车用氮氧化物传感器片芯制备的温等静压工艺研究
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- 英文论文题名：Study on Warm Isostatic Lamination Technological of NOx Sensor Ceramic Chip
- 论文作者：张斌 ; 王金兴 ; 刘宏宇 ; 常潇然 ; 韩建 ; 崔龙 ; 张克金
- 英文论文作者：Zhang Bin ; Wang Jinxing ; Liu Hongyu ; Chang Xiaoran ; Han Jian ; Cui Long ; Zhang Kejin ; China FAW Co. ; Ltd R&D Center
- 年：2016
- 作者机构：中国第一汽车股份有限公司技术中心;
- 论文关键词：氮氧化物传感器 ; 温等静压 ; 工艺参数
- 英文论文关键词：NO_x sensor ; warm isostatic lamination ; technological parameter
- 会议召开时间：2016-10-26
- 会议录名称：2016中国汽车工程学会年会论文集
- 英文会议录名称：Proceedings of 2016 SAE-China Congress
- 语种：中文
- 分类号：U464.134.4;U463.6
- 学会代码：QCGC
- 会议名称：2016中国汽车工程学会年会暨展览会
- 会议地点：中国上海
- 主办单位：中国汽车工程学会
- 学会名称：中国汽车工程学会
- 页数：4
- 文件大小：957k
- 原文格式：O
- 会议级别：全国
摘要
本文针对车用片式氮氧化物传感器片芯制备的温等静压工艺参数进行研究。利用光学显微镜检测片芯腔室端面形状;万能实验机测试片芯机械强度;微反配气系统对片芯进行气敏性能测试;分析了温等静压过程中不同阶段的工艺流程和参数对片芯成型结果的影响。通过调整工艺参数为压力15MPa、预热时间15min、静压温度70℃、恒压时间10min,实现了多片层、多种材料、多腔室的片式氮氧化物传感器片芯的温等静压成型。制备了腔室端面边缘整齐完整、腔室功能完整、机械强度符合使用要求的片芯。
In this paper,technological parameters of NOx sensor ceramic chip were studied.The edge of chamber in the ceramic chip was tested with an optical microscope;the mechanical strength of the ceramic was tested by an universal testing machine;and gassensing property was tested with a micro- dynamic dilution system.Based on the experimental results,the effects of different technological processes and parameters on the forming process of ceramic chip are analyzed.And by adjusting the parameters of warm isostatic lamination process which were treated at 70℃ for 15 min,followed by keeping the pressure by 15 MPa for 10 min.we had prepared the ceramic chip of NOx sensor,the chamber is complete inside and the edge of chamber is also neat and complete,which meets the requirements of use.
In this paper,technological parameters of NOx sensor ceramic chip were studied.The edge of chamber in the ceramic chip was tested with an optical microscope;the mechanical strength of the ceramic was tested by an universal testing machine;and gassensing property was tested with a micro- dynamic dilution system.Based on the experimental results,the effects of different technological processes and parameters on the forming process of ceramic chip are analyzed.And by adjusting the parameters of warm isostatic lamination process which were treated at 70℃ for 15 min,followed by keeping the pressure by 15 MPa for 10 min.we had prepared the ceramic chip of NOx sensor,the chamber is complete inside and the edge of chamber is also neat and complete,which meets the requirements of use.
引文
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[2]尹亮亮.基于氧化锆电解质的NOx传感器的检测系统设计[J].传感器世界,2011(02)16-19.
[3]谌启明.热等静压技术的发展及应用[J].稀有金属与硬质合金,2003,31,2,33-38.
[4]王景道.极限电流型氧敏元件测试系统设计[J].仪表技术与传感器,2006,20,11,47-48.
[5]王金兴.平板极限电流型氧传感器温等静压工艺研究及氧敏性能测试[J].2015中国汽车工程学会年会论文集,2015CG-EE020.