elsevier,2015,pp83-166(ISBN 978-0-444-63527-3).
[7]Hai-Long Wu,Chao Kang,Yong Li,Ru-Qin Yu*.Chapter 4.Practical Analytical Applications of Multiway Calibration Methods Based on Alternating Multilinear Decomposition.In:Alejandro C.Olivieri,Graciela M.Escandar,Héctor C.Goicoechea,Arsenio Mu?oz de la Pe?a,Eds.,Fundamentals and Analytical Applications of Multi-way Calibration.Elsevier,2015,pp167-246(ISBN 978-0-444-63527-3).